• Journal of the Korean Vacuum Society
• /
• v.8 no.2
• /
• pp.93-101
• /
• 1999

The purposed of this paper is to investigate the electrical and thermal stability of Polyvinylidene fluoride(PVDF) organic thin films prepared by the vapor deposition method. The differential scanning calorimetry curve of the PVDF organic thin films prepared by increasing substrate temperature showed that the melting curve increased from $128^{\circ}C$ to $142^{\circ}C$. This result implied that the PVDF organic thin film prepared by increasing substrate temperature increased intermolecular force in the crystalline region. The anomalous properties in dielectric constant and dielectric loss at low frequency and high temperature were described for PVDF organic thin film containing impurity carriers. It was confirmed that in view of electric conductive characteristics the ohm's law is satisfied in the range of lower electric field and ln J was proportional to the electric field ln E as like the conventional property of ionic conduction in the range of higher electric field. It was confirmed that major carrier of conductivity was ions. The electrical stability was improved according to an increase of the substrate temperature. On the basis of this experimental result, it could be observed that the optimum temperature of substrate for the electrical and thermal stability was at $105^{\circ}C$.

• Atmosphere
• /
• v.23 no.1
• /
• pp.13-21
• /
• 2013

In this study, the effects of atmospheric stability and surface temperature on the microscale local airflow are investigated in a hydrological suburban area using a computational fluid dynamics (CFD) model. The model domain includes the river and industrial complex for analyzing the effect of water system and topography on local airflow. The surface boundary condition is constructed using a geographic information system (GIS) data in order to more accurately build topography and buildings. In the control experiment, it is shown that the topography and buildings mainly determine the microscale airflow (wind speed and wind direction). The sensitivity experiments of atmospheric stability (neutral, stable, and unstable conditions) represent the slight changes in wind speed with the increase in vertical temperature gradient. The differential heating of ground and water surfaces influences on the local meteorological factors such as air temperature, heat flow, and airflow. These results consequentially suggest that the meteorological impact assessment is accompanied by the changes of background land and atmospheric conditions. It is also demonstrated that the numerical experiments with very high spatial resolution can be useful for understanding microscale local meteorology.

• Korean Journal of Clinical Pharmacy
• /
• v.8 no.1
• /
• pp.54-58
• /
• 1998

The stability of ceftriaxone sodium 100 mg/ml in the water for injection was tested at two temperature conditions (refrigerator and room temperature) and two storage containers (vitro and syringe). The stability of each sample was determined by high-performance liquid chromatography while storing for 5 days at room temperature and 27 days at refrigerator. The concentration of ceftriaxone sodium was 100 mg/ml which the hospital usually use as a filling preparation for I.V. push or Y-site injection. There was no significant difference between the storage in vials and syringes. There was no significant difference in the change of concentration until storing the reconstituted ceftriaxone sodium injection for 2 days at room temperature and 14 days at refrigerator. In conclusion, the ceftriaxone sodium 100 mg/ml in the water for injection can be stored in vial or syringe for 2 days at room temperature and 14 days at refrigerator after preparation.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2001.07a
• /
• pp.1022-1025
• /
• 2001

This paper presents the characteristics of TaN thin-film as high-temperature strain gauges, which were deposited on Si substrate by DC reactive magnetron sputtering in an argon-nitrogen atmosphere(Ar-(4∼20%)N$_2$). The electrical and mechanical characteristics of these films investigated with the thickness range 1650∼1870${\AA}$ and room temperature resistivities in the range 178.3 ${\mu}$$\Omega$cm to 3175.7 ${\mu}$$\Omega$cm. The TaN thin-film strain gauge deposited in Ar-(20%)N$_2$atmosphere is obtained a temperature coefficient of resistance(TCR), 0∼-1357 ppm/$^{\circ}C$ in the temperature range 25∼275$^{\circ}C$ and a high temporal stability with a longitudinal gauge factor, 2.92∼3.47. Because of their high resistivity, low TCR and linear gauge factor, these cermet thin-film may allow high-temperature strain gauges miniaturization.

• Fire Science and Engineering
• /
• v.28 no.2
• /
• pp.76-81
• /
• 2014

Structural stability of structural beams at high temperature had been evaluated though a horizontal furnace and a standard fire curve. If a structural method and a material are satisfied with the fire test, those are seemed to be guaranteed the safety of residences, fire services men, and properties of the buildings. However, that requires not only longer period but higher cost for making and testing of each structural element. That restrained from developing new methods and new fire protective materials. In this study, an analytic method was executed to demonstrate whether the analytic method using mechanical properties of structural steel at high temperature with heat transfer theory works is working. In this paper, the surface temperature rising and variance of structural stability of a simple H-section beam with a standard fire curve were evaluated and structural stabilities of H-section beam according to differences from length of beam were suggested.

• Interaction and multiscale mechanics
• /
• v.5 no.1
• /
• pp.1-12
• /
• 2012

Considerable longitudinal rail forces and displacements may develop in continuous welded rail (CWR) track on long-span bridges due to temperature variations. The track stability may be disturbed due to excessive relative displacements between the sleepers and ballast bed and the accompanied reduction in frictional resistance. For high-speed tracks, however, solving these problems by installing rail expansion devices in the track is not an attractive solution as these devices may cause a local disturbance of the vertical track stiffness and track geometry which will require intensive maintenance. With reference to temperature, two actions are considered by the bridge loading standards, the uniform variation in the rail and deck temperature and the temperature gradient in deck. Generally, the effect of temperature gradient has been disregarded in the interaction analysis. This paper mainly deals with the effect of temperature gradient on the track-bridge interaction with respect to the support reaction, rail stresses and stability. The study presented in this paper was not mentioned in the related codes so far.

• Journal of the Korean Ceramic Society
• /
• v.47 no.3
• /
• pp.223-231
• /
• 2010

The serious issue of tall building is to ensure the fire-resistance of high strength concrete. The fire resistant finishing method is necessarily essential in order to satisfy the fire resistance time of 3 h required by the law. The fire resistant finishing method is installed by applying a fire resistant material as a method of shotcrete or a fire resistant board to high strength concrete surface. This method can reduce the temperature increase of the reinforcement embedded in high strength concrete at high temperature due to the installation thickness control. This study is interested in identifying the effectiveness of inorganic alumino-silicate compounds including the inorganic admixture such as fly ash and meta-kaolin as the fire resistant finishing materials through the analysis of fire resistance and components properties at high temperature. The study results show that the fire resistant finishing material composed of fly ash and meta-kaolin has the thermal stability of the slight decrease of compressive strength at high temperature. These thermal stability is caused by the ceramic binding capacity induced by alkali activation reaction by the reason of the thermal analysis result not showing the decomposition of calcium hydrate. Inorganic compounds composed of fly ash and meta-kaolin is evaluated to be very effective as the fire resistance material for finishing to protect the concrete substrate by the reason of those simplicity in both application and manufacture. The additional study about the adhesion in the interface with concrete substrate is necessary for the purpose of the practical application.

• Journal of Power System Engineering
• /
• v.21 no.2
• /
• pp.20-26
• /
• 2017

This study was carried out to investigate the effect of precipitate on the high temperature deformation stability of incoloy 825 alloy. $Cr_{23}C_6$ carbide was precipitated under $950^{\circ}C$, but was not detected over $1,000^{\circ}C$. Most of the precipitation consist of $Cr_{23}C_6$ carbide. Strain-rate sensitivity was the highest in 0.01/s and the lowest in 10/s. Strain-rate sensitivity was decreased sharply below $950^{\circ}C$. In the temperature between $850^{\circ}C{\sim}1,150^{\circ}C$, plastic instable area did not exist. It showed the lowest Ziegler Parameter value of 0.06 Ziegler Parameter was the lowest as 0.06 at $850^{\circ}C$ with 10s-1 of strain. The highest Ziegler Parameter value(0.43) was found in plastic deformation at $1,050^{\circ}C$ with 0.01s-1 of strain. It tends to have an higher resistance to the high temperature deformation under $950^{\circ}C$, due to the precipitation.

• Journal of The Korean Digital Architecture Interior Association
• /
• v.12 no.4
• /
• pp.59-66
• /
• 2012

This study is interested in identifying the effectiveness of alkali-activated fire protection material compounds including the alkali-activator such as potassium hydroxide, sodium silicate and fly ash as the fire resistant finishing materials. Also, this paper is concerned with change in compressive strength and pore structure of the alkali-activated fire protection material at high temperatures. The testing methods of fire protection materials in high temperature properties are make use of TG-DSC and mercury intrusion porosimetry measurements. This study results show that compressive strength is rapidly degraded depending on a rise of heating temperature. Porosity showed a tendency to increase irrespective of specimen types. This is due to both the outbreak of collapse of gel comprising the cement and a micro crack by heating. However, alkali-activated fire protection material composed of potassium hydroxide, sodium silicate and fly ash has the thermal stability of the slight decrease of compressive strength and porosity at high temperature. These thermal stability is caused by the ceramic binding capacity induced by alkali activation reaction by the reason of the thermal analysis result not showing the decomposition of calcium hydrate.

• Journal of the Korean Ceramic Society
• /
• v.55 no.1
• /
• pp.50-54
• /
• 2018

This study investigated the long-term durability of catalyst(Pd or Fe)-infiltrated solid oxide cells for $CO_2$/steam co-electrolysis. Fuel-electrode supported solid oxide cells with dimensions of $5{\times}5cm^2$ were fabricated, and palladium or iron was subsequently introduced via wet infiltration (as a form of PdO or FeO solution). The metallic catalysts were employed in the fuel-electrode to promote $CO_2$ reduction via reverse water gas shift reactions. The metal-precursor particles were well-dispersed on the fuel-electrode substrate, which formed a bimetallic alloy with Ni embedded on the substrate during high-temperature reduction processes. These planar cells were tested using a mixture of $H_2O$ and $CO_2$ to measure the electrochemical and gas-production stabilities during 350 h of co-electrolysis operations. The results confirmed that compared to the Fe-infiltrated cell, the Pd-infiltrated cell had higher stabilities for both electrochemical reactions and gas-production given its resistance to carbon deposition.