• 대한약학회:학술대회논문집
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• 대한약학회 2002년도 Proceedings of the Convention of the Pharmaceutical Society of Korea Vol.1
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• pp.140.2-140.2
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• 2002

• Journal of Mechanical Science and Technology
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• 제17권12호
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• pp.2099-2106
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• 2003

In this paper, a novel fast response NDIR analyzer (FRNDIR), which uses an electrically pulsed semiconductor emitter and dual type PbSe detector for the PPM-level detection of carbon dioxide (CO$_2$) at a wavelength of 4.28 $\mu\textrm{m}$, is described. Modulation of conventional NDIR energy typically occurs at 1 to 20 Hz. To achieve real time high-speed measurement, the new analyzer employs a semiconductor light emitter that can be modulated by electrical chopping. Updated measurements are obtained every one millisecond. The detector has two independent lead selenide (PbSe) with IR band pass filters. Both the emitter accuracy and the detector sensitivity are increased by thermoelectric cooling of up to -20 degrees C in all semiconductor devices. Here we report the use of semiconductor devices to achieve improved performance such that these devices have potential application to CO$_2$ gas measurement and, in particular, the measurement of fast response CO$_2$ concentration at millisecond level.

• 한국화재소방학회논문지
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• 제16권4호
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• pp.77-84
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• 2002

본 연구는 플라스틱재료 중 비드발포폴리스티렌폼, 압출발포폴리스티렌폼, 연질폴리우레탄폼, 경질폴리우레탄폼, 경질PVC파이프, 비닐장판, 폴리에틸렌폰(비난연), 폴리에틸렌폼(난연)를 대상으로 연소가스 독성평가를 위하여 NES 713 방법에 따라 발생되는 연소가스를 가스텍(GASTEC) 가스검지관을 이용하여 조사하였다. 연구결과 플라스틱재료의 연소시 발생되는 연소가스에 인간이 30분 동안 노출될 경우 사망에 이르는 독성지수 1 이상을 갖고 있었으며, 각 실험체의 독성지수 결과는 4.3∼179.2로 나타났으며 경질 PVC파이프가 179.2로 가장 높았다.

• 분석과학
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• 제8권4호
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• pp.895-900
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• 1995

Urinary free and acetylated polyamine profiles have been investigated for their potential usefulness as biochemical markers of cancer in a control of group comprised of healthy volunteers (32 cases) and patients with various types of cancers(48 cases). The nine (5 free and 4 acetylated) endogeneous polyamines were simultaneously determined by a sensitive capillary gas chromatography/nitrogen-phosphorus detector (GC/NPD). The newly modified (simple and convenient) method was developed and the compounds were isolated by adsorption onto silica gel and derivatized by heptafluorobutyric anhydride to enhance their specificity on gas chromatograms. The good quality-control data were obtained through the precision and accuracy test and the recovery range of them was 48.6 ~ 101.2 %. The Korean reference values of urinary polyamines were established and significant differences were found in cancer patients compared with normal subjects. Also, to eliminate subject variations, precursors to product concentration ratios were compared between cancer patients and control group. The ratios of both putrescine to spermidine and total (free plus acetylated) putrescine to total spermidine were significantly greater in cancer patients than in normal subjects.

• Journal of Electrical Engineering and Technology
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• 제13권1호
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• pp.201-210
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• 2018

This paper proposes a new start-up method for a load commutated inverter (LCI) in a large synchronous gas-turbine generator. The initial rotor position for start-up torque is detected by the proposed initial angle detector, which consists of an integrator and a phase-locked loop. The initial rotor position is accurately detected within 150ms, and the angle difference between the real position and the detected position is less than 1%. The LCI system operates in two modes (forced commutation mode and natural commutation mode) according to operating speed range. The proposed controllers include a forced commutation controller for the low-speed range, a PI speed controller and a PI current controller, where the forced commutation controller is connected to the current controller in parallel. The current controller is modeled by Matlab/Simulink, where a six-pulse delay of the thyristor and a processing delay are considered by using a zero-order hold. The performance of the proposed start-up method is evaluated in Matlab/Psim at standstill and at low speed. To verify the feasibility of the method, a 5kVA LCI system prototype is implemented, and the proposed initial angle detector and the system performance are confirmed by experimental results from standstill to 900rpm.

• 한국화재소방학회논문지
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• 제15권3호
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• pp.44-48
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• 2001

본 연구에서는, 접촉연소식 가스 탐지 소자를 대상으로 감도특성 및 전기적 특성을 분석하였으며, 24시간 동안 공기중에 노출시킨 후 온도($20^{\circ}c$, $40^{\circ}c$)와 상대습도(65%, 85%)에서 작동시켜 분석하였다. 또한 동일한 주거환경에서 210일 동안 50 cm/sec 유속을 유지하며 가스탐지소자의 동작을 실험하였다. 가스 탐지센서에 공급 전원은 기본회로에 직류 전압별(2.1V, 2.2V, 2.3V)로 인가하였다. 따라서, 상대습도와 온도에 의한 이소부탄과 메탄 특성그래프를 각각 분석한 결과 전반적으로 선형적인 증가를 보임을 확인할 수 있다.

• 센서학회지
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• 제23권5호
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• pp.342-348
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• 2014

This paper introduced a novel multi-gas sensor detector with simple signal processing algorithm. This device was evaluated by investigating the characteristics of combustible materials using fire-generated smell and smoke. Plural sensors including TGS821, TGS2442, and TGS260X were equipped to detect carbon monoxide, hydrogen gas, and gaseous air contaminants which exist in cigarette smoke, respectively. Signal processing algorithm based on the difference of response times in fire-generated gases was implemented with early and accurately fire detection from multiple gas sensing signals. All fire experiments were performed in a virtual fire chamber. The cigarette, cotton fiber, hair, polyester fiber, nylon fiber, paper, and bread were used as a combustible material. This analyzing software and sensor controlling algorithm were embedded into 8-bit micro-controller. Also the detected multiple gas sensor signals were simultaneously transferred to the personnel computer. The results showed that the air pollution detecting sensor could be used as an efficient sensor for a fire detector which showed high sensitivity in volatile organic compounds. The proposed detecting algorithm may give more information to us compared to the conventional method for determining a threshold value. A fire detecting device with a multi-sensor is likely to be a practical and commercial technology, which can be used for domestic and office environment as well as has a comparatively low cost and high efficiency compared to the conventional device.

• 한국가스학회지
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• 제15권4호
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• pp.51-55
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• 2011

본 논문에서는 써모파일을 사용한 비분산 적외선 메탄가스센서의 온도보상 알고리즘을 제시하였다. 가스측정을 위해 적외선 감지부에 내장된 써미스터의 출력전압과 분위기 온도와의 상관성을 도출하고, 협 대역통과 필터 특성과 온도 변화에 따른 센서모듈(광 공동과 적외선램프)의 출력전압 특성 및 메탄가스의 흡수계수와 광 경로에 따른 출력특성 해석을 통하여 가스센서 모듈의 온도보상 알고리즘을 도출하였다.온도보상 전 약 $\pm$ 1,500 ppm 이상의 오차를 갖는 센서는 온도보상 알고리즘을 적용함으로써 $20^{\circ}C$온도변화 구간에서 최대 약 180 ppm 이하의 정밀한 센서모듈을 제작하였다.

• 한국산업보건학회지
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• 제1권1호
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• pp.16-28
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• 1991

A study on comparison of standard charcoal tube method, infrared gas analyzer, and detector tube method were conducted. Measurements were performed simultaneously at same sampling points in an air chamber containing benzene, toluene and xylene vapors. Charcoal tube samles were collected at sampling flowrates of 0.05, 0.2, 0.5, and 1.0 1pm. Results are as follows : 1. Coefficients of variation of results with charcoal tube method for bezene, toluene and xylene mixture vapor were 14.34 % in benzene(0.28-11.12 ppm), 9.20 % in toluene (2.68-135.09 ppm) and 10.21 % in xylene (2.56-82.64 ppm), respectively. 2. Results of infrared gas analyzer in mixture air were non-specific on benzene and toluene. Ratio of results of infrared gas analyzer to those of charcoal tube on benzene, toluene and xylene were 696.4 %, 30.3 % and 36.6 %, respectively. 3. Ratio of responses of detector tubes to those of charcoal tube were 49.4 % in benzene, 22.1 % in toluene and 223.9 % in xylene. Xylene detector tube were interfered by toluene greately. 4. Collection efficiencies of charcoal tubes at low concentraton(benzene : 1 ppm, toluene : 10 ppm, xylene : 10 ppm) were stable on various flowrate from 0.05 to 1.0 1pm, but at high concentrations the efficiency decreased at high flowrate above 0.5 1pm. 5. Within the saturation capacity of charcoal, collection effiency decreased at 0.5-1.0 1pm. Smpling feowrates of 0.05-0.20 1pm were appropriate for sampling organic vapors.

• Journal of Pharmaceutical Investigation
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• 제35권5호
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• pp.383-388
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• 2005

A simple and specific method for determination of methyltestosterone (MT) has been established by a gas chromatography/mass selective detector and applied in plasma of healthy male volunteers received a single oral dose of 50 mg MT $(Testo^{TM}\;tablets,\;25\;mg)$ for bioavailability test. This method involves using liquid-liquid extraction of the sample with diethyl ether and derivatization with MSTFA. MT showed good resolution in this condition. The detection limit of quantitation was 5 ng/ml. A good linearity (r>0.996) was obtained at the range of 5-250 ng/ml of MT. Intra-day precision and accuracy were 2.76-12.56% and 0.39-8.01 %, and inter-day precision and accuracy were 2.29-17.69% and 0.42-7.99%, respectively. The established method was applied on bioavailability test of MT in human volunteers. The value of $AUC_{0\;to\;last}$ to last was $264.5{\pm}123.9\;ng{\cdot}hr/ml$ and that of $AUC_{0\;to\;inf}$ was determined to be $275.2{\pm}126.5\;ng{\cdot}hr/ml$. The values of $C_{max}$ and $T_{max}$ were $95.9{\pm}67.1\;ng/ml$ and $1.13{\pm}0.9\;hr$, respectively. The mean elimination half-life $(t_{1/2})$ was $4.4{\pm}0.9\;hr$. This analytical method is suitable and useful for the pharmacokinetics and bioequivalence studies of MT.