• Title/Summary/Keyword: Material mixing method

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Catalytic growth of carbon nanotubes using plasma enhanced chemical vapor deposition(PECVD) (플라즈마 화학 증착법을 이용한 탄소나노튜브의 촉매 성장에 관한 연구)

  • 정성회;장건익
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.935-938
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    • 2001
  • Carbon nanotubes(CNTs) was successfully grown on Ni coated silicon wafer substrate by applying PECVD technique(Plasma Enhanced Chemical Vapor Deposition). As a catalyst, Ni thin film of thickness ranging from 15∼30nm was prepared by electron beam evaporator method. In order to find the optimum growth condition, the type of the gas mixture such as C$_2$H$_2$-NH$_3$was systematically investigated by adjusting the gas mixing ratio in temperature of 600$^{\circ}C$ under the pressure of 0.4 torr. The diameter of the grown CNTs was 40∼150nm. As NH$_3$etching time increased the diameters of the nanotubes decreased whereas the density of nanotubes increased. TEM images clearly demonstrated synthesized nanotubes was multiwalled. We investigated electrical properties for the application of FED.

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Effect of CNT Diameter on Physical Properties of Styrene-Butadiene Rubber Nanocomposites

  • Park, Young-Soo;Huh, Mong-Young;Kang, Sin-Jae;Yun, Seok-Il;Ahn, Kay-Hyeok
    • Carbon letters
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    • v.10 no.4
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    • pp.320-324
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    • 2009
  • We investigated the effect of diameter and content of carbon nanotubes (CNTs) on the physical properties of styrenebutadiene rubber (SBR)/CNTs nanocomposites. CNTs-reinforced SBR nanocomposites were prepared by the melt mixing process. CNTs with different diameters were synthesized by the chemical vapor deposition method (CVD). In this work, the mechanical property and other physical properties of SBR/CNTS nanocomposites were discussed as a function of the content and diameter of CNTs.

The Manufacturing and Analysis of Planar Dielectric materials for Integrated LC Resonant Module (집적 LC공진 모듈용 평판 유전체의 제조와 물성)

  • Park, Woo-Young;Kim, Jong-Ryung;An, Yong-Woon;Oh, Young-Woo;Kim, Hyun-Sik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07a
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    • pp.497-501
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    • 2003
  • In order to manufacture ceramic capacitors for the industrial electronic parts application using Tape casting method, the dielectric properties as a functions of sintering temperatures and the fabrication conditions of green sheet were investigated to consider the possibility of applications. When the mixing ratio of powder and solvent in slurry was 65:35, the uniform and dense green sheets was obtained. The dielectric constant was increased as the sintering temperature Over 94% of relative density and high were obtained to the specimens sintered at $1000^{\circ}C$. We can find that the device sintered at higher temperature than $1000^{\circ}C$ showed the relative density over 94% and the dielectric constant over 2000.

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Standardization for $Cr^{+6}$ analysis in cement and concrete (시멘트 및 콘크리트의 크롬분석 표준화에 관한 연구)

  • Park, Nam-Kyu;Song, Hun;Chu, Yong-Sik;Lee, Jong-Kyu
    • Proceedings of the Korea Concrete Institute Conference
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    • 2006.11a
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    • pp.729-732
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    • 2006
  • Portland cement is presently the most widely used construction material. The process of manufacture of cement consists essentially of grinding the raw materials, mixing them intimately proportions and burning in a rotary kiln at a temperature of up to about $1450^{\circ}C$. Raw materials have used limestone, clay, silica, and iron oxide and fuel have used bituminous coal. Recently, A standpoint of the recycling of material resources, the production of cement use of industrial waste and residual products. Therefore, the final product of cement were included heavy metals such as $Cr^{+6}$ and Pb. The purpose of this study is standardization for $Cr^{+6}$ analysis in cement and concrete. From the comparative study of the examination method of $Cr^{+6}$ analysis, Japan cement association standard of $Cr^{+6}$ analysis is most suitable for the real state of affairs in korea.

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A Study on the Thermal Performance change due to amount of Carbon Fiber in Poly-Urea Waterproofing Material (폴리우레아 방수재의 탄소섬유함량에 따른 내열성능 변화추이 연구)

  • Park, Wan-Goo;Park, Jin-Sang;Choi, Su-Young;Kim, Dong-Bum;Kim, Byoung-Il;Oh, Sang-Keun
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2017.11a
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    • pp.126-127
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    • 2017
  • This study investigates the effect of improving the heat resistance performance when carbon fiber is mixed in the polyurea coating material. A tensile strength test method was carried out with the carbon fiber mixed polyurea specimens at an interval of 7, 14, and 21 days after heat treatment at 140±2℃. The test results showed that there was a significant decrease in the tensile strength performance. While the elongation and tensile performance decreased greatly, it was confirmed nevertheless the overall performance was maintained. This study proposes that mixing carbon fiber to the polyurea resin can effectively secure long-term heat resistance, thereby solving the problem of deterioration of physical properties caused by exposure to ultraviolet rays.

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직류 전계하 LLDPE/EVA혼합필름의 절연파괴특성

  • 고시현;김형주;이종필;신현택;이충호;홍진웅
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.11a
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    • pp.65-68
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    • 2000
  • Polyethylene, has long history and is widely used, was researched due to good electrical properties by many authors. But PE under stress has the critical defects of space charge accumulation and tree growth, so various methods such as catalyst, additives and blend to improve these problems have been execute, of which we selected blending method. As in our previous papers we investigated electrical conduction, dielectric and AC dielectric breakdown characteristics, we did DC dielectric breakdown characteristics in this paper. We selected pure LLDPE, pure EVA and LLDPE films mixed with EVA as specimens, which were mixed with the weight percentages of 50, 60, 70 and 80[wt%] to be thin film. DC applying voltage speed was 500[V/sec]. The relation between dielectric breakdown characteristics and the variations of super structure due to mixing was investigated, and especially trap level at amorphous region, threshold energy increment of conductive electron at free volume were considered.

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Analysis of Bonding Interfaces between Cemented Carbide and Stainless Steel made via Hot Vacuum Brazing (고온 진공 브레이징을 이용한 초경합금과 스테인리스강의 접합 계면 특성)

  • Park, D.H.;Hyun, K.H.;Kwon, H.H.
    • Transactions of Materials Processing
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    • v.29 no.6
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    • pp.307-315
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    • 2020
  • The cemented carbide and stainless steel were bonded using a hot-vacuum brazing method to analyze the bonding interface. Since it is suitable for the hot vacuum brazing, nickel metal was used as a binder among the main components of the cemented carbide, and a new cemented carbide material was developed by adjusting the alloy composition. The paste, which is one of the important factors affecting the hot vacuum brazing bonding, was able to improve brazing adhesion by mixing solder as Ni powder and a binder as an organic compound at an appropriate ratio. Division of the stainless steel yielded a dense brazing result. This study elucidated the interfacial characteristics of wear-resistant parts by bonding stainless steel and cemented carbide via hot vacuum brazing.

THE ABSORPTION PROPERTIES OF Cu-Zn FERRITE/RUBBER COMPOSITE MICROWAVE ABSORBER WITH PZT ADDITIVE

  • Shin, Kwang-Ho;Geon, Sa-Gong
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.556-560
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    • 1995
  • The absorption properties of Cu-Zn ferrite/rubber composite microwave absorbers with PZT(Lead Zirconate Titanate) additive were evaluated. The composite specimens have prepared by molding and curing the mixture of matrix rubber and Cu-Zn ferrite powders which are synthesized by the coprecipitation method using Fe Cl/sub 3/ .center dot. 6H/sub 2/O, CuCl/sub 2/ .center dot. 2H/sub 2/O and Zn Cl/sub 2/ as a starting raw materials. PZT is used as another filler particles to adjust the material constants of Cu-Zn ferrite/rubber composite specimens. We have found that the material constants of specimens could be controlled by various PZT mixing ratio. On the Cu-Zn ferrite/rubber composite specimens with PZT 10[wt%] additive, the reflection losses were larger than 30[dB] in the frequency range from 2.72 to 4.4[GHz]' by adjusing the thickness.

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Electrochemical Characteristics of TiO2 Photoelectrode for DSSC Prepared by Sol-gel Method (졸겔법에 의한 DSSC 광전극의 전기화학적 특성)

  • Park, A-Reum;Jin, En Mei;Gu, Hal-Bon
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.25 no.4
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    • pp.315-320
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    • 2012
  • In general, a photoelectrode in DSSC(dye sensitized solar cell) are fabricated by using the $TiO_2$ (Titanium dioxide) to realize high efficiency and the efficiency of DSSC is affected by the size, the shape and the property of $TiO_2$. We synthesized the crystalline $TiO_2$ by sol-gel method. In spite of many merits, only weakness for the sol-gel method is taking many process times. To solve this problem, we reduced the fabricating processes. The reduced process is the making process that is $TiO_2$ sol to $TiO_2$ powder with including of two heat treatment and two mixing. We could simplify the process by preparing $TiO_2$ sol to $TiO_2$ paste directly. As a result, DSSC fabrication process is simplified and we have obtained the efficiency best result 3.88% with $V_{OC}$=0.71 V, $J_{SC}=8.70\;mA/cm^{-2}$, and FF=62.37%, respectively.

Engineering Characteristic of High Density Expansion Materials for Structure Restoration Technology (기초침하복원을 위한 급속 팽창재료의 공학적 특성에 관한 연구)

  • Shin, Eun-Chul;Cha, Yong-In
    • Journal of the Korean Geosynthetics Society
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    • v.7 no.2
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    • pp.1-5
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    • 2008
  • The differential settlement on ordinary concrete buildings and paved roads are often occurred and which caused the failure of structure. The grouting method can be used for correcting the settlement of the structure. However, the grouting method has a disadvantage like that it takes a long time period to get a desired strength, and it is not a continuous in the phase of reinforced effect. In this paper, as an injecting material called GPCON to complement disadvantage, it is estimated about the characteristic that has a high-density expansion. With the changing of ground conditions and amount of injection, the change of physical strength on compression, the stability against chemical material are studied through the filming of SEM. The physical strength with compression is developed to high strength due to mixing with other material. It is not react with most of the material on chemical conditions except the component of alcohol. Through the SEM test. it is confirmed that the strength of material was increased as formation is being densified.

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