• 제목/요약/키워드: Holding Time

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뼈 충진재용 생분해성 다공질 Calcium Phosphate 세라믹스의 제조 (Preparation of Biodegradable Porous Calcium Phosphate Ceramics for Bone Fillers)

  • 이중환;김석영
    • 대한의용생체공학회:학술대회논문집
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    • 대한의용생체공학회 1996년도 춘계학술대회
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    • pp.130-132
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    • 1996
  • It is well known when porous calcium phosphate ceramics are used as a bone graft substitute, new tissues or blood vessels are grown into the porous implant due to their excellent biocompatibility. In this study, the ${\beta}$-crystalline form of calcium metaphosphate, $Ca(PO_{3})_{2}$ is prepared by the controlled thermolysis of monocalcium phosphate, $Ca(H_{2}PO_{4})_{2}$. The diameter of cylindrical pores formed during cooling was controlled by a holding time at the melting point of a monocalcium phosphate and by the change of a recrystallization temperature, to obtained the most appropriate size (about $200{\mu}m$) of pores. It was observed that the increasing holding time at the melting point of monocalcium phosphate results in the decreases of pore sizes.

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Effects of Quasi-Carbonization Process on the Mechanical Properties of Spun Yarn Type Quasi-Carbon Fabrics

  • Donghwan Cho;Lee, Jongmoon;Park, Jon-Kyoo
    • Macromolecular Research
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    • 제10권6호
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    • pp.318-324
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    • 2002
  • In this paper we have extensively studied what and how processing parameters for quasi-carbonization influence the breaking strength and modulus of resulting quasi-carbon fabrics that are prepared from stabilized PAN fabrics with a spun yarn texture. Seven processing parameters have been considered as follows: applied tension, final heat-treatment temperature, heating rate, heating step, holding time, cooling rate, and purging gas purity. The results indicate that optimal uses of applied tension, final heat-treatment temperature, heating rate, and heating step during quasi-carbonization process are primarily important to increase the tensile properties of quasi-carbon fabrics and holding time, cooling rate, and purging gas purity are less importantly contributed.

Effect of rapid thermal annealing on CdS films prepared by RF magnetron sputtering

  • 황동현;감대웅;안정훈;손영국
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2009년도 제38회 동계학술대회 초록집
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    • pp.164-164
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    • 2010
  • Cds films were deposited on glass substrates using rf magnetron sputtering method followed by rapid thermal annealing(RTA). Effects of annealing temperature on surface characteristic, structural, electrical and optical property of CdS films were investigated at different temperatures ranging from 250 to $550^{\circ}C$ with various holding time. The film annealed at $450^{\circ}C$ with less than 1 min holding time is attributed to the improved crystalline quality of CdS film due to the effective relaxation of residual compressive stress and achieving maximum grain size. The results show that RTA treatments under optimal annealing condition can provide significant improvements in the properties of CdS films.

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필름 인서트 사출성형 평판의 휨 변형에 관한 실험적 연구 (An Experimental Study on the Warpage of a Film Insert Molded Plate)

  • 유영길;이호상
    • 소성∙가공
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    • 제21권1호
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    • pp.30-35
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    • 2012
  • FIM(Film Insert Molding) is an innovative method of producing decorated parts for a wide range of products. Because it requires fewer steps when compared to conventional production methods, the time and cost of manufacturing high quality components can be reduced considerably. In this paper, the effects of processing conditions on the warpage of film-insert molded plate were investigated by using a design of experiments. The dominant factors affecting warpage were mold temperature and holding pressure. Warpage increased with the temperature difference between stationary mold and fixed one. Even when the mold temperature difference was zero, the plate with a film was bent after ejection such that the film side protruded. As holding pressure increased, warpage decreased significantly. In addition warpage increased with time increment for the film-insert molded plates.

Ni-Al계 금속간화합물 코팅에 미치는 고주파유도 가열 조건의 영향 (Effects of Induction Heating Conditions on Ni-Al Based Intermetallic Compound Coating)

  • 이한영;김태준;조용재
    • 대한금속재료학회지
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    • 제48권2호
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    • pp.141-147
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    • 2010
  • An Ni-Al intermetallic coating has been produced by induction heating on mild steel. The effect of the induction heating conditions on the microstructure of the coating has been investigated. The reaction synthesis of the intermetallic compounds was promoted while increasing the heating rate and the holding time at reaction temperature. Especially, an NiAl phase corresponding to the initial composition of mixed powder was predominantly formed. However, the synthesis at low reaction temperatures occurred by solid state diffusion during the holding time and an Fe-Al reaction layer was formed at the interface with the substrate, regardless of the heating rate. The combustion synthesis of the intermetallic compound occurred at a temperature higher than 1023 K and resulted in an almost single phase NiAl structure.

스팀-에어 레토르트의 온도분포에 미치는 공정 변수 영향 (The Effect of Various Processing Conditions on Temperature Distribution in Steam-air Retort)

  • 이선영;신해헌;인예원;조형용
    • 산업식품공학
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    • 제23권2호
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    • pp.87-93
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    • 2019
  • 공기 주입식 스팀-에어 레토르트 내에서 스팀온도, 내부가압, CUT 등의 공정변수가 레토르트 내부의 온도 균일성에 미치는 영향을 평가하였다. 고온살균(121℃)이 저온살균(82℃) 보다 공정구간동안 온도분포가 더 균일하고 안정적이었다. 내부 가압이 클수록 저온살균조건의 공정에서는 온도분포가 안정적이었고, 이와 반대로 고온살균조건의 공정에서 온도분포가 더 불균일한 것으로 나타났다. 승온구간을 조절한 경우에는 레토르트 내의 온도분포에는 유의적인 차이를 나타내지 않았다. 공정구간동안 레토르트 내부에서 냉점은 수직방향 1층의 위로 확인되었고, 수평방향에서는 맨 뒤쪽 중앙 부분이 가장 높은 온도를 유지하여 공정 동안 이 위치들을 주의를 할 필요가 있었다. 또한 레토르트 내부의 양 옆 위치가 다른 위치에 비해 특히 온도분포가 불안정한 것으로 확인되었으므로 레토르트 가공 공정에서 주의해야 할 것으로 판단되었다.

High Pressure Inactivation Kinetics of Salmonella enterica and Listeria monocytogenes in Milk, Orange Juice, and Tomato Juice

  • Xu, Hua;Lee, Hyeon-Yong;Ahn, Ju-Hee
    • Food Science and Biotechnology
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    • 제18권4호
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    • pp.861-866
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    • 2009
  • Effects of pressure come-up and holding times on the inactivation of Salmonella enterica and Listeria monocytogenes were evaluated in deionized water, milk, orange juice, and tomato juice with pH 6.76, 6.85, 3.46, and 4.11, respectively. The inoculated samples were subjected to high pressure treatments at 300, 400, and 500 MPa for less than 10 min at $30^{\circ}C$. At 500 MPa, the numbers of S. enterica and L. monocytogenes in deionized water, orange juice, and tomato juice were reduced by more than 6 log CFU/mL during the come-up time. Compared to orange and tomato juices, milk showed a considerable baroprotective effect against S. enterica and L. monocytogenes. At 300 MPa, the D values for S. enterica in milk, orange juice, and tomato juice were 0.94, 0.41, and 0.45 min, while those for L. monocytogenes were 9.56, 1.11, and 0.94 min, respectively. Low pH resulted in a noticeable synergistic effect on the inactivation of S. enterica and L. monocytogenes in orange and tomato juices. Therefore, these results might provide more useful information for designing the entire high hydrostatic pressure (HHP) conditions, taking the come-up time reduction, and food system.

V-Nb Microalloyed 강의 오스테나이트역에서 복합 탄질화물의 재용해 및 석출 거동 (Dissolution and Precipitation behaviors of Complex Carbonitrides in Austenite of a V-Nb Microalloyed Steel)

  • 하양수;정재길;이영국
    • 대한금속재료학회지
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    • 제49권12호
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    • pp.917-923
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    • 2011
  • Dissolution and precipitation behaviors of complex carbonitrides in austenite of a V-Nb microalloyed steel were quantitatively examined through electrical resistivity measurement and transmission electron microscopy. The electrical resistivity increased with solution treatment temperature up to $1240^{\circ}C$ and then was saturated at $225n{\Omega}m$ for a holding time of 10 min. The electrical resistivity method was also used to quantitatively measure the isothermal precipitation kinetics of the complex carbonitrides in austenite. Nb-rich precipitates were observed in austenite at the early stages of precipitation, but Nb was replaced by V up to the equilibrium amount within the precipitates with further holding time. The time-temperature-precipitation diagram showed a C-type curve; nose temperature and its incubation time were $900^{\circ}C$ and 100 s, respectively.

Experimental and theoretical justification of passive heat removal system for irradiated fuel assemblies of the nuclear research reactor in a spent fuel pool

  • Ta Van Thuong;O.L. Tashlykov;S.M. Glukhov;D.E. Shumkov;Yu.V. Volchikhina
    • Nuclear Engineering and Technology
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    • 제55권6호
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    • pp.2088-2095
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    • 2023
  • The safety of nuclear installations is largely determined by the tightness of fuel elements cladding. As the Fukushima nuclear accident showed, the main task in case of loss of power supply is to ensure reliable removal of residual heat release from spent fuel pool (SFP) with irradiated fuel assemblies (IFAs). The paper presents the results of calculated-experimental studies and thermal-hydraulic modeling of temperature storage modes of IFAs in SFP. Experimental studies of SFP's temperature regime and calculated evaluation of residual heat removal due to the thermal conductivity of building structures surrounding the SFP were performed. To ensure the safe operation of research reactors, it's necessary to know the IFA's residual heat power (RHP) in the reactor and SFP, which is determined depending on the operating time of fuel assemblies (FAs) and the IFAs calculated holding time. The FAs operating time depends on the reactor energy output. The IFAs calculated holding time is determined by the fuel burnup, U-235 mass in the fuel, and reactor utilization factor. The IFAs fuel burnup was calculated using the MCU-PTR program. Also presented are the RHP's calculation results using some of the empirical dependencies. The concept of a passive heat removal system (PHRS) based on thermosyphon's operating principle was proposed.