• Applied Chemistry for Engineering
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• v.33 no.5
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• pp.496-501
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• 2022

In this study, an anode material for lithium secondary batteries was manufactured using petroleum-based residual oil, which is a petroleum refining by-product. Among petroleum-based residual oils, pyrolysis fuel oil (PFO), fluidized catalyst cracking-decant oil (FCC-DO), and vacuum residue (VR) were used as carbon precursors. The physicochemical characteristics of petroleum-based residual oil were confirmed through Matrix-assisted laser desorption/ionization Time-of-Flight (MALDI-TOF) and elemental analysis (EA), and the structural characteristics of anode materials manufactured from residual oil were evaluated using X-ray crystallography (XRD) and Raman spectroscopic techniques. VR was found to contain a wide range of molecular weight distributions and large amounts of impurities compared to PFO and FCC-DO, and PFO and FCC-DO exhibited almost similar physicochemical characteristics. From the XRD analysis results, carbonized PFO and FCC-DO showed similar d₀₀₂ values. However, it was confirmed that FCC-DO had a more developed layered structure than PFO in Lc (Length of a and c axes in the crystal system) and La values. In addition, FCC-DO showed the best cycle characteristics in electrochemical characteristics evaluation. According to the physicochemical and electrochemical results of the petroleum-based residual oil, FCC-DO is a better carbon precursor for a lithium secondary battery than PFO and VR.

• The Proceeding of the Korean Institute of Electromagnetic Engineering and Science
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• v.7 no.1
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• pp.4-13
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• 1996

미국 연방통신위원회(FCC)에서는 1996. 5. 14일 부로 Digital Device에 대한 인증제도를 자기입증방식(DoC)으로 변경한다는 방침을 확정, 발표하였다(FCC 96-206, ET Docket No. 95-19, Report and Order). 이 새로운 자기입증제도는 기존 FCC의 타율규제방식(Certification, Verification, Notification등) 을 탈피하여 제조자 자율에 의한 인증개념을 도입한 것으로서, 어떤 제품(Digital Device에 대해서 FCC가 정한 기술기준에 의거 시험하여 합격하였을 경우, 제조자(인증권자) 스스로 적합선언서 (DoC : Declaration of Conformity)를 채택하고 해당 제품에 인증마크를 부착하여 출하시킨다는 것으로 기존 EU의 CE-Mark 인증제도 중 Module A와 유사한 제도이다. FCC는 이와 같은 제도변경을 위해서 1995년 2월에 이미 기본방침을 발표하여 그동안 관련업계 의 광범위한 의견수렴을 거쳤으며, 필요한 법적보완사항을 위해서 일부 통신법을 개정, 완료하였 고(1996 통신법 403(f), 상무성, NIST 등 관계기관과의 의견조정을 마친 후 본 시행안을 확정, 공표 하였다.

• Carbon letters
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• v.2 no.2
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• pp.99-104
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• 2001

Partial mesophase (PM) pitch precursor was prepared from fluidized catalytic cracking-decant oils (FCC-DO) by chemical reaction in the presence of $Br_2$. The PM pitch heated-treatment at $420^{\circ}C$ for 9 h exhibited the softening point of $297^{\circ}C$ with 23% yield, and 55% anisotropic content. The PM pitch precursor was melt-spun through circular nozzle by pressurized $N_2$, stabilized at $310^{\circ}C$, carbonized at $700^{\circ}C$, $1000^{\circ}C$, and $1200^{\circ}C$. The enough stabilization introduced 16.4% of the oxygen approximately. The stacking height ($L_{c002}$) and interlayer spacing ($d_{002}$) of the as-spun fibers were 4.58 nm and $3.45{\AA}$ and the value became minimum and maximum at $700^{\circ}C$ respectively in the carbonization procedure. The tensile strength increased with an increase in the heat treatment temperature exhibiting highest value of 750 MPa at $1200^{\circ}C$ carbonization.

• Proceedings of the Korea Air Pollution Research Association Conference
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• 2008.10a
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• pp.196-198
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• 2008

• Applied Microscopy
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• v.45 no.1
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• pp.9-15
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• 2015

In the present study, microstructural evolution in CuCrFeNi, CuCrFeNiMn, and CuCrFeNiMnAl alloys has been investigated. The as-cast CuCrFeNi alloy consists of a single fcc phase with the lattice parameter of 0.358 nm, while the as-cast CuCrFeNiMn alloy consists of (bcc+fcc1+fcc2) phases with lattice parameters of 0.287 nm, 0.366 nm, and 0.361 nm. The heat treatment of the cast CuCrFeNiMn alloy results in the different type of microstructure depending on the heat treatment temperature. At $900^{\circ}C$ a new thermodynamically stable phase appears instead of the bcc solid solution phase, while at $1,000^{\circ}C$, the heat treated microstructure is almost same as that in the as-cast state. The addition of Al in CuCrFeNiMn alloy changes the constituent phases from (fcc1+fcc2+bcc) to (bcc1+bcc2).

• Advances in concrete construction
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• v.14 no.1
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• pp.1-13
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• 2022

Due to the physical-chemical characteristics of some bottom ash (BA), there are technical, economic and environmental limitations to find a destination that will add value to it. In Brazil, this residue is eventually used for filling coal extraction pits or remains in sedimentation ponds, creating a susceptible panorama to environmental issues. The geopolymers binders are one of the alternatives to the proper use high amounts of these materials. In this work, geopolymeric binder pastes were produced with BA mixed to activators with different alkali contents (expressed as %Na₂O), as well as the incorporation of soluble silicates (Ms content). The production of binary geopolymeric pastes based on the use of two industrial wastes: fluid catalytic cracking (FCC) and aluminum anodizing sludge (AAS), was also assessed. The content in mass of BA/FCC and BA/AAS ranged from 100/0, 90/10; 80/20 and 70/30. Systems with soluble silicates as activator in a molar ratio SiO₂/Na₂O of 1.0 (Ms = 1.0) and Na₂O content of 15%, showed the best results of mechanical strength (42 MPa at day 28^th). The improvement is up to 5X when compared to NaOH based systems. For systems with partial replacement of BA of 10% of AAS and 20% of FCC (80/20), the presence of soluble silicates was also effective to increase compressive strength.

• Journal of Aerospace System Engineering
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• v.17 no.1
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• pp.33-41
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• 2023

As seen in the case of the Boeing 737 Max accident, the proportion of aircraft software is rapidly increasing. However, it is vulnerable to safety issues. In case of domestic aircraft software, to operate a Light Unmanned Aerial Vehicle (LUAV) less than an empty weight of 150 kg, safety certification is required for an Ultra-Light Vehicle (ULV). However, software certification procedure is not included. Since the use of LUAVs has increased recently, software verification is required. This paper proposed a checklist of LUAV software that could be applied to LUAV referring DO-178C, an aviation software certification standard. A case study of applying the proposed checklist to the Model-based Development-based Helicopter Flight Control Computer (FCC) project currently used by domestic and foreign advanced companies and institutions was conducted.

• Proceedings of the Korean Vacuum Society Conference
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• 2011.08a
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• pp.185-185
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• 2011

서로 결정구조가 다른 물질 사이의 계면을 연구하기 위해 실온에서 W(bcc) 표면에 Al(fcc)를 성장시켜, 그 흡착구조를 연구하였다. 실온에서 W(110)면에 Al원자를 0.5 ML, 1.0 ML, 2.0 ML, 3.0 ML과 4.0 ML으로 증착시켜 Al/W(110)계의 흡착구조를 저에너지 전자회절(LEED)을 이용하여 관찰하였고, 각 coverage의 Al/W(110)계에서 이온산란분광법(CAICISS-TOF)을 이용하여 흡착구조를 연구하였다. 연구결과, Al의 coverage가 증가함에 따라 표면의 Al이 crystal되어, 4.0 ML Al/W(110)계에서 Al은 6-fold symmetry를 이루는 fcc 구조의 (111)면으로 성장하였으며 성장된 Al(111)면의 [T10]방향과 [1T0]방향이 substrate인 W(110)면의 [001]방향과 서로 평행한 double domain의 표면구조이다.

• Journal of the Korean Magnetics Society
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• v.12 no.4
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• pp.132-136
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• 2002

Enhancement of crystallinity and exchange bias characteristics for NiFe/FeMn/NiFe trilayer with Si buffer layer fabricated by ion-beam deposition were examined. A Si buffer layer promoted (111) texture of fcc crystallities in the initial growth region of NiFe layer deposited on it. FeMn layers deposited on Si/NiFe bilayer exhibited excellent (111) crystal texture. The antiferromagnetic FeMn layer between top and bottom NiFe films with the buffer Si 50 ${\AA}$-thick induced a large exchange coupling field Hex with a different dependence. It was found that H$\sub$ex/ of the bottom and top NiFe films with Si buffer layer revealed large value of about 110 Oe and 300 Oe, respectively. In the comparison of two Ta and Si buffer layers, the NiFe/FeMn/NiFe trilayer with Si could possess larger exchange coupling field and higher crystallinity.

• Applied Microscopy
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• v.45 no.1
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• pp.32-36
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• 2015

The microstructural features of FeCoCrNi, FeCoCrNiAl and FeCoCrNiSix (x=0, 5, 10, 15, 20) alloys have been investigated in the present study. The microstructure of FeCoCrNi alloy changes dramatically with equiatomic addition of Al. The fcc irregular shaped grain structure in the as-cast FeCoCrNi alloy changes into the bcc interconnected structure with phase separation of Al-Ni rich and Cr-Fe rich phases in the as-cast FeCoCrNiAl alloy. The microstructure of FeCoCrNi alloy changes with the addition of Si. With increasing the amount of Si, the fcc structure of the grains is maintained, but new phase containing higher amount of Si forms at the grain boundary. As the amount of Si increases, the fraction the Si-rich grain boundary phase increases.