• Title/Summary/Keyword: Fused silica

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Advanced surface processing of NLO borate crystals for UV generation

  • Mori, Yusuke;Kamimur, Tomosumi;Yoshimura, Masashi;Sasaki, Takatomo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.5
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    • pp.459-462
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    • 1999
  • Recent advances in NLO Borate Crystals for UV Generation are reviewed with the particular emphasis on the technique to improve the life time of UV optics. The laser-damage resistance of CLBO and fused silica surfaces was successfully improved after removing polishing compound by ion beam etching. The polishing compound embedded in the CLBO and fused silica surfaces were to a depth of less than 100nm. We were able to remove polishing compound without degrading the surface condition when the applied ion beam voltage was less than 200 V. The laser-induced surface damage threshold of CLBO was improved up to 15J/$\textrm{cm}^2$(wavelength: 355 nm, pulse width: 0.85 ns)as compared with that of the as-polished surface (11 J/$\textrm{cm}^2$). The laser-induced surface damage of fused silica also increased from 7.5J/$\textrm{cm}^2$ to 15J/$\textrm{cm}^2$. For the irradiation of a 266 nm high-intensity and high-repetition laser light, the surface lifetime of CLBO and fused silica could be more doubled compared with that of the as-polished surface.

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The Analysis of VOCs by GC/MS with Whole Column Coldtrapping on a Fused Silica Capillary Column in Indoor Environment

  • Dai, Shugui;Zhang, Lin;Bai, Zhipeng
    • Analytical Science and Technology
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    • v.8 no.4
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    • pp.829-834
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    • 1995
  • Whole column coldtrapping(WCC) on a fused silica capillary (FSCC)combined with GC/MS analysis was evaluated for use in the investigation of volatile organic compounds(VOCs) in indoor air. Research had indicated that a temperature of $-80^{\circ}C$ is optimal for WCC. Samples were analyzed on a $50m{\times}0.2mm$ cross-linked 5% phenylmethylsilicone fused silica column. Liquid nitrogen was used as the coolant for the peak resolution significantly. The analysis can be performed quickly and conveniently. More than 112 of VOCs were determined in the samples from three typical indoor environment including: (1) a room which had just been decorated involving building materials and paints; (2)a kitchen used for Chinese cooking, and (3) a room had tobacco smoke. The method is could be readily applied to rapid sample screening for VOCs contamination surveys or initial investigations with its valid and simple sampling and analytical technique.

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Efficient Purification Of Fused Ferritin[$F_{H}+F_{L}$] using Silica Powder and Gel Filtration Chromatography (실리카 분말과 젤 여과 크로마토그래피를 이용한 효과적인 융합 페리틴의 정제)

  • 허윤석;김인호
    • KSBB Journal
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    • v.17 no.4
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    • pp.365-369
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    • 2002
  • An iron-storage protein, ferritin is a spherical shell consisting of 24 H-and L-chain subunits. Soluble form of fused($F_{H}+F_{L}$ chain) ferritin was separated from disrupted recombinant E. coii cells, followed by silica powder adsorption. Ferritin was recovered from silica-poweder by distilled water, which was applied to gel filtration chromatography(GFC). Collected ferritin fractions from the GFC were assayed via iron-uptake and its molecular weight determined using GF-HPLC. Fused ferritin showed a higher activity than the M- or L- chain ferritin by two times.

Development of a Cross Capacitor Electrode for Measurements of Liquids Dielectric Constants (액체의 유전상수 정밀측정용 크로스 커패시터 전극 개발)

  • ;;;YU. p. Semenov
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.07a
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    • pp.675-678
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    • 2000
  • Using the principle of the cross capacitor, a precise system for measuring the electric constants of liquids has been developed. The four electrodes of the cross capacitor were formed around fused-silica tube by plating a gold film. The effect of a non-uniform tube wall ok the measured permittivity was investigated As the individual characteristics of the tubes were determined to be constant, the pure dielectric constants extracted from any effect of the fused-silica material could be precisely derived with uncertainty of less than ${\pm}$ 0.02∼0.05 %.

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Study on the Effect of Silica Particle Size on Dielectric Properties of Silica and Low Loss Polymer Composite Material (실리카-저손실 폴리머 복합 재료의 유전 특성에 관한 연구)

  • Kim, Sang-Hyun;Kim, Jun-Young;Yoo, Myong-Jae;Park, Seong-Dae;Lee, Woo-Sung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.275-276
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    • 2008
  • 통신기기가 고주파수화 함에 따라서 저유전 저손실 재료의 필요성이 증대되고 있으며, 세라믹/폴리머 복합재료를 고주파 회로 기판 소재로 이용하려는 관심이 증폭되고 있다. 본 연구에서는 저손실, 저유전율 특성을 구현하기 위해 $SiO_2$를 세라믹 필러로 복합물을 제작하였다. 평균 입자 크기가 16nm, $2.3{\mu}m$의 fumed 실리카와 평균 입자 크기 $1{\mu}m$, $4{\mu}m$의 fused 실리카를 사용하였다. 이 4종류 실리카를 사용하여 slurry를 제작하고 이를 활용하여 tape을 제작하였다. 제작된 복합체 tape을 적층하여 기판을 제작해 기판의 유전특성을 측정하였다. fumed 실리카의 경우 $SiO_2$ 10vol%이상에서는 균일한 tape성형이 어려워졌으며, 유전 손실이 fused 실리카와 비교하였을 때 큰 폭으로 증가하였다. fumed silica, fused silica 두 종류 모두 입도가 증가하면 유전손실이 증가하였다.

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Fabrication of BCP/Silica Scaffolds with Dual-Pore by Combining Fused Deposition Modeling and the Particle Leaching Method (압출 적층 조형법과 입자 추출법을 결합한 이중 공극 BCP/Silica 인공지지체의 제작)

  • Sa, Min-Woo;Kim, Jong Young
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.40 no.10
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    • pp.865-871
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    • 2016
  • In recent years, traditional scaffold fabrication techniques such as gas foaming, salt leaching, sponge replica, and freeze casting in tissue engineering have significantly limited sufficient mechanical property and cell interaction effect due to only random pores. Fused deposition modeling is the most apposite technology for fabricating the 3D scaffolds using the polymeric materials in tissue engineering application. In this study, 3D slurry mould was fabricated with a blended biphasic calcium phosphate (BCP)/Silica/Alginic acid sodium salt slurry in PCL mould and heated for two hours at $100^{\circ}C$ to harden the blended slurry. 3D dual-pore BCP/Silica scaffold, composed of macro pores interconnected with micro pores, was successfully fabricated by sintering at furnace of $1100^{\circ}C$. Surface morphology and 3D shape of dual-pore BCP/Silica scaffold from scanning electron microscopy were observed. Also, the mechanical properties of 3D BCP/Silica scaffold, according to blending ratio of alginic acid sodium salt, were evaluated through compression test.

Fabrication of $Al_2O_3/Al$ Composites by Replacement Reaction of Molten Metal Al (용융 Al의 치환반응에 의한 $Al_2O_3/Al$ 복합체의 제조)

  • 정두화;김용진;배원태
    • Journal of the Korean Ceramic Society
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    • v.34 no.6
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    • pp.591-600
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    • 1997
  • Al2O3/Al composites were produced by displacement reaction method, which was carried out by immersing the sintered silica preform, which was prepared from fused silica powder, in molten aluminum. Because the molten aluminum did not penetrate into the silica preform with higher than 20% of porosity when the displacement reaction was accomplished at 100$0^{\circ}C$ for 10 hours in air atmosphere, the optimum range of sintering temperature of silica preform was from 135$0^{\circ}C$ to 140$0^{\circ}C$. The microstructure of this Al2O3/Al composites showed three-dimentionally co-continuous alumina, which provides wear resistance and high stiffness, and aluminium which acts as a toughnening phase. The grain size of the alumina in composites did not change with the particle size of the silica preform. The exact shape of the preform was retained and a net-shaped composite was produced. The representative Al2O3/Al composite prepared in this study showed 3.30mg/㎤ of bulk density, 350-430 MPa of flexural strength, 7.0 MPa.m1/2 of fracture toughness, and good machinability.

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Measurement of Ultrasonic Nonlinearity Parameter of Fused Silica and Al2024-T4 (Fused Silica와 Al2024-T4의 비선형 파라미터 측정)

  • Kang, To;Lee, Taekgyu;Song, Sung-Jin;Kim, Hak-Joon
    • Journal of the Korean Society for Nondestructive Testing
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    • v.33 no.1
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    • pp.14-19
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    • 2013
  • Nonlinearity parameter is an inherent property of materials measuring fundamental acoustic amplitude($A_1$) and second harmonic amplitude($A_2$). However, measurement of $A_1$ and $A_2$ has complex calibration procedure, many researchers prefer to measure relative nonlinearity parameter rather than absolute nonlinearity parameter. But, relative nonlinearity parameter is only detect materials degradation with various degradation samples, it is limited application in determining third order elastic constants of materials. Therefore, in this study, the piezoelectric detection method is adopted to measure absolute nonlinearity parameter due to experimental simplicity compare to capacitive detector. Linearity of measurement system is verified by $A_1^2vsA_2$ plot, and we measured ultrasonic nonlinearity parameters of fused silica and Al2024-T4.

Tuning Thermal Expansion Coefficient of Composites Containing Epoxy Resin/Inorganic Additives for Stone Conservation (에폭시 수지/무기물 첨가제 복합체의 열팽창계수 조절 및 석조문화재의 응용)

  • Choi, Yong-Seok;Chae, Il-Seok;Kang, Yong-Soo;Won, Jong-Ok;Kim, Jeong-Jin;Kim, Sa-Dug
    • Journal of Conservation Science
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    • v.27 no.4
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    • pp.431-440
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    • 2011
  • The thermal expansion coefficient of epoxy/inorganic additives composites was controlled by changing the amount of the inorganic additives such as talc and fused silica. The epoxy resin comprises hydrogenated bisphenol A (HBA)-based epoxide, difunctional polyglycidyl epoxide (DPE) as a diluent and isophorone-diamine (IPDA) as a crosslinking agent, which was subsequently mixed with inorganic additives (talc and fused silica). The thermal expansion coefficient was decreased by increasing amount of inorganic additives, nearly to fresh granite. Fused silica was more effective than talc in lowering the thermal expansion coefficient. Additionally, lexural and tensile strengths of the composites were getting lower and higher with the amount of the inorganic fillers, respectively. It was thus concluded that an epoxy composite containing inorganic fillers was developed to show much lower thermal expansion coefficient, similar to fresh granite, than the neat epoxy resin, and also proper mechanical strengths for applications.