• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2013년도 춘계학술대회 논문집
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• pp.835-841
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• 2013

Modern solid-state gyroscopes (HRG) with hemispherical resonators from high-purity quartz glass and special surface superfinishing and ultrathin gold coating become the best instruments for precise-grade inertial reference units (IRU) targeting long-term space missions. Designing of these sensors could be a notable contribution into development of Korea as a space nation. In participial, 40mm diameter thin-shell resonator from high-purity fused quartz, fabricated as a single-piece with its supporting stem has been designed, machined, etched, tuned, tested, and delivered by STM Co. (ATS of Ukraine) several years ago; an extremely-high Q-factor (upto 10~20 millions) has been shown. Understanding of the best way how to match such a unique sensor with inner glass assembly of the gyro means how to use the high potential in a maximal extent; and this has become the urgent task. Inner quartz glass assembly has a very thin indium (In) layer soldered the resonator and its silica base (case), but effects of internal resonances between operational modal pair of the shell-cup and its side (parasitic) modes can notable degrade the potential of the sensor as a whole, instead of so low level of resonator's intrinsic losses. Unfortunately, there are special combinations of dimensions of the parts (so-called, "resonant sizes"), when intensive losses of energy occurs. The authors proposed to use the length of stem's fixture as an additional design parameter to avoid such cases. So-called, a cyclic scheme of finite element method (FEM) and ANSYS software were employed to estimate different combinations of gyro assembly parameters. This variant has no mismatches of numerical origin due to FEM's discrete mesh. The optimum length and dangerous "resonant lengths" have been found. The special attention has been paid to analyses of 3D effects in a cup-stem transient zone, including determination of a difference between the positions of geometrical Pole of the resonant hemisphere and of its "dynamical Pole", i.e., its real zone of oscillation node. Boundary effects between the shell (cup) and 3D short "beams" (inner and outer stems) have been ranged. The results of the numerical experiments have been compared with the classic model of a quasi-hemispherical shell band with inextensional midsurface, and the solution using Rayleigh's functions of the $1^{st}$ and $2^{nd}$ kinds. To guarantee the truth of the recommended sizes to a designer of the real device, the analytical and FEM results have been compared with experimental data for a party of real resonators. The consistency of the results obtained by different means has been shown with errors less than 5%. The results notably differ from the data published earlier by different researchers.

• 대한화학회지
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• 제47권6호
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• pp.619-624
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• 2003

졸겔법을 사용하여 $Gd_{1.9-x}Li_{0.1}Eu_xO_3$(x=0.02, 0.05, 0.08, 0.12) 형광체 분말을 합성하였다. 형광체 입자의 표면을 나노 크기의 $SiO_2$(입자크기${\thickapprox}30 nm$)로 코팅한 후 스핀-코팅법으로 유리 기판에 형광체 막을 제작하였다. 유리의 연화온도인 $700^{\circ}C$ 부근에서 융착 되는 $SiO_2$ 나노 입자들에 의해 $Gd_{1.9-x}Li_{0.1}Eu_xO_3$ 입자들은 유리 기판 표면 위에 강하게 융착 되었다(>9H, 연필 경도계). 본 연구에서 채택한, 형광체 막을 제조하는 간단하고 비용이 저렴한 이 방법은 디스플레이장치의 응용 분야에 적용될 수 있을 것으로 생각한다.

• 한국생산제조학회지
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• 제21권5호
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• pp.767-772
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• 2012

Generally, abrasive fluid jet polishing system has been used for polishing of complex shape or freeform surface which has steep local slopes. In the system, abrasive fluid jet is injected through a nozzle at high pressure; however, it is inevitable to lose its coherence as the jet exits a nozzle. This problem causes incorrect polishing results because of unstable and unpredictable workpiece material removal at the impact zone. In order to solve this problem, MR fluid jet polishing method has been developed using a mixture of abrasive and MR fluid which can maintain highly collimated and coherent jet by applied magnetic field. Thus, in this study, an injection nozzle and an electromagnetic module, most important parts in the MR polishing system, were designed and verified by magnetic field and flow analysis. As the results of experiments, it can be confirmed that stable fluid jets for polishing were generated since smooth W-shapes and uniform spot size were observed regardless of standoff distance changes.

• 한국정밀공학회지
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• 제27권3호
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• pp.18-26
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• 2010

Diffraction gratings with precise spatial periods of 2 ${\mu}m$ and 5 ${\mu}m$ have been fabricated by using a femtosecond laser which does not have limits on materials of micromachining and small thermal effects due to high peak power. Diffraction angle and diffraction efficiency of those were measured. Simulation results of diffraction angle and diffraction efficiency of the diffraction grating calculated with the parameters such as line width, depth, and spatial period of the fabricated gratings were compared with experimental results measured with a He-Ne laser. Besides these, Fresnel Zone Plates (FZPs) with focal distances of 50 mm and 25 mm were fabricated and focal distances of fabricated FZP were measured. Those experimental results for diffraction gratings and FZPs match well with experimental results.

• 반도체디스플레이기술학회지
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• 제9권2호
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• pp.33-39
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• 2010

The moisture absorption properties such as diffusion coefficient and moisture content ratio of liquid type epoxy resin systems with the filler were investigated. Bisphenol A type and Bisphenol F type epoxy resin, Kayahard MCD as hardener and 2-methylimidazole as catalyst were used in these epoxy resin systems. The nano-sized spherical type fused silica as filler were used in order to study the moisture absorption properties of these liquid type epoxy encapsulant according to the change of filler size. The temperature of glass transition (Tg) of these epoxy resin systems was measured using Dynamic Scanning Calorimeter (DSC), and the moisture absorption properties of these epoxy resin systems according to the change of time were observed at $85^{\circ}C$ and 85% relative humidity condition using a thermo-hygrostat. The diffusion coefficients in these systems were calculated in terms of modified Crank equation based on Ficks' law. An increase of Tg and diffusion coefficient with filler size in these systems can be observed, which are attributed to the increase of free volume with Tg. The change of maximum moisture absorption ratio according to the filler size and filler content cannot be observed; however, the diffusion coefficients of these systems decreased with filler content. The diffusion via free volume is dominant in the epoxy resin systems with low nano-sized filler content; however, the diffusion with the interaction of absorption according the increase of the filler surface area is dominant in the liquid type epoxy encapsulant with high nano-sized filler content.

• 한국결정성장학회지
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• 제25권5호
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• pp.218-224
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• 2015

최근 세라믹 다공체를 이용하여 적조 생물을 여과, 제거하려는 연구가 시도되고 있다. 하지만 해양 환경에서 1개월 이상이 경과하면 다공체 표면에 해양 생물 오손(biofouling)이 발생하여 기능이 저하되는 문제가 나타난다. 본 논문에서는 세라믹 다공체의 특성 변화 또는 표면 개질을 통하여 해양 생물 오손을 억제하는 방법에 대하여 연구하였다. 6 종류의 세라믹 다공체를 시험한 결과, 기공율과 흡수율이 낮을수록 생물 오손량이 낮게 나타났다. 또한 다공체 표면에 실리카 입자를 결합시켜 표면 거칠기를 증가시키면, 따개비 등의 대형 해양 생물로 인한 오손량을 감소시킬 수 있었다. 한편 세라믹 다공체 표면에 유리분말을 융착 코팅시키면 오히려 생물 오손량이 증가하였는데, 이는 유리에서 용출되어 나오는 무기질 성분 이온들이 미생물의 생육을 촉진했기 때문이다. 본 연구로부터 세라믹 다공체의 물리적 성질 및 표면 거칠기를 제어하면 위험 물질을 사용하지 않고도 친환경적으로 해양 생물 오손량을 줄일 수 있음을 확인하였으며, 따라서 본 결과를 향후 해양 구조물 등에 적용할 수 있을 것으로 기대된다.

• Applied Biological Chemistry
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• 제35권1호
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• pp.36-41
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• 1992

면실유, 옥배유 및 채종유의 산패도를 신속하고 재현성 있게 측정하고자 $60^{\circ}C$ 및 $70^{\circ}C$로 저장한 식용유의 pentanal과 hexanal을 headspace 가스크로마토그라피 방법으로 분석하였고, 그 결과를 관능검사 결과와 상관분석을 실시하였다. Headspace 가스크로마토그라피 방법에서 휘발성 산화생성물의 포집 및 용출은 cold trap-thermal desorption 방법으로 실시하였으며, GC 주입부에 들어가는 splitless mode glass liner insert에 Tenax GC를 충전하여 사용하였다. 23종의 휘발성 산화생성물이 gas chromatography 및 gas chromatography-mass spectrometry에 의하여 검출되었으며, 저장 기간에 따른 pentanal과 hexanal 함량 변화와 관능검사에 의한 산패취 측정 결과의 상관분석을 실시한 결과, pentana(PE), hexanal(HE) 및 log{PE) log(HE) $log(PE){\times}log(HE)$의 세 가지를 변수로 한 회귀식의 상관계수의 값이 각각 0.831, 0.866 및 0.896으로 다같이 높을 값을 보였다. 따라서 headspace 가스크로마토그라피를 이용하여 면실유, 옥배유 및 채종유의 휘발성 산화생성물 중 pentanal과 hexanal을 분석하면 각각의 식용유의 산패도를 객관적으로 평가할 수 있음을 알 수 있었다.

• 천문학회보
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• 제36권2호
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• pp.156-156
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• 2011

VPH (Volume Phase Hologram) grating is one of the transmission gratings and is known as its remarkable efficiency (>90%). It has two different densities of gelatins causing interference patterns. The VPH grating is favored in many astronomical instruments these days and also IGRINS, which is up coming near infrared high-resolution spectroscope expected to see the first light next year, uses the VPH grating as its cross-disperser. The infrared astronomical instruments operate at cryogenic temperature (~100K) in order to cut down thermal noise and the optical components of IGIRNS will be operated at 130K. The VPH grating is sandwiched in between fused silica or glass and glued together using optical adhesive. IGRINS is expected to go through 50 times of thermal cycling in 10 years including the performance test and this research is to check whether the physical characteristic such as the adhesion or dichromatic gelatin does not break and change from the several cryogenic thermal cycling. The two identical test gratings provided from Kaiser Optical System, Inc. are used in this test. One VPH grating is cooled down to 100K for 2 hours with maximum dT/dt = 5 and warmed up to the room temperature and another grating is kept stored in the room temperature and used as a control sample. In order to check the change, we inspected the grating with eyes and checked its efficiency and transmission at the room temperature every 10 cycling. From the 40 times of cryogenic temperature cool down cycling, the VPH grating showed no signs of change within the error compared to the control sample. We concluded the VPH grating is durable through several cryogenic thermal cycling.

• Journal of the Optical Society of Korea
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• 제19권6호
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• pp.705-710
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• 2015

The fabrication process of thin boron-doped nanocrystalline diamond (B-NCD) microelectrodes on fused silica single mode optical fiber cladding has been investigated. The B-NCD films were deposited on the fibers using Microwave Plasma Assisted Chemical Vapor Deposition (MW PA CVD) at glass substrate temperature of 475 ℃. We have obtained homogenous, continuous and polycrystalline surface morphology with high sp³ content in B-NCD films and mean grain size in the range of 100-250 nm. The films deposited on the glass reference samples exhibit high refractive index (n=2.05 at λ=550 nm) and low extinction coefficient. Furthermore, cyclic voltammograms (CV) were recorded to determine the electrochemical window and reaction reversibility at the B-NCD fiber-based electrode. CV measurements in aqueous media consisting of 5 mM K₃[Fe(CN)₆] in 0.5 M Na₂SO₄ demonstrated a width of the electrochemical window up to 1.03 V and relatively fast kinetics expressed by a redox peak splitting below 500 mV. Moreover, thanks to high-n B-NCD overlay, the coated fibers can be also used for enhancing the sensitivity of long-period gratings (LPGs) induced in the fiber. The LPG is capable of measuring variations in refractive index of the surrounding liquid by tracing the shift in resonance appearing in the transmitted spectrum. Possible combined CV and LPG-based measurements are discussed in this work.

• 대한화학회지
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• 제54권5호
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• pp.594-602
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• 2010

반도체의 경박단소화, 고밀도화에 따라 향후 반도체 패키지의 주 형태는 CSP(Chip Scale Package)가 될 것이다. 이러한 CSP에 사용되는 에폭시 수지 시스템의 흡습특성을 조사하기 위하여 에폭시 수지 및 충전재 변화에 따른 확산계수와 흡습율 변화를 조사하였다. 본 연구에 사용된 에폭시 수지로는 RE-304S, RE-310S, 및 HP-4032D를, 경화제로는 Kayahard MCD를, 경화촉매로는 2-methyl imidazole을 사용하였다. 충전재 크기 변화에 따른 에폭시 수지 성형물의 흡습특성을 조사하기 위하여 충전재로는 마이크로 크기 수준 및 나노 크기 수준의 구형 용융 실리카를 사용하였다. 이러한 에폭시 수지 성형물의 유리전이온도는 시차주사열량계를 이용하여 측정하였으며, 시간에 따른 흡습특성은 $85^{\circ}C$ and 85% 상대습도 조건하에서 항온항습기를 사용하여 측정하였다. 에폭시 수지 성형물의 확산계수는 Ficks의 법칙에 기초한 변형된 Crank 방정식을 사용하여 계산 하였다. 충전재를 사용하지 않은 에폭시 수지 시스템의 경우, 유리전이온도가 증가함에 따라 확산계수와 포화흡습율이 증가 하였으며 이는 유리전이온도 증가에 따른 에폭시 수지 성형물의 자유부피 증가로 설명하였다. 충전재를 사용한 경우, 충전재의 함량 증가에 따라 유리전이온도와 포화흡습율은 거의 변화가 없었으나, 확산계수는 충전재의 입자 크기에 따라 많은 변화를 보여주었다. 마이크로 크기 수준의 충전재를 사용한 경우 확산은 자유부피를 통하여 주로 이루어지나, 나노 크기 수준의 충전재를 사용한 에폭시 수지 성형물에서는 충전재의 표면적 증가에 따른, 수분 흡착의 상호작용을 통한 확산이 지배적으로 이루어진다고 판단된다.