• 제목/요약/키워드: GLASS

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Measurement of Adhesion Strength and Nanoindentation of Metal Interconnections of Al/Ni and TiW/Ni Layers Formed on Glass Substrate (유리기판 위에 형성된 Al/Ni 및 TiW/Ni 다층 금속배선막의 계면 접합력 및 나노압입특성 평가)

  • Joe, Chul Min;Kim, Jae Ho;Hwang, So Ri;Yun, Yeo Hyeon;Oh, Yong Jun
    • Korean Journal of Metals and Materials
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    • v.48 no.12
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    • pp.1116-1122
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    • 2010
  • Metal interconnections of multilayer Al/Ni and TiW/seed-Ni/Ni were formed on glass, and the adhesion strength and nanoindentation response of the composite layers were evaluated. The Al/Ni multilayer was formed by an anodic bonding of glass to Al and subsequent electroless plating of Ni, while the TiW/Ni multilayer was fabricated by sputter deposition of TiW and seed-Ni onto glass and electroless plating of Ni. Because of the diffusion of aluminum into glass during the anodic bonding, anodically bonded glass/Al joint exhibited greater interfacial strength than the sputtered glass/TiW one. The Al/Ni on glass also showed excellent resistance against delamination by bending deformation compared to the TiW/seed-Ni/Ni on glass. From the nanoindentation experiment of each metal layer on glass, it was found that the aluminum layer had extremely low hardness and elastic modulus similar to the glass substrate and played a beneficial role in the delamination resistance by lessening stress intensification at the joint. The indentation data of the multilayers also supported superior joint reliability of the Al/Ni to glass compared to that of the TiW/seed-Ni/Ni to glass.

Chemical Compositions and Lead Isotope Ratios of Some Glass Beads from Seokga-tap, Gyeongju

  • Kang, Hyung-Tae;Yun, Eun-Young
    • Conservation and Restoration of Cultural Heritage
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    • v.1 no.1
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    • pp.3-8
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    • 2012
  • Chemical compositions and lead isotope ratios for four glass bead samples of Seokga-tap were analyzed and the results were organized. Among 4 glass beads found in the Seokga-tap, 3 pieces were lead glass. Manufacturing method was to firstly grind pebbles finely and mix lead ore to be melt at $740{\sim}760^{\circ}C$. The mixed ratio of silica and lead was 3:7. Moreover, The evaluation on the lead isotope ratio indicated that two lead glass pieces used lead ore from northern Korea. One piece has the direction of southern Korea lead ore, but it requires a further review. One glass bead of Seokga-tap was brown and it was potash lead glass ($K_2O-PbO-SiO_2$) System. The mixed ratio was approximately 50:10:40 for silica, natural saltpeter, and lead, respectively. Lead isotope ratio data fell within the lead ore from northern China. Therefore, it was concluded that potash lead glass found in the Seokga-tap was produced in northern area of China at the end of $10^{th}$ century and transferred to the Seokga-tap.

Preparation of Glass-Ceramic by Recycling of Various Slags and Its Properties (다종슬래그를 재활용한 Glass-Ceramic의 제조 및 물성)

  • Lee, Duk-Hee;Shin, Dongyoon;Yoon, Mijung;Park, Hyun Seo;Yoon, Jin-Ho
    • Korean Journal of Materials Research
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    • v.26 no.5
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    • pp.266-270
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    • 2016
  • Glass-ceramics were developed many years ago and have been applied in many fields such as electronics, chemistry, optics, etc. Much is already known about glass-ceramic technology, but many challenges in glass-ceramic research are still unresolved. Recently, large amounts of slag have steadily increased in the steel industry as by-products. To promote recycling of industrial waste, including steel industry slags, many studies have been performed on the fabrication of basalt-based high-strength glass-ceramics. In this study, we have fabricated such ceramics using various slags to replace high performance cast-basalt, which is currently imported. Glass-ceramic material was prepared in similar chemical compositions with commercial cast-basalt through a pyro process using slags and power plant by-product (Fe-Ni slag, converter slag, dephosphorization slag, Fly ash). The properties of the glass-ceramic material were characterized using DTA, XRD, and FE-SEM; measurements of compressive strength, Vicker's hardness, and abrasion were carefully performed. It is found that the prepared glass-ceramic material showed better performance than that of commercial cast-basalt.

COMPUTATIONAL ANALYSIS ON THE COOLING PERFORMANCE OF GLASS FIBER COOLING UNIT WITH HELIUM GAS INJECTION (헬륨가스 주입식 유리섬유 냉각장치의 냉각성능 해석)

  • Oh, I.S.;Kim, D.;Umarov, A.;Kwak, H.S.;Kim, K.
    • Journal of computational fluids engineering
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    • v.16 no.4
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    • pp.110-115
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    • 2011
  • A modern optical fiber manufacturing process requires the sufficient cooling of glass fibers freshly drawn from the heated and softened silica preform in the furnace, since the inadequately cooled glass fibers are known to cause improper polymer resin coating on the fiber surface and to adversely affect the product quality of optical fibers. In order to greatly enhance the fiber cooling effectiveness at increasingly high fiber drawing speed, it is necessary to use a dedicated glass fiber cooling unit with helium gas injection between glass fiber drawing and coating processes. The present numerical study features a series of three-dimensional flow and heat transfer computations on the cooling gas and the fast moving glass fiber to analyze the cooling performance of glass fiber cooling unit, in which the helium is supplied through the discretely located rectangular injection holes. The air entrainment into the cooling unit at the fiber inlet is also included in the computational model and it is found to be critical in determining the helium purity in the cooling gas and the cooling effectiveness on glass fiber. The effects of fiber drawing speed and helium injection rate on the helium purity decrease by air entrainment and the glass fiber cooling are also investigated and discussed.

Buildup Characteristics of Radiophotoluminescent Glass Dosimeters with Exposure Time of X-ray (엑스선의 조사시간에 따른 형광유리선량계의 빌드업 특성)

  • Kweon, Dae Cheol
    • Journal of Biomedical Engineering Research
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    • v.38 no.5
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    • pp.256-263
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    • 2017
  • By using the buildup characteristics of the radiophotoluminescence glass dosimeter(RPLGD), it is aimed to help the measurement of the accurate dose by measuring the radiation dose according to the time of the glass element. Five glass elements were arranged on the table and the source to image receptor distance(SID) was set to 100 cm for the build-up radiation dose measurement of the fluorescent glass dosimeter glass element(GD-352M). Radiation doses and saturation rates were measured over time according to irradiation time, with the tube voltage (30, 60, 90 kVp) and tube current (50, 100 mAs) Repeatability test was repeated ten times to measure the coefficient of variation. The radiation dose increased from 0.182 mGy to 12.902 mGy and the saturation rate increased from 58.3% with increasing exposure condition and time. The coefficient of variation of the glass elements of the fluorescent glass dosimeter was ranged from 0.2 to 0.77 according to the X - ray exposure conditions. X - ray exposure showed that the radiation dose and saturation rate were increased with buildup characteristics, and degeneration of glass elements was not observed. The reproducibility of the variation coefficient of the radiation generator was included within the error range and the reproducibility of the radiation dose was excellent.

The scientific analysis of glass beads excavated from Naesanri in Gosung (고대 유리구슬의 재질분석 연구-고성 내산리 출토 유리구슬을 중심으로)

  • Moon, Whan-Suk;Hwang, Jin-Ju;Cho, Nam-Chul;Hong, Jong-Ouk
    • 보존과학연구
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    • s.21
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    • pp.57-75
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    • 2000
  • We performed the scientific analysis through composition analysis, micro-structure investigation, melting point and hardness test to the glass beads excavated at Naesanri in Gosung. Through this investigation, we could examine closely the characterization of raw materials and manufacture technique As a result of micro-structure investigation of glass beads, it appeared that the bubbles in glass beads have remained. Coloring agents of yellow glass bead was remained to the shape of inclusion. And on observing the transparent solid particle, we can know that these do not melt the raw materials because of low melting temperature of a crucible. The result of composition analysis of all glass beads using ICP, these were classified as $Na_2O_2$-$SiO_2$ type of glass. Also, these added to $AI_2O_3$ to improve the durability. The value of Vickers hardness of glass beads appeared the HV 490-530. The HV 1,440 of the transparent solid particle was much more than that of inner glass bead. This means that raw materials do not melt because of a low melting temperature of a crucible. The result of melting temperature analysis of glass beads using DSC/TGA, it was measured about $1,250^{\circ}C$.

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Numerical and Experimental Investigation of the Heating Process of Glass Thermal Slumping

  • Zhao, Dachun;Liu, Peng;He, Lingping;Chen, Bo
    • Journal of the Optical Society of Korea
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    • v.20 no.2
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    • pp.314-320
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    • 2016
  • The glass thermal forming process provides a high volume, low cost approach to producing aspherical reflectors for x-ray optics. Thin glass sheets are shaped into mirror segments by replicating the mold shape at high temperature. Heating parameters in the glass thermal slumping process are crucial to improve surface quality of the formed glass. In this research, the heating process of a thermal slumping glass sheet on a concave parabolic mold was simulated with the finite-element method (FEM) to investigate the effects of heating rate and soaking temperature. Based on the optimized heating conditions, glass samples 0.5 mm thick were formed in a furnace with a steel concave parabolic mold. The figure errors of the formed glass were measured and discussed in detail. It was found that the formed glass was not fully slumped at the edges, and should be trimmed to achieve better surface deviation. The root-mean-square (RMS) deviation and peak-valley (PV) deviation between formed glass and mold along the axial direction were 2.3 μm and 4.7 μm respectively.

Influence of Different Methods of Cutting Ampules on Drug Contamination by Glass Flakes from the Ampule (유리앰플 주사제 개봉방법이 유리조각 혼입 및 약물오염에 미치는 영향)

  • Jeong, Hyeon-Cheol;Jeon, Mi-Yang
    • Journal of Korean Academy of Fundamentals of Nursing
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    • v.16 no.2
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    • pp.207-213
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    • 2009
  • Purpose: This study was done to examine how medication contamination in a single-dose glass ampule is affected by minute glass flakes generated in different methods of cutting the ampule. Method: Sixty medication-containing glass ampules were randomly assigned to two groups. The number of glass flakes, resulting from two different cutting methods (with cotton and without cotton), were counted under the microscope. Contamination was evaluated by extracted the medication with a syringe and culturing it in E. coli, coliform, and aerobic bacteria culture media. Result: Fewer glass flakes were found in the ampules when the ampule was cut with cotton. The use of cotton, however, did not significantly change the degree of drug contamination. Conclusion: Although minute glass flakes generated in the ampule cutting operation did not significantly contaminate the medication and the use of cotton decreased the number of glass flakes in the ampules, glass flakes injected into the blood and tissues of the patient remain a risk factor. Therefore, pre-filled syringes or syringes with filters would be alternative methods and safeguards against the possible injection of glass flakes generated while cutting the ampule.

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Characteristics of 1.9 GHz On-Glass Antenna for Automobil Telephone (차량전화용 1.9 GHz On-Glass 안테나의 특성)

  • 김태원;이원용;김정기
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.7 no.3
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    • pp.211-218
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    • 1996
  • Theorectical and experimental studies of On-Glass antenna in the 1.9GHz bandare performed. In this paper, the structure of designed On-Glass antenna consists of a 5/8-wavelength upper segment and quarter-wavelength lower segment separated by phasing coil. On-Glass antenna may be resonated by the use of suitably spaced phasing coil in series with the antenna wire. This tuning structure leads to an improvement in antenna efficiency. And then, this can be very useful for installation where limited space like automobil is available. The analytical method is based on collocation method with pulse function. The results obtained from numerical method are presented and compared with an experimental evaluation. From this, the VSWR, gain, radiation pattern, and bandwidth of the On-Glass antenna are analyzed.

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Study on Optimization for Heating System of Sequential Feed-Type Mobile Smart Device Cover Glass Molding Machine (모바일 스마트 기기 덮개 유리 순차이송형 성형기기의 가열시스템 최적화에 관한 연구)

  • Lee, Jun Kyoung
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.14 no.5
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    • pp.75-80
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    • 2015
  • Nowadays, flat-shaped cover glass is widely used for mobile devices. However, for its good design and convenience of use, curved cover glass has been demanded. Thus, many companies have tried to produce curved cover glass through the shaving technique, but the production efficiency is very low. Therefore, the molding technique has been adopted to increase the efficiency for the curved-glass production system. For a glass-molding system, several heating blocks are installed, and the flat cover glass is sequentially heated and molded. The production time for the cover glass is very different depending on the heating conditions; thus, the prediction of the production time for different heating conditions should be needed. Therefore, in this study, the computations were performed with different heating conditions (uniform and non-uniform) in the present cover glass-molding machine. For uniform and non-uniform heating conditions, the simple correlation between the heating time and the heater capacity and the heating time to achieve higher durability can be suggested, respectively.