• Title/Summary/Keyword: Fusion temperature

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THE EFFECTS OF TiN PARTICLES ON THE HAZ MICROSTRUCTURE AND TOUGHNESS IN HIGH NITROGEN TiN STEEL

  • Jeong, Hong-Chul;An, Young-Ho;Choo, Wung-Yong
    • Proceedings of the KWS Conference
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    • 2002.10a
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    • pp.217-221
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    • 2002
  • In the coarse grain HAZ adjacent to the fusion line, most of the TiN particles in conventional Ti added steel are dissolved and austenite grain growth is easily occupied during welding process. To avoid this difficulty, thermal stability of TiN particle is improved by increasing the nitrogen content in steel. In this study, the effect of high nitrogen TiN particle on preventing austenite grain growth in HAZ was investigated. Increased thermal stability of TiN particle is helpful for preventing the austenite grain growth by pinning effect. High nitrogen TiN particle in simulated HAZ were not dissolved even at high temperature such as 1400 C and prevented the austenite grain growth in simulated HAZ. Owing to small austenite grain size in HAZ the width of coarse grain HAZ in high nitrogen TiN steel was decreased to 1/10 of conventional TiN steel. Even high heat input welding, the microstructure of coarse grain HAZ consisted of fine polygonal ferrite and pearlite and toughness of coarse grain HAZ was significantly improved.

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Adsorption of SO2 by Zeolite Synthesized from Coal Fly Ash (석탄비산재로부터 합성한 제올라이트의 SO2 흡착특성)

  • Kim, Seong-Soo;Lee, Chang-Han
    • Journal of Environmental Science International
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    • v.21 no.6
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    • pp.687-694
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    • 2012
  • Zeolite 4A was synthesized by fusion method from coal fly ash discharged at the thermal power plants. The synthesized zeolite(FAZ) was characterized through particle size analyzer, XRD, XRF and SEM. $N_2$ adsorption-desorption measurement was used to examine surface and pore structures. The adsorption experiments were carried out under dynamic conditions of trace $SO_2$ in $N_2$ to investigate $SO_2$ adsorption capacity of FAZ. The experiments were conducted to characterize the breakthrough characteristics of $SO_2$ in a fixed bed under different operating conditions including temperature(50-$125^{\circ}C$), concentration of $SO_2$(3000-10000 ppm) and FAZ with 4 kinds of commercial zeolite. The adsorption capacity of FAZ was 53.84 $mgSO_2/g$ adsorbent, larger than that of the same type commercial zeolite(WK4A).

Adsorption Kinetic and Isotherm Characteristics of Mn Ions with Zeolitic Materials Synthesized from Industrial Solid Waste (산업폐기물로부터 합성된 제올라이트 물질의 망간 이온 흡착속도 및 등온흡착 특성)

  • Choi, Jeong-Hak;Lee, Chang-Han
    • Journal of Environmental Science International
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    • v.29 no.8
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    • pp.827-835
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    • 2020
  • Zeolite material having XRD peaks of Na-A zeolite in the 2θ range of 7.18 to 34.18 can be synthesized from the waste catalyst using a fusion/hydrothermal method. The adsorption rate of Mn ions by a commercial Na-A zeolite and the synthesized zeolitic material increased as the adsorption temperature increased in the range of 10 ~ 40℃. The adsorption of Mn ion were very rapid in the first 30 min and then reached to the equilibrium state after approximately 60 min. The adsorption kinetics of Mn ions by the commercial Na-A zeolite and the zeolitic material were found to be well fitted to the pseudo-2nd order kinetic model. Equilibrium data by the commercial Na-A zeolite and the zeolitic material fit the Langmuir, Koble-Corrigan, and Redlich-Peterson isotherm models well rather than Freundlich isotherm model. The removal capacity of the Mn ions by the commercial Na-A zeolite and the zeolitic material obtained from the Langmuir model was 135.2 mg/g and 128.9 mg/g at 30℃, respectively. The adsorption capacity of Mn ions by the synthesized zeolitic material was almost similar to that of commercial Na-A zeolite. The synthesized zeolitic material could be applied as an economically feasible commercial adsorbent.

THE ATMOSPHERE PARAMETERS AND THE LINE PROFILE VARIATIONS OF ρ PUPPIS

  • Yushchenko, A.V.;Dorokhova, T.N.;Gopka, V.F.;Kim, Chul-Hee;Lee, B.C.;Yushchenko, V.A.;Doikov, D.N.
    • Journal of The Korean Astronomical Society
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    • v.43 no.3
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    • pp.65-74
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    • 2010
  • We investigate ${\rho}$ Pup using the high resolution spectral observations taken from the VLT archive and observations at a 1.8m-Korean telescope with BOES spectrograph. The atmospheric parameters are determined using the iron-line abundance analysis. We derive an effective temperature value of $T_{eff}=6890{\pm}250K$, surface gravity of log g=$3.28{\pm}0.3$ dex, microturbulent velocity of ${\upsilon}_{micro}=4.1{\pm}0.4km\;s^{-1}$, and the iron abundance of log N=$7.82{\pm}0.15$. The projected rotational velocity of the star is close to ${\upsilon}$ sin i=3.5km $s^{-1}$. Asymmetric line profiles in the observed spectra and variation of this asymmetry with time show that both strong radial pulsation and weak non-radial pulsations are present in ${\rho}$ Pup.

A study to reduce measurement errors of an ultrasonic rangefinder (초음파 거리 센서의 계측오차 감소를 위한 연구)

  • 도용태;김태호;유석환
    • Journal of the Korean Institute of Telematics and Electronics S
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    • v.34S no.11
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    • pp.43-52
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    • 1997
  • Ultrasonic sensors are widely employed in detecting range to a target by the virtue of their low cost and simplicity. However, the sensor's measurements are corrupted by systematic errors due mainly to the dependency of sound speed upon surrounding conditions and random errors of uncertain origin. In this paper, we present the results of research carried out to reduce these errors for increasing the reliability of an untrasonic sensor system to be used in orbotic or other automated system's range finding. The sensor system designed herein is in a peuliar structure having a reference target and two receivers. Echoes from a small reference target placed at a known distance are used for compensating the variations of sound speed according to the changes of sensing conditions. Unlike existing ones, the technique proposed can compensate the effects of temperature or any other physical parameters without an additional sensor dedicated to the compensation. The measurements by two redundantly employed receivers are fused to reduce random errors in a statistical sense. The correlation of the signals from the receivers sharing a hardware in part is considered in the fusion process. The methodology desicribed in this paepr is conceptually simple, easy to be implemented, and effetive to increase the accuracy of the sensor measurements as experimental results confirm.

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Characterization of HEK293 and Namalwa Cell Cultures by Using Design of Experiment (실험계획법을 이용한 HEK293 및 Namalwa 세포배양 특성 규명)

  • Kang, Kyung-Ho;Seo, Joon-Serk;Kim, Dong-Il
    • KSBB Journal
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    • v.27 no.3
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    • pp.186-194
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    • 2012
  • Various human host cell lines, which are more effective than the other original human cell lines, have been developed and used. Highly efficient human cell line can be obtained from the fusion between human embryonic kidney 293 (HEK293) and human Burkitt's lymphoma cells (Namalwa). Fused cell line has the advantages of both cell lines such as the high transfection efficacy of HEK293 cells and the constitutive expression of Epstein-Barr virus (EBV) genome which is related with high expression of target protein and anti-apoptotic growth of Namalwa cells. In this study, characterization of two original cell lines was performed by using design of experiment (DOE) considering cell maintenance, media development, optimization of culture condition, and scale-up. The formation of aggregates was apparent with high glutamine concentration at more than 6 mM. Supplementation of hydrolysates showed positive effects on the growth performances of HEK293 cells. On the contrary, Namalwa cells showed negative results. It was confirmed that Namalwa cells were more sensitive to lower temperature at $35^{\circ}C$ and hyperosmotic condition over 260 mOsm/kg. In addition, both cell lines showed limited growth in 3-L bioreactor due to shear stress.

Dependence Analysis of Radical and Ion Densities on Plasma Parameters in $Cl_2$/Ar Discharges ($Cl_2$/Ar 방전에서의 플라즈마 변수에 대한 이온과 라디칼 밀도 의존성 분석)

  • An, Choong-Gi;Kwon, Deuk-Chul;Yu, Sin-Jae;Kim, Jeong-Hyeong;Yoon, Nam-Sik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.103-103
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    • 2010
  • Dependence of radical and ion densities on Plasma Parameters is theoretically investigated in $Cl_2$/Ar plasma discharges. Firstly, a set of reliable rate coefficients is obtained by direct calculations with cross section data set and by comparing them with previously reported values. Then, some global discharge simulations are performed for ICP(inductively coupled plasma) discharges and the results are compared with experimental results. Finally, the validated data set is used to analyze the dependence of radical and ion densities, which are usually not easy to be measured, on electron density arid temperature.

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Synthesis of Cobalt Phosphates and their Catalytic Properties of the Hydrogen Generation from the Hydrolysis of NaBH4 (비결정질 코발트 인산염 합성 및 NaBH4 가수분해를 통한 수소발생 촉매 활성 연구)

  • Kim, Youngyong;Park, Joon Bum;Kwon, Ki-Young
    • Applied Chemistry for Engineering
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    • v.26 no.6
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    • pp.743-745
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    • 2015
  • Amorphous cobalt phosphates were synthesized with their distinct morphology by controlling the amount of base in the synthetic condition. The crystallinity and morphology of cobalt phosphates were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The prepared cobalt phosphates were applied as a heterogeneous catalyst for generating hydrogen gas from the hydrolysis reaction of sodium borohydride. We found that the catalyst prepared using the least amount of base condition at room temperature showed a plate shape with less than 10 nm thickness, which resulted in the best catalytic activity among all catalysts due to the large surface area.

Study of Metal(Au) Bump for Transverse Ultrasonic Bonding (금속(Au)범프의 횡초음파 접합 조건 연구)

  • Ji, Myeong-Gu;Song, Chun-Sam;Kim, Joo-Hyun;Kim, Jong-Hyeong
    • Journal of Welding and Joining
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    • v.29 no.1
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    • pp.52-58
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    • 2011
  • In this paper, the direct bonding process between FPCB and HPCB was studied. By using an ultrasonic horn which is mounted on the ultrasonic bonding machine, it is alternatively possible to bond the gold pads attached on the FPCB and HPCB at room temperature without an adhesive like ACA or NCA. The process condition for obtaining more bonding strength than 0.6 Kgf, which is commercially required, was carried out as 40 kHz of frequency, 0.6 MPa of bonding pressure and 2 second of bonding time. The peel off test was performed for evaluating bonding strength which results in more than 0.8 Kgf.

Evaluation of the Performance of Water Electrolysis Cells and Stacks for High-Altitude Long Endurance Unmanned Aerial Vehicle (고고도 무인기용 수전해 셀 및 스택의 제작 및 성능 평가)

  • JUNG, HYE YOUNG;LEE, JUNYOUNG;YOON, DAEJIN;HAN, CHANGHYUN;SONG, MINAH;LIM, SUHYUN;MOON, SANGBONG
    • Transactions of the Korean hydrogen and new energy society
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    • v.27 no.4
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    • pp.341-348
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    • 2016
  • The experiments related on structure and water electrolysis performance of HALE UAV stack were conducted in this study. Anode catalyst $IrRuO_2$ was prepared by Adam's fusion methods as 2~3 nm nano sized particles, and the cathode catalyst was used as commercial product of Premetek. The MEA (membrane electrode assembly) was manufactured by decal methods, anode and anode catalytic layers were prepared by electro-spray. HALE stack was composed of 5 multi-cells as $0.2Nm^3/hr$ hydrogen production rate with hydrogen pressure as 10 bar. The water electrolysis performance was investigated at atmospheric pressure and temperature of $55^{\circ}C$. Best performance of HALE UAV stack was recorded as cell voltage efficiency as 86%.