• 제목/요약/키워드: Heat treatment methods

검색결과 913건 처리시간 0.026초

데침과 열수의 침적과 Trehalose 처리가 오이 물김치의 저장중 품질에 미치는 영향 (The Properties of Blanching and Brining in Hot Solution and Trehalose Treatment on the Quality of Cucumber Kimchi during Fermentation)

  • 이혜정
    • 한국식품영양학회지
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    • 제14권4호
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    • pp.333-338
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    • 2001
  • In research. which Korean pickled cucumber was treated wish various methods, including blanching. brining in hot solution, and treating with trehalose. I examined the changes of properties of material. The Korean pickled cucumber were fermented 4∼5$^{\circ}C$ for 42 days in 1% salt solution. The physiochemical properties were pH, total acidity, total cell count, lactic acid bacteria and texture properties were also evaluated. The result showed that the effect of blanching and soaking cucumber in 100$^{\circ}C$ hot salt solution significantly reduced the softening rate of texture while a rather rapid fermentation was found for those preserved with salt. The effect of trehalose treatment inhenced fermentation but it was significantly reduced softening rate of texture. The texture evaluation of Korean pickled cucumber was found that heat treatment with blanching after soaked in hot solution and trehalose treatment had a positive effect for reduction of softening of cucumber tissue.

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Die Life Estimation of Hot Forging for Surface Treatment and Lubricants

  • Dong-Hwan;Byung-Min;Chung-Kil
    • International Journal of Precision Engineering and Manufacturing
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    • 제5권4호
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    • pp.5-13
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    • 2004
  • This study explains the effects of lubricant and surface treatment on the life of hot forging dies. The thermal load and thermal softening, that occur when there is contact between the hotter billet and the cooler dies in hot forging, cause wear, thermal cracking and fatigue, and plastic deformation. Because the cooling effect and low friction are essential to the long life of dies, the proper selection of lubricant and surface treatment is very important in hot forging process. The two main factors that decide friction and heat transfer conditions are lubricant and surface treatment, which are directly related to friction factor and surface heat transfer coefficient. Experiments were performed for obtaining the friction factors and the surface heat transfer coefficients in different lubricants and surface treatments. For lubrication, oil-base and water-base graphite lubricants were used, and ion-nitride and carbon-nitride were used as surface treatment conditions. The methods for estimating die service life that are suggested in this study were applied to a finisher die during the hot forging of an automobile part. The new techniques developed in this study for estimating die service life can be used to develop more feasible ways to improve die service life in the hot forging process.

침탄 처리 소재의 표면 분석을 위한 나노압입시험법의 응용 (Application of Nanoindentation Technique for Characterizing Surface Properties of Carburized Materials)

  • 최인철;오명훈
    • 열처리공학회지
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    • 제35권3호
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    • pp.139-149
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    • 2022
  • In the automobile and shipbuilding industries, various materials and components require superior surface strength, excellent wear resistance and good resistance to repeated loads. To improve the surface properties of the materials, various surface heat treatment methods are used, which include carburizing, nitriding, and so on. Among them, carburizing treatment is widely used for structural steels containing carbon. The effective carburizing thickness required for materials depends on the service environment and the size of the components. In general, however, there is a limit in evaluation of the surface properties with a standardized mechanical test method because the thickness or cross-sectional area of the carburized layer is limited. In this regard, the nanoindentation technique has lots of advantages, which can measure the mechanical properties of the material surface at the nano and micro scale. It is possible to understand the relationship between the microstructural change in the hardened layer by carburizing treatment and the mechanical properties. To be spread to practical applications at the industrial level, in this paper, the principle of the nanoindentation method is described with a representative application for analyzing the mechanical properties of the carburized material.

Quantification of Karanjin, Tannin and Trypsin Inhibitors in Raw and Detoxified Expeller and Solvent Extracted Karanj (Pongamia glabra) Cake

  • Panda, A.K.;Sastry, V.R.B.;Kumar, A.;Saha, S.K.
    • Asian-Australasian Journal of Animal Sciences
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    • 제19권12호
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    • pp.1776-1783
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    • 2006
  • Despite being a rich source of protein (28-34%), karanj (Pongamia glabra) cake is found to be bitter in taste and toxic in nature owing to the presence of flavonoid (karanjin), tannin and trypsin inhibitor, thereby restricting its safe inclusion in poultry rations. Feeding of karanj cake at higher levels (>10%) adversely affected the growth performance of poultry due to the presence of these toxic factors. Therefore, efforts were made to detoxify karanj cake by various physico-chemical methods such as dry heat, water washing, pressure cooking, alkali and acid treatments and microbiological treatment with Sacchraromyces cerevisiae (strain S-49). The level of residual karanjin in raw and variously processed cake was quantified by high performance liquid chromatography and tannin and trypsin inhibitor was quantified by titrametric and colorimetric methods, respectively. The karanjin, tannin and trypsin inhibitor levels in such solvent and expeller pressed karanj cake were 0.132, 3.766 and 6.550 and 0.324, 3.172 and 8.513%, respectively. Pressure-cooking of solvent extracted karanj cake (SKC) substantially reduced the karanjin content at a cake:water ratio of 1:0.5 with 30-minute cooking. Among chemical methods, 1.5% (w/w) NaOH was very effective in reducing the karanjin content. $Ca(OH)_2$ treatment was also equally effective in karanjin reduction, but at a higher concentration of 3.0% (w/w). A similar trend was noticed with respect to treatment of expeller pressed karanj cake (EKC). Pressure cooking of EKC was effective in reducing the karanjin level of the cake. Among chemical methods alkali treatment [2% (w/w) NaOH] substantially reduced the karanjin levels of the cake. Other methods such as water washing, dry heat, HCl, glacial acetic acid, urea-ammoniation, combined acid and alkali, and microbiological treatments marginally reduced the karanjin concentration of SKC and EKC. Treatment of both SKC and EKC with 1.5% and 2.0% NaOH (w/w) was the most effective method in reducing the tannin content. Among the various methods of detoxification, dry heat, pressure cooking and microbiological treatment with Saccharomyces cerevisiae were substantially effective in reducing the trypsin inhibitor activity in both SKC and EKC. Based on reduction in karanjin, in addition to tannin and trypsin inhibitor activity, detoxification of SKC with either 1.5% NaOH or 3% $Ca(OH)_2$, w/w) and with 2% NaOH were more effective. Despite the effectiveness of pressure cooking in reducing the karanjin content, it could not be recommended for detoxification because of the practical difficulties in adopting the technology as well as for economic considerations.

미세혈관 수술 후 혈관 연축의 예방을 위한 개선된 온열전등 (Improved Heat Lamp for Preventing Arterial Spasm after Microvascular Surgery)

  • 안성민;황소민;허은숙;박정미;박경아;오진아
    • Archives of Reconstructive Microsurgery
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    • 제17권2호
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    • pp.120-125
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    • 2008
  • Purpose: Heat therapy by heat lamp after microvascular surgery is being used for preventing blood vessels's contraction and blood-flow's disturbance. As usually, incandescent lamp has been used. But there have been several problems and need for improvement in the existing heat lamp treatment. So we would like to introduce improved heat lamp to keep an appropriate temperature and intensity of illumination. Methods: The existing heat lamps are the ones of general light stands covered with newspaper, having 60 watt light bulb of incandescence and lampshade made of aluminum. We have tried to improve shortcomings of the existing heat lamps by enlarging the size of aluminum lampshade and attaching a curtain that can block heat and light. We conducted a comparative study between the existing and improved heat lamps. Under the assumption that there are several affected parts, we have also measured the distance from heat lamp to patients' eye region and then intensity of illumination. Result: The target temperature of surface was realized in 11 minutes with the maximum temperature reaching at 36.6 degrees C in 28 minutes at the existing heat lamp while the target temperature reached in 7 minutes with the maximum temperature reaching at 39.0 degrees C in 17 minutes at the improved heat lamp. The existing and improved heat lamp showed 38 lx and 0.1 lx of intensity of lumination, respectively. Conclusion: Using improved heat lamps, we can keep an appropriate temperature and we think we can make contribution to patients' treatment by making them and their neighbors able to sleep with minimized disturbance thanks to low intensity of illumination secured by blocking light.

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An in vivo electromyographic evaluation of pain relief using different therapies in masticatory myalgia patients

  • Balakrishnan, Parvathi K.;Kumar, Sowmya M.;Chippala, Purushotham;Hegde, Chethan
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • 제46권5호
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    • pp.321-327
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    • 2020
  • Objectives: This study is aimed to evaluate and compare the effect of moist heat fomentation therapy with ultrasound therapy in patients with the masticatory myalgia. Materials and Methods: The study was conducted on 42 patients with masticatory myalgia, dividing them into two groups; Group A (21 patients), received moist heat therapy and Group B (21 patients), received ultrasound therapy for seven effective days. Prior and after the treatment the numeric rating scale (NRS) and the electromyography (EMG) scores were recorded and compared. The observations were analyzed clinically and statistical support was taken to assess the NRS and EMG data. Results: Irrespective of the groups, patients testified a significant reduction in pain after the treatment. From the EMG readings; even though the standard deviation for each group was varied considerably, EMG recorded an improved muscle activity. Statistical analysis was used to assess and identify the best treatment methodology between the two modalities. Conclusion: From the statistical analysis, it is concluded that, though both the therapies had significantly reduced the symptomatic response, it is moist heat fomentation that improved muscle activity both statistically and clinically in comparison to ultrasound.

Chemical and Micro-Structural Changes in Glass-Like Carbon during High Temperature Heat Treatment

  • Lim, Yun-Soo;Kim, Hee-Seok;Kim, Myung-Soo;Cho, Nam-Hee;Sahn Nahm
    • Macromolecular Research
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    • 제11권2호
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    • pp.122-127
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    • 2003
  • A glass-like carbon was fabricated using furan resin. The influence of heat treatment temperature during fabrication process on the chemical and micro-structural changes was studied by various analytical and spectroscopic methods including TGA, FT-IR, CHN, TEM and XRD. The chemical resistance properties of the fabricated glass-like carbon were also investigated. It has been found that the heat-treated samples at higher temperature up to 2600 $^{\circ}C$ in $N_2$ atmosphere had little weight loss, small amounts of functional groups, and high carbon content. The fabricated glass-like carbons upon heat treatment at 2600 $^{\circ}C$ showed an amorphous stage without any grain growth and/or reconstruction of structure. The glass-like carbon had much better chemical resistance than the artificial graphite, and exhibited a high chemical resistance due to its low surface areas, minimum impurities, and low graphite crystallites.

볼 밀링에 의한 Al-Ti 계 금속간화합물 생성 거동 (Formation Behaviour Al-Ti Intermetallic Compounds by Ball milling methods)

  • 안인섭
    • 한국분말재료학회지
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    • 제6권1호
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    • pp.42-48
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    • 1999
  • Three mixtures of elemental powders of Al-25at.%Ti, 48at.%Ti and 70at.%Ti were offered to ball milling process for the formation of intermetallic compounds of $Al_3Ti$, AlTi and $Ti_3Al$. Ballmilling or attrition process were carried out at the condition of rotaing speed of 110 or 350 rpm at $10^{-3}$ torr vacuum or argon atmospheres. $Al_3Ti$phases were fully obtained by heat treatment for 1 hors at $600^{\circ}C$ with Al-25at.%Ti composition mixtures milled by 100 hours. The amorphous phase was completely formed at the composition of Al-48at.%Ti mixed powders by milling 100hours at the 50 to 1 weight ratio of ball to powder, and AlTi compounds were obtained by heat treament. In the case of Al-70at%Ti mixed powders milled for 100 hours, $Ti_3Al$ and $Al_3Ti$intermetallic compounds were formed by heat treatment for 1 hour at $600^{\circ}C$. By attrition milling of 350rpm for 10 hours, $Ti_3Al$ phase was formed completley after heat treatment for 1 hour at $600^{\circ}C$.

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FDM에 의한 응고해석시 계산시간 단축을 위한 음적해법의 적용과 잠열처리방법 (Reduction of Computing Time through FDM using Implicit Method and Latent Heat Treatment in Solidification Analysis)

  • 김태규;최정길;홍준표;이진형
    • 한국주조공학회지
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    • 제13권4호
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    • pp.323-332
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    • 1993
  • An implicit finite difference formulation with three methods of latent heat treatment, such as equivalent specific heat method, temperature recovery method and enthalpy method, was applied to solidification analysis. The Neumann problem was solved to compare the numerical results with the exact solution. The implicit solutions with the equivalent specific heat method and the temperature recovery method were comparatively consistent with the Neumann exact solution for smaller time steps, but its error increased with increasing time step, especially in predicting the solidification beginning time. Although the computing time to solve energy equation using temperature recovery method was shorter than using enthalpy method, the method of releasing latent heat is not realistic and causes error. The implicit formulation of phase change problem requires enthalpy method to treat the release of latent heat reasonably. We have modified the enthalpy formulation in such a way that the enthalpy gradient term is not needed, and as a result of this modification, the computation stability and the computing time were improved.

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Influence of heat treatment on the microstructure and the physical and mechanical properties of dental highly translucent zirconia

  • Dimitriadis, Konstantinos;Sfikas, Athanasios Konstantinou;Kamnis, Spyros;Tsolka, Pepie;Agathopoulos, Simeon
    • The Journal of Advanced Prosthodontics
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    • 제14권2호
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    • pp.96-107
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    • 2022
  • PURPOSE. Microstructural and physico-mechanical characterization of highly translucent zirconia, prepared by milling technology (CAD-CAM) and repeated firing cycles, was the main aim of this in vitro study. MATERIALS AND METHODS. Two groups of samples of two commercial highly-translucent yttria-stabilized dental zirconia, VITA YZ-HTWhite (Group A) and Zolid HT + White (Group B), with dimensions according to the ISO 6872 "Dentistry - Ceramic materials", were prepared. The specimens of each group were divided into two subgroups. The specimens of the first subgroups (Group A1 and Group B1) were merely the sintered specimens. The specimens of the second subgroups (Group A2 and Group B2) were subjected to 4 heat treatment cycles. The microstructural features (microstructure, density, grain size, crystalline phases, and crystallite size) and four mechanical properties (flexural strength, modulus of elasticity, Vickers hardness, and fracture toughness) of the subgroups (i.e. before and after heat treatment) were compared. The statistical significance between the subgroups (A1/A2, and B1/B2) was evaluated by the t-test. In all tests, P values smaller than 5% were considered statistically significant. RESULTS. A homogenous microstructure, with no residual porosity and grains sized between 500 and 450 nm for group A and B, respectively, was observed. Crystalline yttria-stabilized tetragonal zirconia was exclusively registered in the X-ray diffractograms. The mechanical properties decreased after the heat treatment procedure, but the differences were not statistically significant. CONCLUSION. The produced zirconia ceramic materials can be safely (i.e., according to the ISO 6872) used in extensive fixed prosthetic restorations, such as substructure ceramics for three-unit prostheses involving the molar restoration and substructure ceramics for prostheses involving four or more units. Consequently, milling technology is an effective manufacturing technology for producing zirconia substructures for dental fixed all-ceramic prosthetic restorations.