• Title/Summary/Keyword: Instrumental method

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A Study on Semi-active Vibration Isolation Table using a Nonlinear Analysis of the MR Damper (MR 댐퍼의 비선형해석을 이용한 반능동형 제진대에 관한 연구)

  • Kim, DoYoung;Chun, ChongKeun;Kwon, YoungChul
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.24 no.11
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    • pp.861-867
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    • 2014
  • In this study, a semi-active isolator was constructed from applying a MR damper that used the MR fluid to an isolator. The parameter identification was also performed to determine the characteristics of this semi-active isolator during which the least squares method and the auxiliary variable method were applied to produce a value closest to the true value. In addition, the MR damper's nonlinear damping force was closely analyzed to greatly reduce the range of error. Based on this analysis, it was discovered that the parameter tended to increase with more electric current. Such analysis of the dynamic properties of semi-active isolator proved that constructing an isolator that provides a more stable operation could be achieved.

An Experimental Study on the Static and Dynamic Characteristics of High Speed Air Foil Bearings (고속 공기 포일 베어링의 정적${\cdot}$동적 특성에 관한 실험적 연구)

  • Jo Jun-Hyeon;Lee Yong-Bok;Kim Chang-Ho;Rhim Yoon-Chul
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2004.11a
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    • pp.186-194
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    • 2004
  • Experiments were conducted to determine the structural static and dynamic characteristics of air foil bearings. The housing of the bearing on the journal was driven by an impact hammer which was used to simulate dynamic forces acting on the bump loll with various leading condition. Two different bump foils (Cu-coated bump and viscoelastic bump) were tested and the static and dynamic coefficients of two bump foils compared, based on the experimental measurements for a wide range of operating conditions. The static and dynamic characteristics of air foil bearings were extracted 0rpm the frequency response function by least square method and IV(Instrumental Variable) method. The experiment was tested at 0rpm and $10,000\~16,000rpm$, and loaded on $50\~150N$. From the test results, the possibility of the application of high load and high speed condition is suggested.

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A Comparative Study for Odor Control Regulations (악취관리제도의 국가간 비교연구)

  • 양성봉;김석만
    • Journal of Korean Society for Atmospheric Environment
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    • v.16 no.1
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    • pp.79-87
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    • 2000
  • This study analyzed the regulations concerning odor management or control in Korea, Japan, and developed countries such as USA and Germany. The Korean restriction standards and measurement methods for offensive odor substances are very similar to the Japanese standards and methods promulgated in 1976. Japan promulgated the odor control act and the specific measurement methods of the offensive odor substances in 1973. In Japan, currently, the local governments can establish their own odor restriction areas and proclaim their own standards suitable for their situations. Also, Japan has more strict regulations and more offensive odor substances to be monitored than Korea. The restriction standards of odor in German is quite similar to the permissible limits and standards of air pollutants at emission sources in Korea. Many states in USA are adopting their own restriction standards and measurement methods, e.q., the ambient air pollution standards, organic functionstest methods by dilation, and establishment and addition of air pollution control equipment at emission sources. Finally, this study analyzed the problems of the regulations, standards, and measurement methods concerning the Korean offensive odor management. Since the direct organic fuctions measurement(DOFMM) method is depending upon the personal sensitives of odor substances, the measurement odor value can be equivocal. That is, the odor measurement value by an examines can differ from that by the other examines. Also, there can be conflicts with the measured odor values depending upon the applied measurement methods, e.q., the DOFMM, the dilation method, and the instrumental analysis method.

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Anodic Stripping Differential Pulse Voltammetric Determination of Trace Amounts of Lead after Preconcentration of Its Complex with 2-(5-Bromo-2-pyridylazo)-5-diethylaminophenol onto Natural Analcime Zeolite by Column Method

  • Taher, Mohammad Ali;Mostafavi, Ali;Afzali, Darush;Rezaeipour, Ebrahim
    • Bulletin of the Korean Chemical Society
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    • v.25 no.8
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    • pp.1125-1129
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    • 2004
  • This work assesses the potential of natural Analcime Zeolite as an adsorbent for preconcentration of lead (II) traces. Lead is quantitatively retained on 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol by column method with Analcime in the pH range of 5-6.5 and 2 mL $min^{?1}$ flow rate. Lead was removed from the column with 10.0 mL of 4 M hydrochloric acid and was determined by anodic stripping differential pulse voltammetry. 0.5ppb detection limit was obtained and linear dynamic range was 3 to $1.2{\times}10^5$ ppb in final solution with correlation coefficient of 0.999 and relative standard deviation of ${\pm}$ 1.2% (for eight replicate determination of 2.5 ${\mu}g\;mL^{?1}$ of lead). Various parameters such as the effect of pH, flow rate, instrumental conditions and interferences of some ions on the determination of lead have been studied in detail for optimization of conditions. The method was successfully applied for determination of lead in various samples.

Study of 4-Axis Machining for Ball Gear Cam (볼기어캠의 4-축 가공에 관한 연구)

  • Cho, Hyun-Deog;Shin, Yong-Bum
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.18 no.9
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    • pp.81-87
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    • 2019
  • The automatic tool changer of a machining center consists of a tool magazine and a cam box, and the core components of the cam box are a roller gear cam and a turret. Recently, the roller gear cam of a cam box has been replaced by a ball gear cam. In this study, the design and machining method of ball gear cam for an automatic tool changer was studied. Additionally, an algorithm for a 4-axis post processing method was established from an instrumental formula by designing a ball gear cam, thus preventing machining at the bottom of ball end mill and enabling the ball on the turret to be driven at the entrance and exit of a curve without collision due to machining errors. In conclusion, machining using only the 4-axis method including the C-axis on a BC -Type 5-axis machine produced the desired ball gear cam.

Simultaneous quantitative analysis of four isothiazolinones and 3-iodo-2-propynyl butyl carbamate in hygienic consumer products

  • Heo, Jin Ju;Kim, Un-Jung;Oh, Jeong-Eun
    • Environmental Engineering Research
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    • v.24 no.1
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    • pp.137-143
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    • 2019
  • In this study, extraction, clean-up and instrumental analytical conditions were optimized for identifying and quantifying methyl-, chloromethylbenzi-, octyl- isothiazolinone (MIT, CMIT, BIT, OIT) and 3-iodo-2-propynyl butyl carbamate (IPBC), widely used biocidal active ingredients in human hygiene consumer products. Accuracy of the developed ultrasonic assisted extraction method followed by HPLC/MS analysis for four isothiazolinones and IPBC ranged between 60.4% and 113% in various types of consumer product samples. Method detection limits ranged 0.011-0.034 mg/kg for wet wipes, 0.57-1.5 mg/kg for liquid detergent and 0.58-1.6 mg/kg for powder detergent. Wet wipes, powder and liquid detergents collected from local market in Korea were analyzed to demonstrate the applicability of the developed method. Even after the regulation of those compounds in wet wipes, CMIT, MIT and IPBC were still frequently detected from complementary wet wipes without brand labels which were distributed to customers at local retail shops and restaurants. The maximum observed concentrations of MIT and CMIT found in those complementary wet wipes were 70.2 mg/kg and 11.3 mg/kg, respectively.

Overestimation of Radioactivity Concentration of Difficult-To-Measure Radionuclides in Scaling Factor Methodology

  • Park, Junghwan;Kim, Tae-Hyeong;Lee, Jeongmook;Kim, Junhyuck;Kim, Jong-Yun;Lim, Sang Ho
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.19 no.3
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    • pp.367-386
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    • 2021
  • The overestimation and underestimation of the radioactivity concentration of difficult-to-measure radionuclides can occur during the implementation of the scaling factor (SF) method because of the uncertainties associated with sampling, radiochemical analysis, and application of SFs. Strict regulations ensure that the SF method as an indirect method does not underestimate the radioactivity of nuclear wastes; however, there are no clear regulatory guidelines regarding the overestimation. This has been leading to the misuse of the SF methodology by stakeholders such as waste disposal licensees and regulatory bodies. Previous studies have reported instances of overestimation in statistical implementation of the SF methodology. The analysis of the two most popular linear models of the SF methodology showed that severe overestimation may occur and radioactivity concentration data must be dealt with care. Since one major source of overestimation is the use of minimum detectable activity (MDA) values as true activity values, a comparative study of instrumental techniques that could reduce the MDAs was also conducted. Thermal ionization mass spectrometry was recommended as a suitable candidate for the trace level analysis of long-lived beta-emitters such as iodine-129. Additionally, the current status of the United States and Korea was reviewed from the perspective of overestimation.

Instrumental Seismic Intensity based on Fourier Acceleration Spectra of the earthquake ground-motion (지진파의 가속도 푸리에스펙트럼 크기를 이용한 계측진도 평가)

  • Yun, Kwan-Hee;Park, Dong-Hee;Park, Se-Moon
    • Journal of the Earthquake Engineering Society of Korea
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    • v.13 no.6
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    • pp.27-37
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    • 2009
  • A method of instrumentally estimating seismic intensity (MMI) based on the Fourier Acceleration Spectrum of earthquake ground-motion, the so-called 'FAS MMI method' of Sokolov and Wald (2002), was evaluated for its applicability to Korea based on the empirical models of mean (m) and standard deviation (${\sigma}$) for Korea according to individual seismic intensity for MMI ${\leq}$ IV (Yun et al., 2009). This evaluation showed that the error in estimating the seismic intensity using the FAS MMI method is ${\sigma}$ = 0.74 MMI, and was further reduced to ${\sigma}$ = 0.61 MMI if the dependency of the error on earthquake magnitude and distance is additionally corrected. It is also shown that FAS MMI based on the FAS semi-empirically evaluated from small earthquakes for damaging earthquakes in Korea with maximum MMI ${\geq}$ VI could predict the observed MMI with the maximum error of 0.63 by using the combined FAS m-${\sigma}$ models of Korea for MMI ${\leq}$ IV and global region for MMI ${\geq}$ V.

Characteristic Impact Odorants of Changpo (Acorus calamus var. angustatus Bess) Root Essential Oil

  • Choi, Hyang-Sook
    • Food Science and Biotechnology
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    • v.14 no.4
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    • pp.450-455
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    • 2005
  • This study was conducted to determine firstly the composition of the essential oil from fresh changpo (Acorus calamus var. angustatus Bess) roots quantitatively and qualitatively by use of two internal standards, and secondly volatile compounds which are primarily responsible for the aroma of changpo roots. Simultaneous steam distillation and extraction method was used for essential oil extraction, and aroma extract dilution analysis (AEDA) and sniffing test by gas chromatography/olfactometry (GC/O) were used to detect the characteristic impact odorants. According to the instrumental analysis of changpo root essential oil, cis, trans-famesol (47.56 mg/kg of fresh wt), octanoic acid (23.73 mg/kg of fresh wt), trans-2-dodecenal (20.28 mg/kg of fresh wt) and trans, trans-farnesol (13.81 mg/kg of fresh wt) were the most abundant compounds. Geranyl acetate, trans-nerolidol and trans, trans-farnesyl acetate were evaluated as the characteristic impact odorants of changpo roots from results of AEDA and sniffing test. Especially, geranyl acetate was considered as the most similar odor component to changpo roots by organoleptic evaluation with GC/O.

Multivariate Classification of Choson Coins (다변수 분석법에 의한 조선시대 동전의 분류연구)

  • Lee, Chang-Keun;Kang, Hyung-Tai;Goh, Sung-Hee
    • 보존과학연구
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    • s.8
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    • pp.1-12
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    • 1987
  • Fifty ancient Korean coins originated in Choson dynasty have been determined for 9 elements such as Sn, Fe, As, Ag, Co, Sb, Ir, Ru and Ni by instrumental neutron activation analysis and for 3 elements such as Cu, Pb, and Zn by atomicalsorption spectrometry. Bronze coins originated in early days of the dynasty contain as major constituents Cu, Pb and Sn approximately in the ratio 90 : 4 : 3, where as, those in latter days contain in the ratio 7 : 2 : 0. Brass coins which had begun in 17century contain as major constituents Cu, Zn and Pb approximately in the ratio 7 : 1: 1. The multivariate date have been analyzed for the relation among elemental contents through the variance-covariance matrix. The data have been fur theranalyzed by a principal component mapping method. As the results training set of 8class have been chosen, based on the spread of sample points in an eigenvector plotand archaeolgical data such as age and the office of minting.

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