• Title/Summary/Keyword: Infrared stress analysis

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Dynamic Quasi-Elastic Light Scattering Measurement of Biological Tissue

  • Youn, Jong-In;Lim, Do-Hyung
    • Journal of Biomedical Engineering Research
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    • v.28 no.2
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    • pp.169-173
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    • 2007
  • During laser irradiation, mechanically deformed cartilage undergoes a temperature dependent phase transformation resulting in accelerated stress relaxation. Clinically, laser-assisted cartilage reshaping may be used to recreate the underlying cartilaginous framework in structures such as ear, larynx, trachea, and nose. Therefore, research and identification of the biophysical transformations in cartilage accompanying laser heating are valuable to identify critical laser dosimetry and phase transformation of cartilage for many clinical applications. quasi-elastic light scattering was investigated using Ho : YAG laser $(\lambda=2.12{\mu}m\;;\;t_p\sim450{\mu}s)$ and Nd:YAG Laser $(\lambda=1.32{\mu}m\;;\;t_p\sim700{\mu}s)$ for heating sources and He : Ne $(\lambda=632.8nm)$ laser, high-power diode pumped laser $(\lambda=532nm)$, and Ti : $Al_2O_3$ femtosecond laser $(\lambda=850nm)$ for light scattering sources. A spectrometer and infrared radiometric sensor were used to monitor the backscattered light spectrum and transient temperature changes from cartilage following laser irradiation. Analysis of the optical, thermal, and quasi-elastic light scattering properties may indicate internal dynamics of proteoglycan movement within the cartilage framework during laser irradiation.

Fabrication and Characteristics of Small Sized PZT Powders by using a Propyl Alcohol based Sol-Gel Method

  • Choi, Kyu-M.;Lee, Yun-S.
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.34 no.11A
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    • pp.904-908
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    • 2009
  • The PZT(lead, zirconium, titanium) based ceramics which, are reported to be ferroelectric materials have their important applications in the areas of surface acoustic waves (SAW), filters, infrared detectors, actuators, ferroelectric random acess memory, speakers, electronic switches etc. Moreover, these PZT materials possess the large electromechanical coupling factor, large spontaneous polarization, low dielectric loss and low internal stress etc. Hence, keeping in view the unique properties of PZT piezoelectric ceramics we also tried to synthesize indigenously the small sized PZT ceramic powder in the laboratory by using the modified sol-gel approach. In this paper, Propyl alcohol based sol-gel method was used for preparation of PZT piezoelectric ceramic. The powder obtained by this sol-gel process was calcined and sintering to reach a pyrochlore-free crystal phase. The characterization of synthesized material was carried out by the XRD analysis and the surface morphology was determined by high resolution scanning electron microscopy.

Studies on Cure Behaviors, Dielectric Characteristics and Mechanical Properties of DGEBA/Poly(ethylene terephthalate) Blends

  • Park, Soo-Jin
    • Macromolecular Research
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    • v.17 no.8
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    • pp.585-590
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    • 2009
  • The cure behaviors, dielectric characteristics and fracture toughness of diglycidylether of bisphenol-A (DGEBA)/poly(ethylene terephthalate) (PET) blend system were investigated. The degree of conversion for the DGEBA/PET blend system was measured using Fourier transform infrared (FTIR) spectroscopy. The cure kinetics were investigated by measuring the cure activation energies ($E_a$) with dynamic differential scanning calorimetry (DSC). The dielectric characteristic was examined by dielectric analysis (DEA). The mechanical properties were investigated by measuring the critical stress intensity factor ($K_{IC}$), critical strain energy release rate ($G_{IC}$), and impact strength test. As a result, DGEBAIPET was successfully blended. The Ea of the blend system was increased with increasing PET content to a maximum at 10 phr PET. The dielectric constant was decreased with increasing PET content. The mechanical properties of the blend system were also superior to those of the neat DGEBA. These results were attributed to the increased cross-linking density of the blend system, resulting from the interaction between the epoxy group of DGEBA and the carboxyl group of PET.

[Retracted]The effect of Massage and Paraffin on Cold Hypersensitivity Patient ([논문표절]수족냉증에 적용한 마사지와 파라핀의 효과)

  • Roh, Hyo-lyun
    • Proceedings of the Korea Contents Association Conference
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    • 2017.05a
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    • pp.101-102
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    • 2017
  • This study of purpose was to evaluate the changes in hands and feet temperature by applying massage and paraffin bath.. The subject of this study was 30 university healthy students. Subjects were divided into paraffin bath group and massages group. The digital infrared thermographic imaging was used for thermographic analysis. The visual analog scale was used for subjective information about the degree of cold sensitivity and cold stress test was used for analyzing the temperature recovery rate. After the interventions showed that temperature difference of the right hand and temperature difference of the left hand are less in the paraffin group than the massage group. When applied paraffin bath and massage to the cold hypersensitivity patient the massage group showed difference in the visual analog scale and the paraffin group showed difference in the temperature of the right hand, left hand, left foot and in the visual analog scale. Paraffin bath treatment seems to be useful to patients with cold hypersensitivity on hands and feet.

The Measurement Errors of Elastic Modulus and Hardness due to the Different Indentation Speed (압입속도의 변화에 따른 탄성계수와 경도의 오차 연구)

  • Lee, Kyu-Young;Lee, Chan-Bin;Kim, Soo-In;Lee, Chang-Woo
    • Journal of the Korean Vacuum Society
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    • v.19 no.5
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    • pp.360-364
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    • 2010
  • Most research groups used two analysis methods (spectroscopy and nanotribology) to measure the mechanical properties of nano-materials: NMR (Nuclear Magnetic Resonance), IR (Infrared Spectroscopy), Raman Spectroscopy as the spectroscopy method and AFM (Atomic Force MicroScope), EFM (Electrostatic Force Microscope), KFM (Kelvin Force Microscope), Nanoindenter as the nanotribological one. Among these, the nano-indentation technique particularly has been recognized as a powerful method to measure the elastic modulus and the hardness. However, this technique are prone to considerable measurement errors with pressure conditions during measurement. In this paper, we measured the change of elastic modulus and hardness of an Al single crystal with the change of load, hold, and unload time, respectively. We found that elastic modulus and hardness significantly depend on load, hold, and unload time, etc. As the indent time was shortened, the elastic modulus value decreased while the hardness value increased. In addition, we found that elastic modulus value was more sensitive to indent load, hold, and unload time than the hardness value. We speculate that measurement errors of the elastic modulus and the hardness originate from the residual stress during indenting test. From our results, the elastic modulus was more susceptible to the residual stress than the hardness. Thus, we find that the residual stress should be controlled for the minimum measurement errors during the indenting test.

Thermographic analysis of failure for different rock types under uniaxial loading

  • Kirmaci, Alper;Erkayaoglu, Mustafa
    • Geomechanics and Engineering
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    • v.23 no.6
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    • pp.503-512
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    • 2020
  • Mining activities focus on the production of mineral resources for energy generation and raw material requirements worldwide and it is a known fact that shallow reserves become scarce. For this reason, exploration of new resources proceeds consistently to meet the increasing energy and raw material demand of industrial activities. Rock mechanics has a vital role in underground mining and surface mining. Devices and instruments used in laboratory testing to determine rock mechanics related parameters might have limited sensing capability of the failure behavior. However, methodologies such as, thermal cameras, digital speckle correlation method and acoustic emission might enable to investigate the initial crack formation in detail. Regarding this, in this study, thermographic analysis was performed to analyze the failure behaviors of different types of rock specimens during uniaxial compressive strength experiments. The energy dissipation profiles of different types of rocks were characterized by the temperature difference recorded with an infrared thermal camera during experiments. The temperature increase at the failure moment was detected as 4.45℃ and 9.58℃ for andesite and gneiss-schist specimens, respectively. Higher temperature increase was observed with respect to higher UCS value. Besides, a temperature decreases of about 0.5-0.6℃ was recorded during the experiments of the marble specimens. The temperature change on the specimen is related to release of radiation energy. As a result of the porosity tests, it was observed that increase in the porosity rate from 5.65% to 20.97% can be associated to higher radiation energy released, from 12.68 kJ to 297.18 kJ.

ANALYSIS OF THE EFFECT OF HYDROXYL GROUPS IN SILICON DIRECT BONDING USING FT-IR (규소 기판 접합에 있어서 FT-IR을 이용한 수산화기의 영향에 관한 해석)

  • Park, Se-Kwang;Kwon, Ki-Jin
    • Journal of Sensor Science and Technology
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    • v.3 no.2
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    • pp.74-80
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    • 1994
  • Silicon direct bonding technology is very attractive for both silicon-on-insulator devices and sensor fabrication because of its thermal stress free structure and stability. The process of SDB includes hydration of silicon wafer and heat treatment in a wet oxidation furnace. After hydration process, hydroxyl groups of silicon wafer were analyzed by using Fourier transformation-infrared spectroscopy. In case of hydrophilic treatment using a ($H_{2}O_{2}\;:\;H_{2}SO_{4}$) solution, hydroxyl groups are observed in a broad band around the 3474 $cm^{-1}$ region. However, hydroxyl groups do not appear in case of diluted HF solution. The bonded wafer was etched by using tetramethylammonium hydroxide etchant. The surface of the self etch-stopped silicon dioxide is completely flat, so that it can be used as sensor applications such as pressure, flow and acceleration, etc..

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Immersion grating mount design of IGRINS

  • Moon, Bong-Kon;Wang, Weisong;Park, Chan;Lee, Sung-Ho;Yuk, In-Soo;Chun, Moo-Young;Lee, Han-Shin;Jaffe, Daniel T.
    • The Bulletin of The Korean Astronomical Society
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    • v.36 no.2
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    • pp.153.2-153.2
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    • 2011
  • The IGRINS (Immersion GRating INfrared Spectrometer) is a high resolution wide-band infrared spectrograph developed by Korea Astronomy and Space Science Institute (KASI) and the University of Texas at Austin (UT). Immersion grating is a key component of IGRINS, which disperses the input ray by using a Silicon material with a lithography technology. Opto-mechanical mount for the immersion grating is important to keep the high spectral resolution and the optical alignment in a cold temperature of $130{\pm}0.06K$. The optical performance of immersion grating can maintain within the de-center tolerance of ${\pm}0.05mm$ and the tip-tilt tolerance of ${\pm}1.5arcmin$. The mount mechanism utilizes the flexure and the kinematic support design to satisfy the requirement and the operation condition. When the IGRINS system is cooled down to a cold temperature, three flexures compensate the thermal contraction stress due to the different material between the immersion grating and the mounting part(Aluminum 6061). They also support the immersion grating by an appropriate preload. Thermal stability is controlled by a copper strap with proper dimensions and a heater. Generally structural and thermal analysis was performed to confirm the mount mechanism. This talk presents the opto-mechanical mount design of the immersion grating of IGRINS.

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Analysis for Thermal Distribution of Low-voltage Condenser by the Variance of Voltage & Frequency (전압 및 주파수 변화에 따른 저압 콘덴서 열 분포 해석)

  • Kim, Jong-Gyeum
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.24 no.4
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    • pp.43-49
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    • 2010
  • Power capacitor has been used to compensate for the low power factor of inductive load and to reduce harmonics generated by the power conversion device with reactor. The increase of voltage and current and thermal generation are extremely hard on the life of condenser. Current will be increased, provided that voltage and frequency of condenser increase also. The increase of voltage and frequency justly extends thermal generation. Both act on insulation stress and can afford to premature fault In this paper, we measured thermal distribution of condenser with infrared rays camera in case of variance of voltage and frequency. We were assured that the increase of voltage and frequency produces high heat and exceedingly shortens the life of condenser.

Mechanical Properties of Styrene-Butadiene Rubber Reinforced with Silica by in situ Tetraethoxysilane Hydrolysis over Acid Catalyst

  • Li, Qingyuan;Li, Xiangxu;Cho, Ur Ryong
    • Elastomers and Composites
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    • v.53 no.2
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    • pp.57-66
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    • 2018
  • Styrene-butadiene rubber (SBR), reinforced with different contents of silica (with or without modification using silane coupling agents), was prepared by a modified sol-gel method involving hydrolyzation of tetraethoxysilane over an acid catalyst. The structures of the as-prepared samples were characterized using various techniques, such as scanning electron microscopy, X-ray photoelectron spectroscopy, Fourier-transform infrared spectroscopy, and thermogravimetric analysis. The mechanical properties of the as-prepared samples were discussed in detail. The results revealed an increasing of the storage modulus (G') with increase in the silica content without modification. In contrast, G' decreased after modification using silane coupling agents, indicating a reduction in the silica-silica interaction and improved dispersion of silica in the SBR matrix. Both tensile stress and hardness increased with increase in the silica content (with modification) in the SBR matrix, albeit with low values compared to the samples with un-modified silica, except for the case of silica modified using (3-glycidyloxypropyl) trimethoxysilane (GPTS). The latter observation can be attributed to the special structure of GPTS and the effort of oxygen atom lone-pair.