• Title/Summary/Keyword: Forming Defects

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Research of Liquid Crystal Alignment on Tantalum Oxide by Using Ion Beam Irradiation (이온빔 조사를 사용한 탄탈륨 산화막에서의 액정 배향에 대한 조사)

  • Lim, Ji-Hun;Oh, Byeong-Yun;Lee, Won-Kyu;Lee, Kang-Min;Na, Hyun-Jae;Park, Hong-Kyu;Seo, Dae-Shik
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.300-300
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    • 2008
  • In this study, the advanced DuoPIGatron-type ion beam (IB) system was applied to inorganic thin film for aligning liquid crystal (LC). LC alignment on $Ta_2O_5$ via IB irradiation was embodied. As a result of IB irradiation, the homogeneously aligned liquid crystal display (LCD) on $Ta_2O_5$ was observed with low pretilt angles. The $Ta_2O_5$ were deposited on indium-tin-oxide coated Coming 1737 glass substrates by rf magnetron sputtering at $200^{\circ}C$. The deposition process resulted in forming very uniform thin film on glass substrates without any defects. To confirm the application of the inorganic alignment on modem display optical devices, we fabricated twisted nematic LCD and measured optical property and response time. As a result of the experiment, the electro optical characteristics of the LCD fabricated by using IB irradiation on $Ta_2O_5$ alignment layer were similar with the other LCD fabricated by using rubbing process.

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A forging die design to improve the flower shape of flange bolt (플랜지 볼트의 플라워 형상 결함 개선을 위한 단조 금형설계)

  • Kim, Kwan-Woo;Lee, Geun-Tae;Cho, Hae-Young
    • Journal of Advanced Marine Engineering and Technology
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    • v.40 no.4
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    • pp.314-319
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    • 2016
  • Flange bolt has a circular flange under the head that acts like a washer to distribute the clamping load over a large area. Flange bolt has usually been manufactured by cold forging. Flower shape defect occurs in the flange forging stage. This defect causes lack of dimensional accuracy and low quality. So it is needed to improve these forging defects. In this study, die design method for flower shape defect of flange bolt was suggested. In order to improve flower shape defect, inner diameter of the addition die in conventional forging process was modified. The forging process with applied modified die was simulated by commercial FEM code DEFORM-3D. The simulated results for modified die were confirmed by experimental trials with the same condition.

Development of SiC Composite Solder with Low CTE as Filling Material for Molten Metal TSV Filling (용융 금속 TSV 충전을 위한 저열팽창계수 SiC 복합 충전 솔더의 개발)

  • Ko, Young-Ki;Ko, Yong-Ho;Bang, Jung-Hwan;Lee, Chang-Woo
    • Journal of Welding and Joining
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    • v.32 no.3
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    • pp.68-73
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    • 2014
  • Among through silicon via (TSV) technologies, for replacing Cu filling method, the method of molten solder filling has been proposed to reduce filling cost and filling time. However, because Sn alloy which has a high coefficient of thermal expansion (CTE) than Cu, CTE mismatch between Si and molten solder induced higher thermal stress than Cu filling method. This thermal stress can deteriorate reliability of TSV by forming defects like void, crack and so on. Therefore, we fabricated SiC composite filling material which had a low CTE for reducing thermal stress in TSV. To add SiC nano particles to molten solder, ball-typed SiC clusters, which were formed with Sn powders and SiC nano particles by ball mill process, put into molten Sn and then, nano particle-dispersed SiC composite filling material was produced. In the case of 1 wt.% of SiC particle, the CTE showed a lowest value which was a $14.8ppm/^{\circ}C$ and this value was lower than CTE of Cu. Up to 1 wt.% of SiC particle, Young's modulus increased as wt.% of SiC particle increased. And also, we observed cross-sectioned TSV which was filled with 1 wt.% of SiC particle and we confirmed a possibility of SiC composite material as a TSV filling material.

Effect of Annealing Temperature on the Electrical Performance of SiZnSnO Thin Film Transistors Fabricated by Radio Frequency Magnetron Sputtering

  • Kim, Byoungkeun;Lee, Sang Yeol
    • Transactions on Electrical and Electronic Materials
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    • v.18 no.1
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    • pp.55-57
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    • 2017
  • Amorphous oxide thin film transistors (TFTs) were fabricated with 0.5 wt% silicon doped zinc tin oxide (a-0.5SZTO) thin film deposited by radio frequency (RF) magnetron sputtering. In order to investigate the effect of annealing treatment on the electrical properties of TFTs, a-0.5SZTO thin films were annealed at three different temperatures ($300^{\circ}C$, $500^{\circ}C$, and $700^{\circ}C$ for 2 hours in a air atmosphere. The structural and electrical properties of a-0.5SZTO TFTs were measured using X-ray diffraction and a semiconductor analyzer. As annealing temperature increased from $300^{\circ}C$ to $500^{\circ}C$, no peak was observed. This provided crystalline properties indicating that the amorphous phase was observed up to $500^{\circ}C$. The electrical properties of a-0.5SZTO TFTs, such as the field effect mobility (${\mu}_{FE}$) of $24.31cm^2/Vs$, on current ($I_{ON}$) of $2.38{\times}10^{-4}A$, and subthreshold swing (S.S) of 0.59 V/decade improved with the thermal annealing treatment. This improvement was mainly due to the increased carrier concentration and decreased structural defects by rearranged atoms. However, when a-0.5SZTO TFTs were annealed at $700^{\circ}C$, a crystalline peak was observed. As a result, electrical properties degraded. ${\mu}_{FE}$ was $0.06cm^2/Vs$, $I_{ON}$ was $5.27{\times}10^{-7}A$, and S.S was 2.09 V/decade. This degradation of electrical properties was mainly due to increased interfacial and bulk trap densities of forming grain boundaries caused by the annealing treatment.

Stepwise verification of bone regeneration using recombinant human bone morphogenetic protein-2 in rat fibula model

  • Nam, Jung-Woo;Kim, Hyung-Jun
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.43 no.6
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    • pp.373-387
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    • 2017
  • Objectives: The purpose of this study was to introduce our three experiments on bone morphogenetic protein (BMP) and its carriers performed using the critical sized segmental defect (CSD) model in rat fibula and to investigate development of animal models and carriers for more effective bone regeneration. Materials and Methods: For the experiments, 14, 16, and 24 rats with CSDs on both fibulae were used in Experiments 1, 2, and 3, respectively. BMP-2 with absorbable collagen sponge (ACS) (Experiments 1 and 2), autoclaved autogenous bone (AAB) and fibrin glue (FG) (Experiment 3), and xenogenic bone (Experiment 2) were used in the experimental groups. Radiographic and histomorphological evaluations were performed during the follow-up period of each experiment. Results: Significant new bone formation was commonly observed in all experimental groups using BMP-2 compared to control and xenograft (porcine bone) groups. Although there was some difference based on BMP carrier, regenerated bone volume was typically reduced by remodeling after initially forming excessive bone. Conclusion: BMP-2 demonstrates excellent ability for bone regeneration because of its osteoinductivity, but efficacy can be significantly different depending on its delivery system. ACS and FG showed relatively good bone regeneration capacity, satisfying the essential conditions of localization and release-control when used as BMP carriers. AAB could not provide release-control as a BMP carrier, but its space-maintenance role was remarkable. Carriers and scaffolds that can provide sufficient support to the BMP/carrier complex are necessary for large bone defects, and AAB is thought to be able to act as an effective scaffold. The CSD model of rat fibula is simple and useful for initial estimate of bone regeneration by agents including BMPs.

Analysis of Tube Extrusion Process Conditions Using Mg Alloy for Automotive Parts (자동차 부품용 마그네슘 합금 관재 압출공정조건 분석)

  • Park, Chul Woo;Kim, Ho Yoon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.12
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    • pp.1675-1682
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    • 2012
  • Weight reduction is increasingly being considered very important in light of air pollution and the exhaustion of resources. As a result, many automotive components are being replaced by Al and Mg alloys, and studies are increasingly focusing on the same. However, the use of Mg alloys is limited because they have higher material cost and lower productivity owing to the difficult forming conditions compared with Al alloys. In this study, the tube extrusion process conditions of an automotive bumper back beam were analyzed using FEA. Material tests were performed to determine the properties, and experiments and analyses for a simple shape were performed to define the data for heat generation during plastic deformation. Then, the analyses of the product were carried out by considering various temperatures and ram speeds. The conditions were then established, and a product without surface defects was extruded successfully.

A Study on the Plate-Type Polymer Hyperfine Pit Structure Fabrication and Mechanical Properties Measurement by Using Thermal-Nanoindentation Process (열간나노압입공정을 이용한 극미세 점구조체 제작을 위한 플라스틱소재 판의 기계적 특성 조사)

  • Lee, E.K.;Kang, C.G.
    • Transactions of Materials Processing
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    • v.17 no.8
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    • pp.633-642
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    • 2008
  • It's important to measure quantitative properties about thermal-nano behavior of polymer for producing high quality components using Nanoimprint lithography process. Nanoscale indents can be used to make the cells for molecular electronics and drug delivery, slots for integration into nanodevices, and defects for tailoring the structure and properties. In this study, formability of polymethylmetacrylate(PMMA) and polycarbonate(PC) were characterized Polymer has extreme variation in thermo mechanical variation during forming high temperature. Because of heating the polymer, it becomes softer than at room temperature. In this case it is particularly important to study high temperature-induced mechanical properties of polymer. Nanoindenter XP(MTS) was used to measure thermo mechanical properties of PMMA and PC. Polymer was heated by using the heating stage on NanoXP. At CSM(Continuous Stiffness Method) mode test, heating temperature was $110^{\circ}C,120^{\circ}C,130^{\circ}C,140^{\circ}C$ and $150^{\circ}C$ for PMMA, $140^{\circ}C,150^{\circ}C,160^{\circ}C,170^{\circ}C$ and $180^{\circ}C$ for PC, respectively. Maximum indentation depth was 2000nm. At basic mode test, heating temperature was $90^{\circ}C$ and $110^{\circ}C$ for PMMA, $140^{\circ}C,160^{\circ}C$ for PC. Maximum load was 10mN, 20mN and 40mN. Also indented pattern was observed by using SEM and AFM. Mechanical properties of PMMA and PC decreased when temperature increased. Decrease of mechanical properties from PMMA went down rapidly than that of PC.

Preparation and Evaluation of Low Viscosity Acrylic Polymer Based Pretreatment Solution for DTP Reactive Ink (DTP 반응성 잉크용 저점도 아크릴계 고분자 전처리액 제조 및 특성 평가)

  • Kim, Hyeok-Jin;Seo, Hye-Ji;Kwak, Dong-Sup;Hong, Jin-Pyo;Yoon, Seok-Han;Shin, Kyung
    • Textile Coloration and Finishing
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    • v.29 no.3
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    • pp.122-130
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    • 2017
  • In the direct digital textile printing process, the pre-treatment process is an essential condition for products by forming a clear pattern by sticking and penetration of DTP dye without spreading on the fabric. Recently, pre-treatment agent is changing from high viscosity to low viscosity in order to reduce defects of fabric during pre-treatment process. In this study, pre-treatment agent of acrylic polymer with low viscosity(less than 50cps) was prepared according to the solid content of the polymer, pre-treated on the cotton fabric, and direct DTP printing was performed to compare the color and sharpness. As a result, it showed high color at a viscosity of 50cps or less. When the solid content of the polyacrylic acid having a high molecular weight(A1) was 2.5wt%, when the solid content of the polyacrylic acid having a low molecular weight(A2) was 1 - 1.5wt%, the color was the best. And when the solid content of A1 and A2 was 1.5wt%, the degree of spreading was small and A1 was superior to A2 at the sharpness.

The Effects of Volume Ratio and Shape on the Formation of Adiabatic Shear Band in WHA (텅스텐 중합금의 부피분율, 입자형상에 따른 단열전단밴드 형성 연구)

  • 이승우;송흥섭;문갑태
    • Transactions of Materials Processing
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    • v.11 no.8
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    • pp.682-690
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    • 2002
  • The formation of adiabatic shearband in tungsten heavy alloys(WHA) was studied in this investigation. Five prismatic specimens were loaded by high velocity impacts and treated as plane strain problems. To find out the effect of particle's volume ratio, specimens containing 81%, 93% and 97% volume percents of tungsten particles were used. Also the effects of particle's geometry and size on the formation of shearband were studied for 81% volume percent alloys by small size particle model, large size particle model and undulated particle models, and the results were discussed.be used to diagnose the causes of necking and fracture in industrial practice and to investigate whether these defects were caused by material property variation, changes in lubrication, or incorrect press settings. In non-axisymmetric deep drawing, three modes of forming regimes are found: draw, stretch, plane strain. The stretch mode for non-axisymmetric deep drawing could be defined when the major and minor strains are positive. The draw mode could be defined when the major strain is positive and minor strain is negative, and plane strain mode could be defined when the major strain is positive and minor strain is zero. Through experiments the draw mode was shown on the wall and flange are one of a drawn cup, while the plane strain and the stretch mode were on the punch head and the punch corner area respectively, We observed that the punch load of elliptical deep drawing was decreased according to increase of die corner radius and the thickness deformation of minor side was more large than major side.

Characteristics of $CO_2$ or Nd:YAG Laser Welded 600MPa Grade TRIP Steel (600MPa급 TRIP강의 $CO_2$ 및 Nd:YAG 레이저 용접부의 특성)

  • Han, Tae-Kyo;Kim, Seung-Jun;Lee, Bong-Keun;Kim, Dae-Up;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • v.24 no.1
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    • pp.56-63
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    • 2006
  • The characteristics of $CO_2$ or Nd:YAG laser welded 600MPa ade TRIP steel was investigated. He or Ar gas was used as a shield gas in case of $CO_2$ laser welding, but the shield gas was not used in case of Nd:YAG laser welding. Bead on plate welding was performed with various welding conditions. Defects in the joints of both welding type occurred at 1.8m/min but were not observed over the welding speed of 2.1m/min in case of Nd:YAG laser welding. However, porosity occurred in $CO_2$ laser welding and the tendency of decreasing with the increase of welding speed. The hardness was the highest at heat affected zone near fusion zone as well as at the fusion zone and decreased on approaching the base metal. In a perpendicular tensile test to the weld line, all specimens that have been welded at optimum conditions were fractured at the base metal, and the tensile properties showed the rather higher than those of raw material. In a parallel tensile test, the strength of the joints was higher than that of the base metal. Elongation was found to be lower than that of the raw material. Forming height by Erichsen test and elongation were deeply related with the ratio of base metal/weld metal and the maximum hardness of the weld metal. Also porosity induced to decrease the strength and the elongation. The maximum formability was recorded at approximately 80% as compared with that of the raw material with the optimum condition.