• 제목/요약/키워드: Food analysis

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LC/MS/MS를 이용한 국내 유통 농산물의 잔류농약 실태조사 (Monitoring of Residual Pesticides in Agricultural Products by LC/MS/MS)

  • 김미옥;황혜신;임무송;홍지은;김순선;도정아;최동미;조대현
    • 한국식품과학회지
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    • 제42권6호
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    • pp.664-675
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    • 2010
  • 국내 유통 농산물 16품목을 대상으로 LC/MS/MS로 분석 가능한 다종다성분 농약 60종을 검사하여 식품의 잔류농약 안전성을 조사하였다. 조사대상 농산물 510건 중 대부분의 농산물인 490건(96.1%)의 농산물은 농약이 검출되지 않았으며, 18건(3.5%)의 농산물에서 농약이 검출되었으나, 대부분 잔류허용기준 미만으로 검출되었다. 들깻잎, 부추 등 엽채류의 검출빈도가 높은 편이었으나 대부분 잔류허용기준 미만으로 검출되었고, 시금치, 부추에서 각각 ethaboxam, fluquinconazole이 잔류허용기준 이상으로 검출되었다. 검출 농약은 9종이었으며, azoxystrbin과 dimethomorph가 가장 많이 검출되었다. 쌀 등 16품목의 다소비 농산물을 대상으로한 모니터링 결과 농약의 잔류량은 대부분 잔류허용기준 미만으로 비교적 안전한 수준으로 농산물에 대한 농약 관리가 이루어지고 있는 것으로 판단되었다.

건조에 따른 채소류 중의 이산화황함량 분석 (Study of Sulfur Dioxide Contents in Various Fresh Vegetables During the Drying Process)

  • 하성용;김현정;우성민;이준배;조유진;김양선;반경녀;박종석;김희연;장영미;김미혜
    • 한국식품위생안전성학회지
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    • 제25권4호
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    • pp.303-309
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    • 2010
  • 본 연구는 신선채소류의 건조전 후의 이산화황함량의 변화를 조사하여 건조채소류에 이산화황사용여부를 판단하기 위한 기초자료를 얻고자 시행하였다. 신선채소류 6품목 182건을 수거하여 열풍건조하였고, 건조온도는 50~60도에서 최종수분함량이 10%정도 되도록 건조하였다. 건조전 신선채소류의 측정값은 발표된 문헌과 유사하였고, 건조후 측정값은 파, 양파, 양배추, 마늘, 무잎, 그리고 무에서 각각 평균적으로 104.6, 75.4, 129.1, 197.6, 23.0, 52.4 mg/kg 검출되었다. 국내 유통중인 건조채소류 41건을 분석한 결과 실험실에서 전처리 없이 건조한 시료들보다는 적은 값이 검출되었고, 아황산처리를 하지 않은 것으로 판단할 수 있었다. 건조에 따른 이산화황함량 변화를 검토한 결과 이산화황함량은 수분이 감소함에 따라 증가하지만, 증가량은 수분감소량을 고려한 예측값과는 다른 결과를 보여 주었고, 그 형태는 품목마다 몇가지 그룹으로 분류할 수 있었다. 무, 양파, 파 등은 측정값이 예측값보다 적게 검출되었고, 무잎은 다른 시료에 비해 매우 낮은 값을 보여주었으며, 양배추는 유사한 값으로 검출되었다. 마늘의 경우는 측정값이 예측값 보다 높은 경우도 있었으며, 일관성있는 결과를 얻을 수 없었다. 이것은 건조채소류에서 검출되는 이산화황함량은 단순하게 수분함량의 변화에 의해 좌우되는 것이 아님을 의미한다. 곧, 시료내에 이산화황함량에 영향을 주는 성분들이 건조과정중에 휘산 또는 효소반응등의 물리 화학적 변화가 수반되며, 수분의 감소가 시료내 이산화황함량의 증가에 중요한 요소이기는 하지만, 그 외에 함유 성분의 특성이나 건조조건 그리고 건조과정에서 발생하는 주요 성분들의 변화등도 의미있는 영향을 미칠 것임을 간접적으로 알 수 있었다. 결과적으로 수입 또는 유통중인 건조채소류에 대한 아황산염류 관리를 위해서는 각 품목별 특정도 고려되어야 한다. 이를 위해 지금까지와 같이 지속적으로 자연발생 이산화황함량에 대한 조사가 이루어져야 할 뿐 아니라 나아가 선택성있는 분석법의 검토가 진행되어야 한다고 생각된다. 본 연구결과는 건조채소류의 아황산염류의 안전한 관리를 위한 자료로서 활용되어질 것으로 판단된다.

한국 식품 관련 학회지(1984 - 1993)에 게재된 '식품성분 분석' 연구논문에 대한 내용 연구 (Study of Food Analysis Research Papers in Food Science related Korean Journals by Content Analysis)

  • 김정숙;김영남
    • 한국생활과학회지
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    • 제3권1호
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    • pp.51-58
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    • 1994
  • The rapid development of science and technology has brought about a quantitative expansion and a decrease of practical life span of information. Food science, a kind of life science and practical science, can not be an exception. Analysis of food components is the fundamental basis of the Food Science. So I would like this to be of some help to the following researches through the quantitative and qualitative analysis of the contents of the food analysis research papers in food science related Korean journals. Five hundred seventy four research papers published from 1984 to 1993 in the three journals, that is, Korean Journal of Food Science & Technology. The Korean Journal of Nutrition, The Korean Journal of Home Economics, which is three major journals read by people in Home Economics area are analyzed in this study. The method applied in this study is content analysis. Followings are the results of the content analysis : 1) When categorize the material foods into food groups, cereal group is analyzed most often(15.8%), followed by fish and shellfish group(12.4%), oil and fat group(11.8%). The least often analyzed food group is egg group. Among the food soybean is most often analyzed(6.0%), followed by polished rice(3.7%), glutinous rice(2.2%), cabbage(2.1%) and human milk(1.8%). 2) About the analyzed food components, the general components such as moisture, crude protein, crude fat, carbohydrate and ash has been analyzed very often but the trace nutrients such as vitamins and minerals has scarcely been analyzed. 3) The method used in the food components analysis is usually AOAC(Association of Official Analytical Chemist, USA). HPLC was applied to the analysis of many food components like amino acids, fatty acids, vitamin A, thiamin, riboflavin, niacin, vitamin C and vitamin E.

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염산부플로메딜 정과 염산티클로피딘 정의 용출시험법 개발 (Development of Dissolution Test Method for Buflomedil Hydrochloride Tablets and Ticlopidine Hydrochloride Tablets)

  • 이륜경;정경록;오현숙;심지연;서상철;이효정;김민아;박성민;이규하;손경희;김인규;사홍기;최후균;조태용;홍충만
    • 약학회지
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    • 제56권4호
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    • pp.211-216
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    • 2012
  • Drug dissolution test has been used for the purpose of both quality control of solid oral dosage forms and predicting in vivo drug release profiles. In this study, the dissolution profiles of buflomedil hydrochloride tablets and ticlopidine hydrochloride tablets were investigated according to the "Guidelines on Specifications of Dissolution tests for Oral dosage forms" of Korean Pharmacopoeia (KP). The analytical method using HPLC was validated. The validation was performed in terms of specificity, linearity, accuracy, precision and limit of quantitation.

Chemical and Sensory Characterization of Korean Commercial Rice Wines (Yakju)

  • Lee, Seung-Joo;Kwon, Young-Hee;Kim, Hye-Ryun;Ahn, Byung-Hak
    • Food Science and Biotechnology
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    • 제16권3호
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    • pp.374-380
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    • 2007
  • Chemical and sensory profiles of 5 Korean commercial rice wines (yakju) were developed using descriptive, physicochemical, and volatile analyses. Color, 6 aroma, and 5 taste attributes of these rice wines were evaluated by a panel of 13 judges. Sample wines were analyzed for titratable acidity, ethanol content, pH, Hunter colorimeter value, organic acids, and free sugars. Volatile analysis of the samples revealed the presence of 2 acids, 7 alcohols, 19 esters, and 5 miscellaneous compounds. Based on principal component analysis of the descriptive data, rice wines were primarily separated along the first principal component, which accounted for 57% of the total variance between the rice wines with high intensities of 'color' and 'sweet aroma' versus 'ginseng' aroma.

DEA를 이용한 식자재유통 및 급식기업의 효율성 분석 (Analysis on Efficiency of Food Material Distributors and Food Service Companies by DEA)

  • 민하나;김석운;최규완
    • 한국식생활문화학회지
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    • 제31권4호
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    • pp.339-347
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    • 2016
  • With the interest on operational efficiency due to the rapid growth of food material distribution industry and food service industry, the study adopts DEA (Data Envelopment Analysis) model and examines to measure the technological, pure technical and scale efficiency those companies engaging in the food material distribution and food service business. As a result of analysis, the companies operating integrated business have relatively higher efficiency than those operating only food material distribution or food service companies while the result indicates that three efficiencies don't have significant difference depending on whether affiliated companies or not. In the results from the measuring by DEA.

Food Choice Questionnaire 방법을 적용한 식품선택 동기요인 분석 (Analysis of the Motives for Food Choice Using Food Choice Questionnaire)

  • 김아영;이슬기;이민아
    • 한국식품조리과학회지
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    • 제31권3호
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    • pp.352-359
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    • 2015
  • The purpose of this study was to analyze the motives for food choice using a Food Choice Questionnaire (FCQ). A FCQ, an instrument that measures the reported importance of nine factors underlying food choice, was administered to a representative sample of 157 adult respondents from 21 to 27 October 2013. Statistical analyses such as Descriptive statistics, Factor analysis, Reliability analysis, Pearson correlation, independent samples t-test, and analysis of variance (ANOVA) were performed on the data using the SPSS PASW Statistics 18.0 for Windows. According to the results, five food choice motivation factors were discerned: health, sensory and mood, convenience, price, and familiarity. The most important factors reported were price, sensory and mood, convenience, health and familiarity. We found that food choice motivation is distinguished by age, frequency of eating out, and consumption of HMR. Females in this study gave higher importance scores to health, sensory and mood, and familiarity. There were higher correlations between 'health' and 'sensory appeal and mood'.

식품산업에서 활용되는 식품안전 분석기술의 현황 (Food safety analytical techniques used in food industry)

  • 김영준
    • 식품과학과 산업
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    • 제51권1호
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    • pp.16-25
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    • 2018
  • Recently, the importance of analytical techniques related to food safety is emerging in the food industry due to changes in diet patterns, environmental changes, climate change and consumer's interest in food safety. In particular, food safety accidents in the food industry may cause economic losses such as media reports, product recalls, consumer distrust, and so on. Therefore, a systematic, proactive and comprehensive food safety management system is increasingly required to prevent food safety issues. Efforts to ensure the reliability of food safety are essential by introducing various analysis instruments such as LC, GC, ICP, LC/MS/MS, GC/MS/MS, ICP/MS, PCR, and RT-PCR. In addition, recent food safety analytical techniques used in food industry should be shifted paradigm by developing multi-component simultaneous analytical method, low cost with high efficient analytical method, and eco-friendly method.

청소년의 식생활 라이프스타일 유형에 따른 불량식품관리 특성 (Adulterated Food Management Characteristics according to Dietary Lifestyles among Adolescents)

  • 김윤화
    • 대한지역사회영양학회지
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    • 제21권6호
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    • pp.509-519
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    • 2016
  • Objectives: Adulterated food education in adolescence period is very important because dietary management related to food safety is not made in a short period. This study aimed to identify dietary lifestyle factors which drive adulterated food management among middle and high school students. Methods: Data was collected from 270 middle and high school students in Daegu using a self-administered questionnaire in March and April of 2015. Data was analyzed using frequency analysis, one-way analysis of variance, ${\chi}^2$-test, factor analysis, reliability analysis, regression analysis, and cluster analysis. Results: The results of factor analysis indicated that adulterated food management awareness was classified into necessity, difficulty, and food purchasing anxiety. The adulterated food management capability was sub-grouped into environmental grasp, food identification, cooking hygiene, and situation management. The adulterated food management efficacy composed of management confidence, action intention, and knowledge. Dietary lifestyle comprised of gustation, family, and health factors after factor analysis, and it consisted of all seeking group, gustation seeking group, family seeking group, health seeking group, and family and health seeking group after cluster analysis. The gustation, family and health factors were significantly affected the factors of awareness, capability and efficacy of adulterated food management (p < 0.05). The frequency of health conditions, helping with meal preparation, and the times of eating out were significantly different according to seeking groups of dietary lifestyle (p < 0.01). The scores of awareness, capability and efficacy of adulterated food management of family and health seeking group were significantly higher than the other seeking groups (p < 0.05). Conclusions: This study suggests that adulterated food management education programs should account for gustation, family and health factors of dietary lifestyle to be effective for adolescents.

조리식품의 기호에 대한 연구(제 1 보) -조리식품기호에 대한 분석적 연구 <전북지방의 3도시를 중심으로>- (Studies on the Preference for Prepared Food (Part 1) -An Analytical Study on the Preference for the Prepared Food-)

  • 한진숙;신미경
    • 한국식생활문화학회지
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    • 제3권1호
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    • pp.57-66
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    • 1988
  • The results obtained by survey on 599 respondents of different age groups for preference of 84 prepared foods were subjected to statistical principal component analysis, factor analysis, analysis of variance, scheffe verification, and discriminant analysis so as to find a structure of preference for foods. The results may be summarized as follows: 1. The results of the factor analysis indicate that 84 prepared food items may be classified into 3 groups and that by knowing an indvidual's preference to one prepared food, one can presume his preference to the others in the same group without carrying out actual test. 2. The results from an analysis of variance showed that most of primary school children extremely liked snacks, seniors liked Korean cooking, primary school children and collegians had weaknesses for western cookings while kindergarden children and adults over 50 years old disliked them.

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