• Title/Summary/Keyword: Fabrication route

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Spark Plasma Sintering of the Ni-graphite Composite Powder Prepared by Electrical Explosion of Wire in Liquid and Its Properties

  • Thuyet-Nguyen, Minh;Kim, Jin-Chun
    • Journal of Powder Materials
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    • v.27 no.1
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    • pp.14-24
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    • 2020
  • In this work, the electrical explosion of wire in liquid and subsequent spark plasma sintering (SPS) was introduced for the fabrication of Ni-graphite nanocomposites. The fabricated composite exhibited good enhancements in mechanical properties, such as yield strength and hardness, but reduced the ductility in comparison with that of nickel. The as-synthesized Ni-graphite (5 vol.% graphite) nanocomposite exhibited a compressive yield strength of 275 MPa (about 1.6 times of SPS-processed monolithic nickel ~170 MPa) and elongation to failure ~22%. The hardness of Ni-graphite composite had a value of 135.46 HV, which is about 1.3 times higher than that of pure SPS-processed Ni (105.675 HV). In terms of processing, this work demonstrated that this processing route is a novel, simple, and low-cost method for the synthesis of nickel-graphite composites.

Fabrication of Macroporous Carbon Foam with Uniform Pore Size Using Poly(methyl methacrylate) Particles As The Template

  • Kim, Jin-Sil;Rhym, Young-Mok;Shim, Sang-Eun
    • Journal of Powder Materials
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    • v.18 no.2
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    • pp.129-134
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    • 2011
  • Herein, macroporous carbon materials were readily prepared by carbonization of cured body of resorcinol and formaldehyde using poly(methyl methacrylate) colloid microspheres which were employed as the template in the gelation of resorcinol with formaldehyde. The gel in the water was solvent exchanged with methanol and the wet gel was dried. After carbonization of the template-gel composite at $800^{\circ}C$, it was found that pores were left corresponding to the size of the template, yielding carbon materials with a fine porous structure with enlarged surface area and significant porosity. Properties of the carbon foams including the structure, morphology, thermal stability, and porosity were investigated. Finally, it was concluded that the method using polymer colloids as the template provided a facile route to prepare carbon foams.

High Quality Vertical Silicon Channel by Laser-Induced Epitaxial Growth for Nanoscale Memory Integration

  • Son, Yong-Hoon;Baik, Seung Jae;Kang, Myounggon;Hwang, Kihyun;Yoon, Euijoon
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.14 no.2
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    • pp.169-174
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    • 2014
  • As a versatile processing method for nanoscale memory integration, laser-induced epitaxial growth is proposed for the fabrication of vertical Si channel (VSC) transistor. The fabricated VSC transistor with 80 nm gate length and 130 nm pillar diameter exhibited field effect mobility of $300cm^2/Vs$, which guarantees "device quality". In addition, we have shown that this VSC transistor provides memory operations with a memory window of 700 mV, and moreover, the memory window further increases by employing charge trap dielectrics in our VSC transistor. Our proposed processing method and device structure would provide a promising route for the further scaling of state-of-the-art memory technology.

Fabrication of Reaction Sintered SiC Materials by Complex Slurry with Nano Size Particles (나노입자 혼합 복합슬러리를 이용한 반응소결 SiC 재료의 제조)

  • Lee Sang-Pill
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.29 no.3 s.234
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    • pp.425-431
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    • 2005
  • The efficiency of complex slurry preparation route for developing the high performance SiC matrix of $RS-SiC_{f}/SiC$ composites has been investigated. The green bodies for RS-SiC materials prior to the infiltration of molten silicon were prepared with various C/SiC complex slurries, which associated with both the sizes of starting SiC particles and the blending conditions of starting SiC and C particles. The characterization of Rs-SiC materials was examined by means of SEM, EDS and three point bending test. Based on the mechanical property-microstructure correlation, the process optimization is also discussed. The flexural strength of Rs-SiC materials greatly depended on the content of residual Si. The decrease of starting SiC particle size in the C/SiC complex slurry was effective for improving the flexural strength of RS-SiC materials.

Fabrication of Mesoporous Hollow TiO2 Microcapsules for Application as a DNA Separator

  • Jeon, Sang Gweon;Yang, Jin Young;Park, Keun Woo;Kim, Geon-Joong
    • Bulletin of the Korean Chemical Society
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    • v.35 no.12
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    • pp.3583-3589
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    • 2014
  • This study evaluated a simple and useful route to the synthesis of mesoporous $TiO_2$ microcapsules with a hollow macro-core structure. A hydrophilic precursor sol containing the surfactants in the hydrophobic solvents was deposited on PMMA polymer surfaces modified by non-thermal plasma to produce mesoporous shells after calcination. The surface of the PMMA polymer spheres was coated with $NH_4F$ and CTAB to control the interfacial properties and promote the subsequent deposition of inorganic sols. These hollow type mesoporous $TiO_2$ microcapsules could be applied as an efficient substrate for the immobilization of DNA oligonucleotides.

Electrochemical Synthesis of Compound Semiconductor Photovoltaic Materials

  • Yu, Bong-Yeong;Jeon, Byeong-Jun;Lee, Dong-Gyu
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.11.1-11.1
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    • 2010
  • As one of the non-vacuum, low temperature fabrication route, electrochemical synthesis has been focused for pursuing the cost-effective pathway to produce high efficiency photovoltaic devices. Especially the availability to form the thin film structure on flexible substrate would be the great advantage of electrochemical process. The successful synthesis of the most favorable absorber materials such as CdTe and CIGS has been reported by many researchers, however, the efficiency of electrochemically synthesized could not exceed that from vacuum process, because of microstructural controllability and compositional variation on devices. In this study, we represent the effect of process parameters on the microstructure and composition of compound semiconductor during the synthesis, and propose the photovoltaic characteristics of electrochemically synthesized solar cells.

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Development of Enzyme Immobilization Method to Remove Interference by Physiological Chemicals for Implantable Glucose Sensors (이식형 혈당 센서의 생리활성 물질에 의한 방해 효과를 제거하기 위한 새로운 효소고정법 개발)

  • Chung, T.D.;Kim, H.C.
    • Proceedings of the KOSOMBE Conference
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    • v.1998 no.11
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    • pp.72-73
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    • 1998
  • A new method for enzyme immobilization has been developed to remove interference by potential interferents in body fluids. Instead of using electron mediators, we chose direct hydrogen peroxide measurement route. Extremely hydrogen peroxide-selective polymer was coated as an inner membrane to exclude interferents and then glucose oxidase(GOx) was entrapped by electropolymerization of inert monomers. There was no solvent casting step throughout the whole fabrication procedure but all membranes on Pt-Ir electrode were formed by electropolymerization. Thus, membrane thickness, quantity of enzyme loaded and can be controlled by electrochemical parameters. As a result, reproducibility of biosensor characteristics becomes remarkably improved in terms of mass production.

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Alumina Templates on Silicon Wafers with Hexagonally or Tetragonally Ordered Nanopore Arrays via Soft Lithography

  • Park, Man-Shik;Yu, Gui-Duk;Shin, Kyu-Soon
    • Bulletin of the Korean Chemical Society
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    • v.33 no.1
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    • pp.83-89
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    • 2012
  • Due to the potential importance and usefulness, usage of highly ordered nanoporous anodized aluminum oxide can be broadened in industry, when highly ordered anodized aluminum oxide can be placed on a substrate with controlled thickness. Here we report a facile route to highly ordered nanoporous alumina with the thickness of hundreds-of-nanometer on a silicon wafer substrate. Hexagonally or tetragonally ordered nanoporous alumina could be prepared by way of thermal imprinting, dry etching, and anodization. Adoption of reusable polymer soft molds enabled the control of the thickness of the highly ordered porous alumina. It also increased reproducibility of imprinting process and reduced the expense for mold production and pattern generation. As nanoporous alumina templates are mechanically and thermally stable, we expect that the simple and costeffective fabrication through our method would be highly applicable in electronics industry.

Blended Elemental P/M Synthesis of Titanium Alloys and Titanium Alloy-based Particulate Composites

  • Hagiwara, Masuo;Emura, Satoshi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1030-1031
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    • 2006
  • Titanium alloys and Titanium alloy-based particulate composites were synthesized using the blended elemental P/M route. First, processing conditions such as the fabrication of master alloy powder were investigated. Ti-6Al-4V, Ti-5Al-2.5Fe, Ti-6Al-2Sn-4Zr-2Mo, IMI685, IMI829, Timetal 1100 and Timetal 62S, and Ti-6Al-2Sn-4Zr-2Mo/ 10%TiB and Timetal 62S/10%TiB were then synthesized using the optimal processing conditions obtained. The microstructures and mechanical properties such as tensile strength and high cycle fatigue strength were evaluated.

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Solid-state Synthesis of $Mg_2X$ (X=Si, Ge, Sn and Pb) via Bulk Mechanical Alloying

  • Aizawa, Tatsuhiko;Song, Renbo
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.831-832
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    • 2006
  • Solid-state processing via the bulk mechanical alloying enables us to directly fabricate $Mg_2X$ semi-conductive material performs. Precise control of chemical composition leads to investigation on the dilution and enrichment of X in $Mg_2X$. Two types of solid-state reactivity are introduced: e.g. synthesis of $Mg_2Si$ from elemental mixture Mg-Si is nucleation-controlled process while synthesis of $Mg_2Sn$ from Mg-Sn, diffusion-controlled process. Thermoelectricity of these $Mg_2X$ is evaluated for discussion on the validity and effectiveness of this new PM route as a reliable tool for fabrication of thermoelectric compounds.

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