• Title/Summary/Keyword: Linearity and response time

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Determination of Polar Secondary Metabolomes in Arabidopsis thaliana using High Performance Liquid Chromatography Coupled with Tandem Mass Spectrometry

  • Cho, Young-Ah;Park, Se-min;Bae, Dong-Won;Seo, On-Nuri;Lee, Ji-Eun;Jeong, Sung-Woo;Kwon, Young-Sang;Cha, Jae-Yul;Bae, Han-Hong;Shin, Sung-Chul
    • Journal of agriculture & life science
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    • v.46 no.6
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    • pp.165-171
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    • 2012
  • As a preceding study for investigating the influence of sound wave stimulus on Arabidopsis thaliana metabolomics, the polar secondary metabolomes of the plant were determined using high performance liquid chromatography coupled with tandem mass spectrometry. A total of 10 polar secondary metabolomes were characterized and quantified. Among them, 4 metabolomes, p-coumaroylagmatine isomer (7 and 8), p-coumaroylagmatine isomer (9 and 10) were identified in the plant for the first time. The validation was conducted in terms of linearity, recovery, precision, limit of detection (LOD) and limit of quantification (LOQ). The validated method was applied to the simultaneous quantification of the 10 polar secondary metabolomes.

Experimental and numerical investigations into the composite behaviour of steel frames and precast concrete infill panels with window openings

  • Teeuwen, P.A.;Kleinman, C.S.;Snijder, H.H.;Hofmeyer, H.
    • Steel and Composite Structures
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    • v.10 no.1
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    • pp.1-21
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    • 2010
  • As an alternative for conventional structures for tall buildings, a hybrid lateral load resisting structure has been designed, enabling the assembly of tall buildings directly from a truck. It consists of steel frames with discretely connected precast concrete infill panels provided with window openings. Besides the stiffening and strengthening effect of the infill panels on the frame structure, economical benefits may be derived from saving costs on materials and labour, and from reducing construction time. In order to develop design rules for this type of structure, the hybrid infilled frame has recently been subjected to experimental and numerical analyses. Ten full-scale tests were performed on one-storey, one-bay, 3 by 3 m infilled frame structures, having different window opening geometries. Subsequently, the response of the full-scale experiments was simulated with the finite element program DIANA. The finite element simulations were performed taking into account non-linear material characteristics and geometrical non-linearity. The experiments show that discretely connected precast concrete panels provided with a window opening, can significantly improve the performance of steel frames. A comparison between the full-scale experiments and simulations shows that the finite element models enable simulating the elastic and plastic behaviour of the hybrid infilled frame.

Development of a hygroscopic polymer-coated QCM humidity sensor and its characteristics (감습 고분자막이 코팅된 수정미소저울 습도센서 제작 및 특성연구)

  • Kwon, Su-Yong;Kim, Jong-Chul;Choi, Byung-Il;Nham, Hyun-Soo
    • Journal of Sensor Science and Technology
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    • v.14 no.6
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    • pp.395-401
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    • 2005
  • A highly stable quartz crystal microbalance (QCM) that showed a stability of frequencies and exhibited a very low noise level has been developed. The long-term drift was <0.05 Hz/h over a period of 10 h, and the short-term rms (root mean square) noise was <0.015 Hz. Our QCM sensor was used as a humidity sensor employing a poly(methyl methacrylate) (PMMA) polymer film as a hygroscopic layer, which showed good characteristics in the relative humidity (RH) range of $2{\sim}90%$ RH. Comparing the characteristics of the QCM sensor with those of other types of humidity sensors employing PMMA film as a hygroscopic layer, and with other QCM sensors employing other hygroscopic layers is represented.

Thermopiezoelastic Nonlinear Dynamic Characteristics of Piezolaminated Plates (압전적층판의 열-압전-탄성 동적 비선형 작동특성)

  • Oh, Il-Kwon
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.15 no.7 s.100
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    • pp.836-842
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    • 2005
  • Nonlinear dynamic characteristics of active piezolaminated plates are investigated with respect to the thermopiezoelastic behaviors. For largely deformed structures with small strain, the incremental total Lagrangian formulation is presented based on the virtual work principles. A multi-field layer-wise finite shell element is proposed for assuring high accuracy and non-linearity of displacement, electric and thermal fields. For dynamic consideration of thermopiezoelastic snap-through phenomena, the implicit Newmark's scheme with the Newton-Raphson iteration is implemented for the transient response of various piezolaminated models with symmetric or eccentric active layers. The bifurcate thermal buckling of symmetric structural models is first investigated and the characteristics of piezoelectric active responses are studied for finding snap-through piezoelectric potentials and the load-path tracking map. The thermoelastic stable and unstable postbuckling, thermopiezoelastic snap-through phenomena with several attractors are proved using the nonlinear time responses for various initial conditions and damping loss factors. Present results show that thermopiezoelastic snap-through phenomena can result in the difficulty of buckling and postbuckling control of intelligent structures.

ZnO thin film Gas sensors for detection of TMA gas with Pt/Ti thin film heater (Pt/Ti 발열체가 내장된 TMA 가스 측정용 ZnO 박막 가스 센서)

  • 류지열;박성현;최혁환;권태하
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.33A no.6
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    • pp.127-135
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    • 1996
  • To increase the sensitivity and the selectivity of the sensors to TMA gas, the composition ratio and the growth conditions of the ZnO films are studied. Annealing of the ZnO films in the various time ranges and temperatures in the oxygen is carried out to enhance the stbility of the electrical resistance. Pt/Ti heater deposited on backside of the substrates in used to control the operating temperature of th esensor. The ZnO thin film sensors doped to 4.0 wt% $Al_{2}$O$_{3}$ 1.0wt.% TiO$_{2}$ and 0.2wt.% V$_{2}$O$_{5}$ exhibited a high sensitivity and an excellent selectivity for TMA gas. The sensors made with the thin films annealed at 700$^{\circ}$C for 60 minutes in the oxygen atmosphere had a good stability and linearity. The heater deposited in the ratio of 1 to 1 (Pt:Ti) had a good heating properties. The sensors fabricated using above conditions showed a good response to the actual gases of a mackerel at a step of deterioration after death.

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Combined X-ray CT-SPECT System with a CZT Detector

  • Kwon, Soo-Il;Koji Iwata;Hasegawa, B-H
    • Proceedings of the Korean Society of Medical Physics Conference
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    • 2002.09a
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    • pp.379-381
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    • 2002
  • A single CdZnTe detector is tested for suitability in a prototype CT/ SPECT system designed to acquire both emission and transmission data. The detector has the size of 1${\times}$l-cm$^2$ with 4${\times}$4 1.5${\times}$l.5mm$^2$ pixellated anodes. Since the detector is smaller than imaged object, we translated it in an arc centered at the x-ray tube to image larger objects. Pulse counting electronics with very short shaping time (50 ns) are used to satisfy high photon rates in x-ray imaging, and response linearity up to 3${\times}$10$\^$5/ counts per second per detector element is achieved. The energy resolution of 122-keV gamma-ray is measured to be 14%. We have characterized the system performance by scanning a radiographic resolution phantom .and the Hoffman brain phantom. The spatial resolution of CT and SPECT are about 1 mm and 7 mm, respectively.

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Capacitance-type Alcohol Sensors using Porous Silicon Layer (다공질 실리콘 층을 이용한 정전용량형 알코올 센서)

  • Kim, Seong-Jeen
    • Journal of the Korean Institute of Telematics and Electronics D
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    • v.36D no.9
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    • pp.31-36
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    • 1999
  • A capacitance-type sensor using porous silicon layer is developed to measure aqueous alcohol concentration. Since alcohol, so called ethanol, is very permeable into the silicon wafer, it is often used to help chemical reaction when the silicon wafer is processed under some aqueous solution. In this work, the sensing property was measured for the alcohol concentration from zero to near 100 percent with two types of samples with porous silicon layer formed in 25 and 35% HF solution, respectively. Good reliability as well as fast response time and good linearity were shown over 10kHz and the measured capacitance was observed to be inverse to alcohol concentration due to the decrease of the whole dielectric constant in porous silicon layer.

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Effects of Material Characteristics on the Dynamic Response of the Reinforced Concrete Slabs (재료 특성이 철근 콘크리트 슬래브의 동적 거동에 미치는 영향)

  • Oh, Kyung-Yoon;Cho, Jin-Goo;Hong, Chong-Hyun
    • Journal of The Korean Society of Agricultural Engineers
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    • v.49 no.4
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    • pp.43-49
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    • 2007
  • The reinforced concrete slab is one of main structure members in the construction industry sector. However, most of researches regarding to RC slabs have been focused on two-dimensional Mindlin-type plate element on the basis of laminated plate theory since three-dimensional solid element has a lot of difficulties in finite element formulation and costs in CPU time. In reality, the RC slabs are subjected to dynamic loads like a heavy traffic vehicle load, and thus should insure the safety from the static load as well as dynamic load. Once we can estimate the dynamic behaviour of RC slabs exactly, it will be very helpful for design of it. In this study, the 20-node solid element has been used to analyze the dynamic characteristics of RC slabs with clamped edges. The elasto-visco plastic model for material non-linearity and the smeared crack model have been adopted in the finite element formulation. The applicability of the proposed finite element has been tested for dynamic behaviour of RC slabs with respect to characteristics of concrete materials in terms of cracking stress, crushing strain, fracture energy and Poisson's ratio. The effect on dynamic behaviour is dependent on not crushing strain but cracking stress, fracture energy and Poisson's ratio. In addition to this, it is shown the damping phenomenon of RC slabs has been identified from the numerical results by using Rayleigh damping.

A Study on Fatigue Analysis of Non-Gaussian Wide Band Process using Frequency-domain Method (주파수 영역 해석 기법을 이용한 비정규 광대역 과정의 피로해석에 관한 연구)

  • Kim, Hyeon-Jin;Jang, Beom-Seon
    • Journal of the Society of Naval Architects of Korea
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    • v.55 no.6
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    • pp.466-473
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    • 2018
  • Most frequency domain-based approaches assume that structural response should be a Gaussian random process. But a lot of non-Gaussian processes caused by multi-excitation and non-linearity in structural responses or load itself are observed in many real engineering problems. In this study, the effect of non-Normality on fatigue damages are discussed through case study. The accuracy of four frequency domain methods for non-Gaussian processes are compared in the case study. Power-law and Hermite models which are derived for non-Gaussian narrow-banded process tend to estimate fatigue damages less accurate than time domain results in small kurtosis and in case of large kurtosis they give conservative results. Weibull model seems to give conservative results in all environmental conditions considered. Among the four methods, Benascuitti-Tovo model for non-Gaussian process gives the best results in case study. This study could serve as background material for understanding the effect of non-normality on fatigue damages.

Disposable Strip-Type Biosensors for Amperometric Determination of Galactose

  • Gwon, Kihak;Lee, Seonhwa;Nam, Hakhyun;Shin, Jae Ho
    • Journal of Electrochemical Science and Technology
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    • v.11 no.3
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    • pp.310-317
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    • 2020
  • A development of disposable strip-type galactose sensor for point-of-care testing (POCT) was studied, which was constructed using screen-printed carbon electrodes. Galactose levels were determined by the redox reaction of galactose oxidase in the presence of potassium ferricyanide as an electron transfer mediator in a small sample volume (i.e., less than 1 µL). The optimal performance of biosensor was systematically designated by varying applied potential, operating pH, mediator concentration, and amount of enzyme on the electrode. The sensor system was identified as a highly active for the galactose measurement in terms of the sensitivity (slope = 4.76 ± 0.05 nA/µM) with high sensor-to-sensor reproducibility, the linearity (R2 = 0.9915 in galactose concentration range from 0 to 400 µM), and response time (t95% = <17 s). A lower applied potential (i.e., 0.25 V vs. Ag/AgCl) allowed to minimize interference from readily oxidizable metabolites such as ascorbic acid, acetaminophen, uric acid, and acetoacetic acid. The proposed galactose sensor represents a promising system with advantage for use in POCT.