• Title/Summary/Keyword: High-temperature design

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Microstructural analysis of the single crystalline AlN and the effect of the annealing on the crystalline quality (단결정 AlN의 미세구조 분석 및 어닐링 공정이 결정성에 미치는 영향)

  • Kim, Jeoung Woon;Bae, Si-Young;Jeong, Seong-Min;Kang, Seung-Min;Kang, Sung;Kim, Cheol-Jin
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.28 no.4
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    • pp.152-158
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    • 2018
  • PVT (Physical Vapor Transport) method has advantages in producing high quality, large scale wafers where many researches are being carried out to commercialize nitride semiconductors. However, complex process variables cause various defects when it had non-equilibrium growth conditions. Annealing process after crystal growth has been widely used to enhance the crystallinity. It is important to set appropriate temperature, pressure, and annealing time to improve crystallinity effectively. In this study, the effect of the annealing conditions on the crystalline structure variation of the AlN single crystal grown by PVT method was investigated with synchrotron whitebeam X-ray topography, electron backscattered diffraction (EBSD), and Rietveld refinement. X-ray topography analysis showed secondary phases, sub-grains, impurities including carbon inclusion in the single crystal before annealing. EBSD analyses identified that sub-grains with slightly tilted basal plane appeared and the overall number of grains increased after the annealing process. Rietveld refinement showed that the stress caused by the temperature gradient during the annealing process between top and bottom in the hot zone not only causes distortion of grains but also changes the lattice constant.

Optimization of Roasted Perilla Leaf Tea Using Response Surface Methodology (반응표면분석을 이용한 들깨잎차 볶음처리의 최적화)

  • Han, Ho-Suk;Park, Jung-Hye;Choi, Hee-Jin;Sung, Tae-Su;Woo, Hi-Seob;Choi, Cheong
    • Applied Biological Chemistry
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    • v.47 no.1
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    • pp.96-106
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    • 2004
  • Response surface methodology (RSM) was applied in roasting processes of perilla leaves to develop a high quality perilla leaf tea. The Hunter color parameters and electron donating ability were monitored to optimize organoleptic properties of perilla leaf tea. The roasting processes were based on the central composite design with primary variables-roasting temperature $(140{\sim}220^{\circ}C)$, time $(5{\sim}25)$, and reaction variables-sensory test, electron donating ability. From the variables, the roasting condition was optimized using statistical analysis system (SAS) program as developing the functional tea using perilla leaf. Hunter color L and b values of the powdered samples increased with the roasting processes, but Hunter color a value decreased. Electron donating ability was influenced by roasting temperature (p<0.01) and time (p<0.01), and optimum condition selected was at $220^{\circ}C$ for 15 min with coefficient of determinations $(R^2)$ above 0.98. After preference test of perilla leaf tea using parameter of taste, color, and flavor, we can estimate that the optimal roasting condition of preilla leaf for function tea manufacturing are $210{\sim}220^{\circ}C$ for $10{\sim}20$ min by response surface methodology (RSM). Tyrosinase, xanthine oxidase and electron donating ability were 10.14, 14.37 and 59.19% of perilla leaf tea.

Method of Decreasing Cracking Index by Different Mix Conditions for Separated Placement and its Field Application (콘크리트 배합요인별 상·하부 분리타설에 의한 수화열 균열지수 저감방안 및 현장적용)

  • Kim, Min-Ho;Han, Cheon-Goo
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.4 no.3
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    • pp.292-298
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    • 2016
  • In this research, considering the practical situation of separated placing method for mass concrete structure, an efficient method of controlling the heat of hydration is suggested by comparing between the simulated values and actual measurements conducted with the optimum mix design obtained from the various mix conditions with different types and amount of supplementary cementitious materials(SCMs). As the result of the research, firstly, the optimum mix designs for top and bottom layers were determined by Midas gen as OPC to FA of 85 to 15, and OPC to FA to BS of 50 to 20 to 30, respectively. The concrete mixtures prepared with the mix designs determined from the simulation satisfied the target performance range in slump, air content and compressive strength. Additionally, from temperature measurement for the actual mass concrete placed during spring, the maximum temperature difference between surface and core was about $10^{\circ}C$ with 59 and $49^{\circ}C$ for top and bottom layers, respectively, and 1.4 of cracking index was obtained. Therefore, considering the practical conditions of mass concrete construction, it is considered that the different heat of hydration method using different mix designs with SCMs can be an efficient method for controlling thermal cracking and settling cracking of mass concrete.

Optimization of growth conditions for cultivation of Phellinus linteus mycelia using swine waste as a growth substrate (돈분뇨를 기질로 활용한 고부가 가치 상황버섯 균사체 배양조건 최적화 연구)

  • Koo, Taewoan;Lee, Joonyeob;Cho, Kyungjin;Lee, Jangwoo;Shin, Seung Gu;Hwang, Seokhwan
    • Journal of the Korea Organic Resources Recycling Association
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    • v.23 no.2
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    • pp.53-60
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    • 2015
  • Newly, nutrients recovery by bioconversion in the swine waste which caused serious problems due to its high organic fraction and content of nutrients such as phosphorus and nitrogen is viewed as a considerable approach since it produces valuable product as well as recycling of resources. Consequently, it is necessary to find new methods to treat swine waste. One possible solution to this problem is to use this potential pollutant as a growth substrate for economically valuable products. The study for the fundamental improvement of bioconversion efficiency by finding optimum growth conditions using statistical models and biotechnology was performed. A novel approach to utilize swine waste by cultivating mycelia of the mushroom Phellinus linteus are described. A central composite face-centered design (CCF) for the experiments was used to develop empirical model providing a quantitative interpretation of the relationships among the three variables, which were substrate concentration, pH, and temperature. The maximal radial extension rate (2.78mm/d) of P.linteus was determined under the condition of 5.0 g COD/L, pH 5.0, and temperature $29.7^{\circ}C$. The results of this study suggest that swine waste could be utilized as a growth substrate for the cultivation of mushroom mycelia enhancing an efficiency of utilizing this by-product of the livestock industry.

Effect of Hydrogen(H2) Addition on Flame Shape and Combustion Products in Mixed Coflow Diffusion Flames of Methane(CH4), Ethane(C2H6) and Propane(C3H8) (동축류 메탄(CH4), 에탄(C2H6), 프로판(C3H8) 혼합 확산화염내의 수소(H2) 첨가가 화염 형상 및 연소 생성물에 미치는 영향)

  • Park, Ho-Yong;Yoon, Sung-Hwan;Rho, Beom-Seok;Lee, Won-Ju;Choi, Jae-Hyuk
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.25 no.6
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    • pp.780-787
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    • 2019
  • As a carbon-free, green growth alternative, internal and external interest in hydrogen energy and technology is growing. Hydrogen was added to co-axial methane, methane-propane, and methane-propane-ethane diffusion flames, which are the main ingredients of LNG, to evaluate its effect on flame formation and combustion products. The variation in combustion products produced by adding hydrogen gradually to diffusion pyrolysis at room temperature and normal pressure conditions was observed experimentally by using a gas analyzer, and the shape of diffusion pyrolysis was observed step by step using a digital camera. The experimental results showed that the production volume of nitrogen oxides tended to increase and became close to linear as hydrogen was added to the diffusion pyrotechnic. This is because the relatively high temperature of heat insulation and fast combustion speed of hydrogen facilitated the production of thermal NOx. On the other hand, CO2 production tended to decrease as hydrogen was added to reduce the overall carbon ratio contained in the mixed diffusion flame of methane, methane-propane, and methane-ethane-propane. This means that the mixed fuel use of LNG-hydrogen in ships may potentially reduce emissions of CO2, a greenhouse gas.

A Study on the Cleanup Process of HOCs-Contaminated Soil by Ex-situ Soil Washing Technology (Ex-situ 토양세척기법에 의한 소수성 유기오염물질로 오염된 토양의 정화에 관한 연구)

  • Choi, Sang-Il;Ryoo, Doo-Hyun;Jang, Min
    • Journal of Korea Soil Environment Society
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    • v.2 no.1
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    • pp.99-107
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    • 1997
  • In this study, a series of batch-scale tests were conducted to optimize the design parameters for the application of soil washing techniques to the hydrophobic organic compounds(HOCs)-contaminated soil and to find the effective methods for the recovery of surfactants from washing effluent by using solvent. Several nonionic surfactants (polyoxyethylene oleyl ester) and sophorolipid were applied to the artificially contaminated soil (4,000 mg n-dodecane/kg dry soil). The effects of washing time, concentration of surfactant solution, dilution ratio, and temperature on washing efficiencies were examined. Hydrophile-liphophile balance (HLB) number was proven to be one of the important parameters for soil washing. The HLB numbers of OA-5 and sophorolipid are too low to form a stable soil-water emulsion. They showed very low washing efficiencies less than 10e1o. If HLB number is in the proper range to form a stable soil-water emulsion, surfactant having higher solubility for HOCs shows higher washing efficiency. OA-14 having higher HLB number than OA-9 formed more stable soil-water emulsion. But its washing efficiency was about 20% due to a lower molar solubility ratio (MSR) than OA-9. OA-9, which forms a stable soil-water emulsion and has comparatively high sotubility for HOCs, showed about 60% washing efficiency by itself. To recover anthracene effectively from OA-9 washing effluent by using benzene as an organic solvent, desirable temperature and pH were $30^{\circ}C$ and 2, respectively.

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Characteristics of Germination and Early Growth of Parasenecio firmus in Container by Shading Treatment (차광처리에 따른 병풍쌈의 용기 내 발아 및 초기생장 특성)

  • Song, Ki Seon;Jeon, Kwon Seok;Kim, Chang Hwan;Yoon, Jun Hyuck;Park, Yong Bae;Kim, Jong Jin
    • Journal of Korean Society of Forest Science
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    • v.103 no.4
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    • pp.547-555
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    • 2014
  • This study was carried out in order to investigate the germination and the early growth characteristics of Parasenecio firmus. Seed pre-treatment before the each experiment was carried out by shading treatment (with drying at room temperature (DRT), drying at low temperature (DLT) and water soaking (WS) for 48 hours). Experiment was performed by shading treatment (full sunlight, 35%, 50%, 75%, and 95% shading). Seeds of Parasenecio firmus were surveyed the highest germination rate (61.1%) in full sunlight with WS (overall 25.7~61.1%). Height was surveyed the highest under 95% shading. And root collar diameter was surveyed the highest in full sunlight. Fresh weights (leaf, shoot, root and total) were the highest under 50% shading. Dry weights (leaf, shoot and total) were the highest under 75% shading. It was indicated the lowest leaf, shoot, root and total under 95% shading. Leaf growth (leaf area, leaf length, leaf width and leaf thickness) and root growth (total root length, root project area, root surface area, root diameter and root volume) were good under 35%~75% shading, but the lowest under 95% shading. As a result of surveying the whole experiment, seed of Parasenecio firmus grows well under 50%~75% shading after germination by high sunlight with water soaking (WS).

Functionalities of Squid Liver Hydrolysates (오징어 간 가수분해물의 기능성)

  • Lee, Su-Seon;Park, Si-Hyang;Park, Joo-Dong;Konno, Kunihiko;Choi, Yeung Joon
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.41 no.12
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    • pp.1677-1685
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    • 2012
  • The autolysate and hydrolysate of a common squid liver, Todarodes pacificus, were prepared. Autolysis (liver ratio, pH, temperature) and Protamex-treated hydrolysis (pH, temperature, ratio of protease to liver) conditions were optimized by response surface methodology using central composite design for under 1 hr of hydrolysis time. The desirability profile indicated that maximum DH could be achieved at a squid liver of 93.5%, pH 6.4, and $47^{\circ}C$ in autolysis, while that of Protamex-treated hydrolysis did at a Protamex-to-squid liver level of 0.33%, pH 6.0, and $55^{\circ}C$. Three amino acids, proline, cysteine, and methionine, were not detected in the total amino acid composition of the Protamex-treated hydrolysate, while they were detected in the free amino acid composition. Cadmium was $8.32{\pm}0.03$ mg/100 g-powder for raw, $3.56{\pm}0.02$ mg/100 g-powder for the autolysate, and $13.26{\pm}0.04$ mg/100 g powder for the Protamex-treated hydrolysate. The major molecular weight ranged from 1.0 to 1.5 kDa for the autolysate and from 210 to 470 Da for the Protamex-treated hydrolysate. Food functionalities of the autolysate, such as surface hydrolphobicity, emulsion activity index, emulsion stability, water, and fat adsorption, were similar to the Protamex-treated hydrolysate. Both the autolysate and Protamex-hydrolysate showed high inhibitory activities on the angiotensin-I converting enzyme. Cell toxicity against the HepG2 cell line was not detected in the autolysate or the Protamex-treated hydrolysate by 200 ${\mu}g/mL$.

Application of CFD Simulation to Cooling System Design of Agricultural Products Processing Center Workplace (농산물산지유통센터 작업장의 냉방 설계를 위한 CFD 시뮬레이션 적용)

  • Kwon, Jin-Kyung;Lee, Sung-Hyun;Moon, Jong-Pil;Lee, Su-Jang;Kim, Keyong-Won
    • Journal of Bio-Environment Control
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    • v.19 no.4
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    • pp.195-202
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    • 2010
  • Cooling air-conditioning of APC (Agricultural Products processing Center) workplace is important to improve the working environment in the summer season. As existing cooling systems for air-conditioning of whole workplace are inefficient because of their high equipment operating costs, relatively inexpensive cooling system is required. The objectives of this study were to simulate the thermal flow fields in APC workplace having the positive and negative pressure type fan and pad systems and spot cooling system by using CFD software (FLUENT, 6.2) and estimate the cooling effectiveness of respective cooling systems. The results showed that the negative pressure type fan and pad system was inappropriate for the present APC workplace because of excessive outside air influx from open gateway and the positive pressure type fan and pad system created relatively low temperature field but non-uniform velocity field at worker positions. The spot cooling system could supply cool air to worker positions with relatively constant air velocity and temperature.

The Wearing Effect of Sport Underwear -Focusing on the Loss of Weight and Amount of Sweat according to the Materials- (운동용 속옷의 착용효과 -소재별 발한량과 체중감량을 중심으로-)

  • Na, Mi-Hyang;Kim, Mi-Sun;Jung, Bock-Hee
    • Korean Journal of Human Ecology
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    • v.11 no.3
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    • pp.273-285
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    • 2002
  • Three materials for sport underwear were manufactured by order for study, and among them, suitable material in order to perform an experiment on the effect of wearing was adopted. The results are as follows: The result of wearing an experimental clothes for sports manufactured as a foundation-type underwear for sports showed that if the same compositional materials were applied, laminating material had higher rate than that of others in the amount of sweat. Concerning relative humidity in clothes and the amount of sweat absorbed in clothes among the two kinds of materials which were produced by laminate, material 2(nylon+modal) was statistically exerts higher influence on the amount of sweat. The humidity in clothes keeps the optimal condition of 59.8%, and breast part showed the highest relative humidity. The material 2(nylon+modal) showed the highest comfortableness, the sense of warmth, humidity and voluminousness, and the sense of pressure. Follow-up survey revealed that in case of material 2, higher amount of sweat than that of the group objects in its early phase, and the amount of sweat varies from individuals. The temperature in clothes of folded parts of experimental clothes and maximum surface temperature was equivalent to that of average skin. With the lapse of time, the weight decreased of 11.03% in maximum, and 3.12% in minimum. The amount of change in the girth was greater in part of body frame than that of limbs, and especially, navel and waist part showed high decrease, and upper breast, breast and the largest part of abdomen showed relatively low decrease. The above experiment revealed that materials for suitable to the underwear for sports for loss of weight by an exercise should be made of doubled-nylon and modal, along with the laminate processing, which heightens the amount of sweat. Thus, wearing an experimental wear gave satisfaction in the view of the beauty of appearance as it did not discharge flowing secretion to the outside at the time of exercise.

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