• Corrosion Science and Technology
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• v.7 no.3
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• pp.182-186
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• 2008

The microstructures of the oxide scale developed at high temperature on steels are very complex and their development depends on many factors including time, temperature, oxidation conditions and alloying elements. The classical model of an oxide scale on steel consisting of wüstite, magnetite and haematite layers, is more complicated in reality and its properties change with the factors that affect their development. An understanding of the oxide scale formation and its properties can only be achieved by careful examination of the scale microstructure. The oxide scale microstructure may be difficult to characterise by conventional techniques such as optical or standard scanning electron microscopy. An unambiguous characterisation of the scale and the correct identification of the phases within the scale are difficult unless the crystallographic structure for each phase in the scale is considered and a simultaneous microstructure-microtexture analysis is carried out. In the current study Electron Backscatter Diffraction (EBSD) has been used to investigate the microstructure of iron oxide layers grown on low carbon steels at different times and temperatures. EBSD has proved to be a powerful technique for identifying the individual phases in the oxide scale accurately. The results show that different grain shapes and sizes develop for each phase in the scale depending on time and temperature.

• Journal of the Korean institute of surface engineering
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• v.43 no.4
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• pp.205-210
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• 2010

The A106 Gr B low carbon steel, which was used in the electric power plants and heavy chemical plants, was welded by multi-pass arc welding. The heat affected zone (HAZ) formed by welding was corroded in acid chloride solution, or in saturated $H_2S$ containing acid chloride solution, or in saturated $H_2S$ containing acid chloride solution under applied current. In this order of corrosion solution, the rate of corrosion increased, because $H_2S$ accelerated the iron dissolution, hydrogen evolution, and the formation of nonprotective FeS, whereas the applied current accelerated the electrochemical reaction. The scales formed in acid chloride solution consisted primarily of $Fe_3O_4$, while those formed in $H_2S$ containing acid chloride solution consisted primarily of $Fe_3O_4$ and FeS.

• Korean Journal of Materials Research
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• v.21 no.6
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• pp.303-308
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• 2011

The effect of heat treatment on the micro-structures and the mechanical properties of 0.002% boron added low carbon steel was investigated. The tensile strength reached the peak at about $880-890^{\circ}C$ with the rising quenching temperature and then the hardness decreased sharply, but the tensile strength hardly decreased. The tensile and yield strength decreased and the total elongation increased with a rising tempering temperature, but the tensile and yield strength sharply fell and the total elongation prominently increased from above a $400-450^{\circ}C$ tempering temperature. Tempered martensite embrittlement (TME) was observed at tempering condition of $350-400^{\circ}C$. In the condition of quenching at $890^{\circ}C$ and tempering at $350^{\circ}C$, the boron precipitates were observed as Fe-C-B and BN together. The hardness decreased in proportion to the tempering temperature untill $350^{\circ}C$ and dropped sharply above $400^{\circ}C$ regardless of the quenching temperature.

• Journal of the Korean Society for Precision Engineering
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• v.8 no.2
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• pp.27-35
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• 1991

We propose the crack growth rate equation which applied over three regions (threshold region, stable region, unstable region) of fatigue crack propagation. Constant stress amplitude fatigue tests are conducted for four materials under three stress ratios of R=0.05, R=0.2 and R=0.4. Materials which have different mechanical properties i.e. stainless steel, low carbon steel, medium carbon steel and aluminum alloy are used. The fatigue crack growth rate equation is given by $da/dN={\beta} (1-R)^{\delta}\({\DELTA}K-{\DELTA}K_t)^{\alpha} / (K_{cf}-K_{max})$${\alpha}, {\beta}$ , and ${\delta}$ are constants, and ${\Delta}K_t$ is stress intensity factor range at low ${\Delta}K$ region. The constants are obtained from nonlinear least square method. $K_{ef}$is critical fatigue stress intensity factor. The relation between half crack length and number of cycles obtained by integrating the crack growth rate equation is in agreement with the experimental data. It is also experimented with constant maximum stress and decreasing stress ratios, and the fatigue growth rate of each material is in accord with the proposed equation.

• Journal of the Korean institute of surface engineering
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• v.55 no.1
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• pp.18-23
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• 2022

Presence of cracks in electrodeposited hard chromium layer, which provide a path of corrosive media to steel substrate, is a serious issue in metal finishing with chromium electroplating. In this study, we added sodium molybdate in an electrolyte for chromium electroplating bath. 130g/L of sodium molybdate in Sargent bath for chromium electroplating causes a codepostion of molybdenum with chromium in a rage of 0.61 ~ 3.14 wt.%. The co-deposited molybdenum enhances the crystallinity of chromium layer, thus the hardness is slightly decreases by the addition of molybdate in electrolyte. However, due to the co-deposition of molybdenum, a crack-free chromium layer could be electrodeposited. Such crack-free chromium layer shows a significantly improved corrosion resistance.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.14 no.2
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• pp.59-68
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• 2018

This study compares true stress-true strain curves obtained by tensile tests of various piping materials with bi-linear stress-strain approximation suggested in the JSME Code Case(CC) Draft, a guideline for piping seismic inelastic response analysis. Based on the comparisons, the reliability of the bi-linear approximation is evaluated. It is found that bi-linear stress-strain curve of TP316 stainless steel is in good agreement with its true stress-true strain curve. However, Bi-linear stress-strain curves of TP304 stainless steel and carbon steels determined by the approximation cannot appropriately estimate their stress-strain behavior. Accordingly new bi-linear approximations for carbon steels and low-alloy steels are proposed. The proposed bi-linear approximations for carbon and low-alloy steels, which include the temperature effect on strength and hardening of material, estimate their stress-strain behavior reasonably well.

• Korean Journal of Materials Research
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• v.3 no.1
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• pp.43-49
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• 1993

Excellent deep drawability and strain aging rsistance are obtained by the addition of alloying elements such as Ti and Nb which can form carbide and nitride easily into Al killed extra low carbon steel. Recrystallization textures and mechanical properties of the three different extra low carbon steels with B containing Nb only, Ti only, and both Nb and Ti, respectively, along with have been compared. Inverse pole figure shows that (100) and (111) texture intensities of Nb containing steel changed a lot during the annealing treatment and the degree of texture-structural change in the steel containing both Nb and Ti is about the same as that in the Ti-containing 5teel. After annealing the pole figure shows that the {Ill} < 110 > and {112} < 110> textures are the strongest in the cold rolled state and the annealed state, respectively. However, there is little difference in texture structure among the three kinds of steels. There is a tendency that the steel containing both Nb and Ti the grain size of which is the smallest is the highest in hardness. Nb-containing steel is the next and Ti -containing steel is the last in hardness.

• Transactions of the Korean Society of Mechanical Engineers
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• v.6 no.2
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• pp.107-112
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• 1982

In order to analyze and investigate in the fatigue behavior of the notched specimens under the two level stressing, the U-notched specimens of structural carbon steel which is generally used is prepared. The obtained results are summarized as follows; (1) The fatigue limit of the U-notched specimens is lower than that of the unnotched. The fatifue notch factor (.betha.) of the U-notched specimens is 1.44 for mild steel and 1.52 for harden steel. The notch sensitivity (q) is 0.68 for mild steel and o.8 for harden steel. That is, these facts show that harden steel is more sensitive to the notch than mild steel. (2) The fatigue life time of the U-notched specimens under the overstressing is shorter than under the constant stressing, and the degree of fatigue life time decrease is different to each stress level; the degree for the high stress level is more than for the low stress level. (3) The fatigue life time of the U-notched specimes under the understressing is longer than under the constant stressing, and the degree of fatigue life time increase for the low stress level is more than for the high stress level.

• Corrosion Science and Technology
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• v.22 no.4
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• pp.273-286
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• 2023

Rebar is embedded in concrete to create reinforced concrete (RC). Rebar carries most of the tensile stress and gives compressively loaded concrete fracture resistance. However, embedded steel corrosion is a significant cause of concern for RC composite structures worldwide. It is one of the biggest threats to concrete structures' longevity. Due to environmental factors, concrete decays and reinforced concrete buildings fail. The type and surface arrangement of the rebar, the cement used in the mortar, the dosing frequency of the concrete, its penetrability, gaps and cracks, humidity, and, most importantly, pollutants and aggressive species all affect rebar corrosion. Either carbonation or chlorides typically cause steel corrosion in concrete. Carbonation occurs when carbon dioxide in the atmosphere combines with calcium within the concrete. This indicates that the pH of the medium is falling, and the steel rebar is corroding. When chlorides pass through concrete to steel, corrosion rates skyrocket. Consideration must be given to concrete moisture. Owing to its excellent resistance, dry concrete has a low steel corrosion rate, whereas extremely wet concrete has a low rate owing to delayed O₂ transfer to steel surfaces. This paper examines rebar corrosion causes and mechanisms and describes corrosion evaluation and mitigation methods.

• Tribology and Lubricants
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• v.9 no.1
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• pp.62-69
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• 1993

Friction and wear behavior of a carbon/carbon composite material for aircraft brake material was experimentally investigated. Friction and wear test setup was designed and built for the experiment. Friction and wear tests were conducted under various sliding conditions. Friction coefficients were measured and processed by a data acquisition system and amount of wear measured by a balance. Stainless steel disk was used as the counterface material. Temperature was also measured by inserting thermocouple 2.5 mm beneath the sliding surface of the carbon/carbon composite specimen. Wear surfaces were observed by SEM, and analyzed by EDAX. The experimental results showed that sliding speed and normal force did not have significant effects on friction coefficient and wear factor of the composite. Temperature increase just below the surface was not large enough to cause any thermal degradation or oxidation which occurred at higher temperature when tested by TGA. Wear film was generated both on the specimen and on the counterface at relatively low sliding speed but cracks, grooves, and wear debris were observed at high sliding speed. Friction coefficient remained almost constant when the sliding speed or normal load was varied. It is believed that the adhesive and abrasive components contributed mainly to the friction coefficient. Wear behavior at low sliding speed was governed by wear film formation and adhesive wear mechanism. At high speed, fiber orientation, ploughing by counterface asperities, and fiber breakage dominated wear of the carbon/carbon composite.