• Journal of the Korean Ceramic Society
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• v.29 no.8
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• pp.601-608
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• 1992

We investigated the influence of several processes, including the preparation of slurry and preform and the heat-treatment of the preform, on the properties of composites to fabricate the carbon-fiber reinforced glass composites having good mechanical properties. Cerander was determined to be the best binder among Cerander, Rhoplex and Elvacite 2045 by the dipping test and the binder within a preform could be completely eliminatd by burning out the specimen under 10-6 Torr at 400$^{\circ}C$ for more than 1h. The fracture behavior of a composite was largely dependent on the uniformity of carbon-fiber distribution within the composite and the heat-treatment condition of the composite. The higher the glass content, the more difficult to obtain uniform distribution of carbon-fiber. As the hot-pressing temperature increased, the densification process of the composite and the formation of pore due to oxidation of carbon fiber occurred competitively. But, above 1000$^{\circ}C$ the latter played a predominant role. We could fabricated the densest 15 vol.% carbon-fiber-content glass composite having the highest toughness and flexural strength of 250 MPa by hot-pressing under 15 MPa at 900$^{\circ}C$ for 30 min.

• Fire Science and Engineering
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• v.30 no.2
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• pp.35-42
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• 2016

The membrane structure provides high satisfaction with lightweight, improved workability, reduced cost, and a free shape. Thus, its applications expanding. On the other hand, in an architectural membrane that is vulnerable to fire, the development of various architectural membranes with flame resistance is in demand. Therefore, this study applied basalt woven fabric safety for flame resistance, excellent heat insulation and thermal properties on an architectural membrane. The PTFE- coated basalt woven fabric membrane was compared with a PTFE coated glass fiber membrane by DSC/TGA, strength properties, flammability, and incombustibility properties. In addition, this study confirmed the membrane applicability of basalt woven fabric and basalt-glass hybrid woven fabric through a comparison with existing architectural membranes.

• Korean Journal of Materials Research
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• v.34 no.3
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• pp.175-183
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• 2024

Geopolymer, also known as alkali aluminum silicate, is used as a substitute for Portland cement, and it is also used as a binder because of its good adhesive properties and heat resistance. Since Davidovits developed Geopolymer matrix composites (GMCs) based on the binder properties of geopolymer, they have been utilized as flame exhaust ducts and aircraft fire protection materials. Geopolymer structures are formed through hydrolysis and dehydration reactions, and their physical properties can be influenced by reaction conditions such as concentration, reaction time, and temperature. The aim of this study is to examine the effects of silica size and aging time on the mechanical properties of composites. Commercial water glass and kaolin were used to synthesize geopolymers, and two types of silica powder were added to increase the silicon content. Using carbon fiber mats, a fiber-reinforced composite material was fabricated using the hand lay-up method. Spectroscopy was used to confirm polymerization, aging effects, and heat treatment, and composite materials were used to measure flexural strength. As a result, it was confirmed that the longer time aging and use of nano-sized silica particles were helpful in improving the mechanical properties of the geopolymer matrix composite.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2000.11a
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• pp.11-14
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• 2000

This paper presents the vibration control of a glass-fiber reinforced thermoplastic composite beam with a distributed PVDF sensor and piezo-ceramic achlator. The three types of different controllen which are PID, H$\infty$ , and p-synthesis ontrollcr are employed to achieve vibration suppression in the transient vibration of composite beam. In the H$\infty$ , controller design, 1st and 2nd natural frequencies are considered in the modeling, because robust control theory which has robustness to struchred uncertainty is adopled Lo suppress the vibration. If the controller designed by H$\infty$ , theory does not satisfy control performance, it is improved by $\mu$ -synthesis method with D-K iteration so that the$\mu$-contoller based on the structured singular value satisfies the nominal performance and robust performance Simulations and experiments were carried out with the designed controllers m order to demonstrate the suppression efficiency of each controller.

• Korean Journal of Materials Research
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• v.31 no.1
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• pp.54-59
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• 2021

In this work, narrow-band green-emitting CsPbBr3 particles are embedded in commercialized glass composites by a facile dry process. By optimizing the method through sintering in glass frit (GF) composites including CsBr and PbBr2, used as precursors, the encapsulation of CsPbBr3 particles made them waterproof with green fluorescence. To improve the fluorescent properties by reducing aggregation of CsPbBr3, fumed silica (FS) is additionally used to help particles avoid bulking up in the glass matrix. The CsPbBr3 perovskite/glass composites are characterized using scanning electron microscopy (SEM) images and energy-dispersive X-ray spectroscopy (EDS) maps, which support the existence of CsPbBr3 particles in the glass matrix. The photoluminescence (PL) properties demonstrate that the emission spectrum peak, full width at half maximum (FWHM), and photoluminescence quantum yield (PLQY) values are 519 nm, 17 nm, and 17.7 %. We also confirm the water-resistant properties. To enhance water/moisture stability, the composite sample is put directly into water, with its PLQY monitored periodically under UV light.

• Journal of the Korean Ceramic Society
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• v.53 no.4
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• pp.386-392
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• 2016

Heat insulation plates of fumed silica were prepared by mixing fumed silica, SiC powder and chopped glass fiber by a high speed mixer followed by pressing of the mixture powder in a stainless steel mold of $100{\times}100mm$. Composition of the plates, particle size of SiC, and type of inorganic binder were varied for observation of their contribution to heat insulation of the plate. The plate was installed on the upper portion of an electric furnace the inside temperature of which was maintained at $400^{\circ}C$ and $600^{\circ}C$, for investigation of heat transfer through the plate from inside of the electric furnace to outside atmosphere. Surface temperatures were measured in real time using a thermographic camera. The particle size of SiC was varied in the range of $1.3{\sim}17.5{\mu}m$ and the insulation was found to be most excellent when SiC of $2.2{\mu}m$ was incorporated. When the size of SiC was smaller or larger than $2.2{\mu}m$, the heat insulation effect was decreased. Inorganic binders of alkali silicate and phosphate were tested and the phosphate was found to maintain the heat insulation property while increasing mechanical properties.

• Journal of the Korean Ceramic Society
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• v.43 no.10 s.293
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• pp.607-612
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• 2006

In VARTM (Vacuum Assisted Resin Transfer Molding) process, the permeability generally controls the filling time of the resin and it also affects the void characteristics of the fiber composite. In this study, carbon and glass fiber inter-layered hybrid composites (carbon fiber centered stack) with an epoxy matrix were fabricated by VARTM process and evaluated the resin flow and macro void characteristics. The permeability of glass fiber was higher than that of carbon fiber used in this study. Using Darcy's equation, the permeability of hybrid composites could be predicted and experimentally confirmed. After curing, the macro void content of hybrid composites was investigated using image analyzer. The calculated filling time was well agreed with experimental result and the void content was significantly changed in hybrid composites.

• Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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• v.18 no.1
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• pp.31-41
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• 2020

We studied the anisotropic shrinkage and deformation characteristics of large size sintered bodies in the manufacturing of glass-ceramic composite wasteform. We used uranium-bearing waste, generated from the treatment of spent uranium catalyst. Sintered specimens were prepared in several forms, comprising a circular disk, and a quarter disk in several diameters of up to 40 cm. Regardless of form or size, the sintered bodies had high isotropic shrinkage when they were fabricated using green bodies prepared at 60 MPa. The average anisotropy rate and average shrinkage rate were 1.6%, and 37.4%, respectively. We confirmed that the glass-ceramic composite wasteform in a large scale disk-type for packing in a 200 L drum could be fabricated with a tolerable anisotropy shrinkage. This has resulted in a significant reduction in the volume of radioactive waste to be disposed of with highly stable wasteform.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2007.06a
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• pp.309-309
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• 2007

The LTCCs (low-temperature co-fired ceramics) are very important for electronic industry to build smaller RF modules and to fulfill the necessity for miniaturization of devices in wireless communication industry. The dielectric materials with sintering temperature $T_{sint}$<$900^{\circ}C$ are required. In this study, we investigated with glass-ceramic composition, which was crystallized with two crystals. The microstructure, crystal phases, thermal and mechanical properties, and dielectric properties of the composites were investigated using FE-SEM, XRD, TG-DTA, 4-point bending strength test and LCR measurement. The starting temperature for densification of a sintered body was at $779{\sim}844^{\circ}C$ and the glass frits were formatted to the crystal phases, $CaAl_2Si_2O_8$(anorthite) and $CaMgSi_O_6$(diopside), at sintering temperature. The sintered bodies exhibited applicable dielectric properties, namely 6-9 for ${\varepsilon}_r$. The results suggest that the glass-ceramic composite would be potentially possible to application of low dielectric L TCC materials.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.20 no.1
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• pp.19-24
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• 2007

The effects of $B_2O_3-SiO_2-R(R;CaO,\;BaO,\;ZnO,\;Bi_2O_3)$ borosilicate glass system on the sintering behavior and microwave dielectric properties of ceramic/glass composites were investigated as functions of modifier, glass addition ($30{\sim}50\;vol%$) and sintering temperature ($500{\sim}900^{\circ}C$ for 2 hrs). The addition of 50 and 45 vol% glass ensured successful sintering below $900^{\circ}C$. Sintering characteristics of the composites were well described in terms of modifier. Borosilicate glass enhanced the reaction with $Al_{2}O_{3}$ to form pores, second phases and liquid phases, which was responsible to component of modifier. Dielectric constant (${\varepsilon}_{r},\;Q{\times}f_{o}$) and temperature coefficient of resonant frequency (${\tau}_{f}$) of the composite with 50 and 45 vol% glass contents($B_{2}O_{3}:SiO_{2}:R=25:10:65$) demonstrated A-CaBS(7.8, 2,560 GHz, -81ppm/$^{\circ}C$), A-BaBs(5.8, 3.130 GHz, -64 ppm/$^{\circ}C$), A-ZnBS(5.7, 17,800 GHz, -21 ppm/$^{\circ}C$), A-BiBs(45 vol% glass in total)(8.3, 2,700 GHz, -45 ppm/$^{\circ}C$) which is applicable to substrate requiring an low dielectric properties.