• Title/Summary/Keyword: Hexagonal plate

Search Result 50, Processing Time 0.034 seconds

The Preparation and Magnetic Properties in Ba-ferrite Film on the A12O3 Substrate (A12O3을 하지층으로 하는 Ba-ferrite 박막의 제조 및 자기적 특성에 관한 연구)

  • Sur, Jung-Chul;Park, Chul-Jin;Choi, Jung-Wan
    • Journal of the Korean Magnetics Society
    • /
    • v.15 no.2
    • /
    • pp.125-129
    • /
    • 2005
  • Ba-Ferrite thin films were prepared on $A1_2O_3$ substrate by a pulsed laser deposition system and characterized by SEM, $M\ddot{o}$ssbauer spectroscopy and VSM. The appropriate conditions of pulsation in Ba-ferrite was the oxygen pressure of 0.1 Torr at a substrate temperature of $400^{\circ}C$ and the thickness was variable with the deposition time. Ba-ferrite crystals had the forms of hexagonal plate in the 5 minute deposited film and the needle grains coexisted with the increasing film thickness. $M\ddot{o}ssbauer$ spectroscopy assured that the direction of atomic spin in Fe ion tends to normal to the substrate in the hexagonal plate. The VSM curves have the two types hysteresis of hexagonal and needle phase.

Fabrication of Size- and Shape- Controlled Gold Particles using Wet Chemical Process (환원 석출법을 이용한 모양과 크기가 제어된 금 입자의 제조)

  • Hong, So-Ya;Lee, Chang-Hwan;Kim, Joo-Yong
    • Textile Coloration and Finishing
    • /
    • v.22 no.2
    • /
    • pp.123-131
    • /
    • 2010
  • Shape and size controlled synthesis of gold particles has been studied by using wet-chemical method. When ${AuCl_4}^-$ in aqueous $HAuCl_4$ precursor was reduced using $Na_2SO_3$ as a reducing agent, mixtures of spherical, triangular and hexagonal particles were prepared in a few minutes. It was found that the shape selective oxidative etching by ${AuCl_4}^-\;+\;Cl^-$ anions and crystal growth took place simultaneously. As the ${AuCl_4}^-$ and $Cl^-$ concentration increased, yields of large triangular and hexagonal plate type particles increased, while the spherical particles decreased in most cases. Possible etching and growth mechanisms are discussed.

Growth of GaN Thin-Film from Spin Coated GaOOH Precursor (GaOOH 선구체의 스핀코팅에 의한 GaN 박막의 성장)

  • Lee, Jae-Bum;Kim, Seon-Tai
    • Korean Journal of Materials Research
    • /
    • v.17 no.1
    • /
    • pp.1-5
    • /
    • 2007
  • GaN thin fan were grown by spin coated colloidal GaOOH precursor. Polycrystalline GaNs with crystalline size of $10{\sim}100nm$ were grown on $SiO_2$ substrate. The shape of crystallite above $900^{\circ}C$ had the hexagonal plate and column type. X-ray diffraction patterns for them correspond to those of the hexagonal wurtzite GaN. With increasing droplets. i.e, thickness of deposited layers, XRD intensity increased. PL (photoluminescence) spectrum consisted with an weak near band-edge emission at 3.45 eV and a broad donor-acceptor emission band at 3.32 eV. From the low temperature PL measurement on GaN grown at $800^{\circ}C$ that the shallow donor-acceptor recombination induced emission was more intense than the near band-edge excitonic emission.

Crystal Habits of Corundum Single Crystals Grown in Cryolite Flux (빙정식 융제로 성장한 Corundum 단결정의 결정형)

  • 장진욱;이태근;정수진
    • Journal of the Korean Ceramic Society
    • /
    • v.29 no.6
    • /
    • pp.463-470
    • /
    • 1992
  • Corundum single crystals were grown in cryolite flux with the composition of Na3AlF6:Al2O3=80:20 wt%. This mixture was melted at 115$0^{\circ}C$, followed by slow cooling at a rate of 2$^{\circ}C$/hr to 96$0^{\circ}C$. And by adding of La2O3 to the flux, the change of crystal forms were observed. Crystal forms of corundum grown in cryolite flux had the habits of hexagonal plate which consist of well developed {0001} face and small {101} face. As La2O3 was added and its content was increased, {223} and {110} faces were developed, and crystal habits of equidimensional forms changed into hexagonal prism form. In a charge of 8 mole% B2O3, Al2O3:La2O3=15:1, transparent corundum single crystals of equent form were grown. As the content of B2O3 was increased, twineed crystals which have twin law of 2-fold parallel to [0001], and composition plane of (110) were grown.

  • PDF

Synthesis of $Ni_2Y$ magnetic particles by coprecipitation method (공침법에 의한 $Ni_2Y$ 자성 분말의 합성)

  • 김한근;사공건
    • Electrical & Electronic Materials
    • /
    • v.9 no.9
    • /
    • pp.906-910
    • /
    • 1996
  • Ferroxplana N $i_{2}$Y(B $a_{2}$N $i_{2}$F $e_{12}$ $O_{22}$ ) magnetic particles, which is one of the hexagonal ferrite were synthesized by a coprecipitation method. The coprecipitates were prepared by adding aqueous solution of BaC $I_{2}$ - 2 $H_{2}$O, NiC $I_{2}$ - 6 $H_{2}$O and FeC $I_{3}$ - 6 $H_{2}$O(of which the mole ratio is $Ba^{+2}$ : N $i^{+2}$ : F $e^{3+}$= 1 : 1 : 6) to a mixture of NaOH and N $a_{2}$C $O_{3}$. The shape of Ferroxplana N $i_{2}$Y magnetic particles obtained at 1, 100(.deg. C) was hexagonal plate-like, average particle size and aspect ratio were 2(.mu.m) and 7, respectively.y.

  • PDF

Synthsis of Ferroxplana Y-type($Ni_2Y$) Magnetic Particles (Ferroxplana Y-type($Ni_2Y$) 자성(磁性) 분체의 합성)

  • Park, S.H.;Kim, H.G.;SaGong, G.
    • Proceedings of the KIEE Conference
    • /
    • 1993.07b
    • /
    • pp.1140-1142
    • /
    • 1993
  • It has been prepared by a coprecipitation method for Ferroxplana $Ni_2Y\;(Ba_2Ni_2Fe_{12}O_{22}$ magnetic particles, which is one of the Hexagonal ferrite. The coprecipitates were synthesized by adding aqueous solution of $BaCl_2{\cdot}2H_2O,\;NiCl_2{\cdot}6H_2O\;and\;FeCl_2{\cdot}4H_2O$ (of which the mole ratio is $Ba^{2+}:Ni^{2+}:Fe^{2+}$=1:1:6) to a mixture of NaOH and $Na_2CO_3$ solution. The shape of Ferroxplana $Ni_2Y$ magnetic particles obtained at the calcined temperature 1,100($^{\circ}C$) was hexagonal plate-like, average particle size was 2(${\mu}m$), and aspect ratio was more than 7.

  • PDF

Transient Piezothermoelasticity of a Piezo Ceramic Plate Subjected to Antisymmetric Thermal Load and Symmetric Thermal Load (압전 Ceramics 평판의 비대칭열부하와 대칭열부하에 의한 과도 압전열탄성 해석에 관한 연구)

  • Kim, Gyeong-Seok;Choe, Jeong-Seok;Yang, Seung-Pil;Kim, Yong-Uk
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.21 no.1
    • /
    • pp.133-143
    • /
    • 1997
  • Piezoelastic materials have recently attracted considerable attention because of their potential use in intelligent structural systems. In this paper, we treat a transient piezothermoelastic problem in a hexagonal plate of crystal class 6mm subjected to antisymmetric heating temperature. We analyze this problem by use of the potential function method. Numerical calculations are carried out for a cadmium selenide solid, and the results are presented graphically in comparison with those derived from the similar problem in a cadmium selenide plate subjected to symmetric heating temperature for a symmetry transient problem.

A Preliminary Study on a Method for the Morphological and Quantitative Analyses of Individual Snow Crystals and Its Application for Field Measurement

  • Ma, Chang-Jin
    • Asian Journal of Atmospheric Environment
    • /
    • v.5 no.3
    • /
    • pp.196-203
    • /
    • 2011
  • The main aim of this study is to establish methods of morphological preservation and elemental quantification for individual snow crystals. Individual snow crystals were collected at a height of 20 m above ground level. To stabilize and preserve the original morphologies of the snow crystals, cyanoacrylate, which has been used to fix liquid droplets, was applied (Kasahara et al., 2000). Several different kinds of snow crystals (dendrite, sectored plate, quasi-sectored plate, and hexagonal plate) were successively stabilized using this method. The stabilized snow crystals were pretreated with acetone, and then the elemental components contained in a whole snow crystal were quantified with the Particle Induced X-ray Emission (PIXE) analytical technique. The snow crystal residual composition determined in the present study was dominated by sulfur and mineral components, and the elemental mass showed an apparent crystal size dependence, where the elemental mass gradually decreased as the crystal size increased.

Electron Microscopical Observation on the Phage of Bacillus subtilis SNU 816 (Bacillus subtilis SNU 816의 Phage에 대한 전자현미경적 관찰)

  • Ahn, Kyung-Joon;Lee, Zoo-Shik;Lee, Woong-Jik
    • Applied Microscopy
    • /
    • v.12 no.1
    • /
    • pp.69-73
    • /
    • 1982
  • The phages of Bacillus subtilis SNU 816 were observed by electron microscope with their host. The results are as follows; The phage had hexagonal head, contractile tail sheath and base plate with six tail fibers. During the lysis of bacteria due to attack of phage, dissolution of flagella were initiated from distal end of flagella.

  • PDF

Conditions for the Formation of Ba-Ferrite by Hydrothermal Synthesis (수열합성에 의한 Ba-Ferrite의 형성조건)

  • 이경희;이병하;윤갑중
    • Journal of the Korean Ceramic Society
    • /
    • v.22 no.5
    • /
    • pp.61-65
    • /
    • 1985
  • This stud deals with the conditions for the Formation of Ba-Ferrite by Hydrothemal synthesis Suspensions Containing either iron(III) hydroxide or hydroxide oxide and barium ians were subjected to autoclavings at various temperatures from 150 to 30$0^{\circ}C$. A ferromagnetic precipitate BaO.$6Fe_2O_3$ consisting of hexagonal plate-like particle was obtained by suitable combination of temperature and concentration of KOH

  • PDF