• Proceedings of the Materials Research Society of Korea Conference
• /
• 2010.05a
• /
• pp.41.2-41.2
• /
• 2010

In this work, HAp-(t-ZrO2) ceramic composites of biomimic artificial bone were fabricated by multi-extrusion process in order to replace nature bone. HAp-(t-ZrO2) and graphite powders were mixed separately with ethylene vinyl acetate (EVA) and stearic acid using shear mixer. Extruded HAp-(t-ZrO2) filaments and carbon filaments were arranged in the die to fabricate the first pass filament. The first pass filaments were arranged in the same die with a central carbon core for making the space for spongy bone. Burning out and sintering processes were performed to remove the binder and lubricant. The microstructure channel diameter was researched around $300{\mu}m$. Microstructure analysis was carried out by OM, SEM, and $\mu$-CT. Compressive strength was investigated for the artificial bone. Some preliminary bio-compatibility test was evaluated.

• Journal of Pharmaceutical Investigation
• /
• v.5 no.1
• /
• pp.41-48
• /
• 1975

Extrusion-Spheronization Processing (ESP) was applied to preparate sustained release spherical particles as a form of matrix spherical particle (MSP). dl-methylephedrine HCI (ME) was the drug chosen and several dissolution retardants and binders were selected to estimate a relatively good formulation on this purpose. The effect of physicochemical nature, concentration, and solvents of these dissolution retardants and binders on regularity in shape of MSP and in vitro release rate was investigated. The effect of Particle size of matrix particles was also evaluated. It is, therefore, concluded that this ESP would be a relatively good preparation method of sustained release MSP of ME which has the sustained action of about 5 and 8 hours by formulating of ethylcellulose and ethylcellulose-paraffin as a dissolution retardant, respectively, and then ethylcellulose solution of 80% EtOH is recommended as a binder.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2006.09a
• /
• pp.495-496
• /
• 2006

The kneading process and formulations of feedstock obviously affect the quality of MIM products. In the present work, the rheological behaviour of the composite MIM feedstock, metal matrix (Cu) with few additions of ceramic powders $(Al_2O_3)$, was measured by a self-designed/manufactured simple capillary rheometer. Experimental results show that the distribution between powders and binder is more uniformly when blending time increased. Though high powder loading will increase the feedstock viscosity, the fluidity reveals relatively stable through the load curves of extrusion. Besides, the temperature-dependence of viscosity of the feedstock approximately follows an Arrehnius equation. Basing on Taguchi's method, the kneading optimization conditions and the rheological model of the feedstock were established, respectively.

• Journal of the Korean Ceramic Society
• /
• v.42 no.4
• /
• pp.260-268
• /
• 2005

A heat-resisting diatomite protection tube, using diatomite as a main component, was manufactured through an extrusion molding of ceramic slurry in different component ratios. And its mechanical strength, carbon analysis and microstructural non-homogeneity were investigated. After fixing $60wt\%$ of porous diatomite whose particle size was $50\~100\;{\mu}m$, the optimum mixture ratio with composition variables by changing $1\;wt\%$ of each component that was silica sol$(4.3\~7.3\;wt\%)$ as an inorganic binder, CMC (Sodium CarboxyMethyl Cellulose $(6\~9\;wt\%)$) as an organic binder and paper powder$(4.7\~7.7\;wt\%)$ was obtained. As a result of the investigation on a composition containing $60\;wt\%$ diatomite, $5.3\;wt\%$ silica sol, and $7\;wt\%$ CMC, a heat-resisting protection tube that could be used as a molten steel probe for measuring the temperature and components of molten steel was developed. The bending strength, compressive strength, and elastic modulus of the protection tube developed, that contained $\le2.3\;wt\%$ carbon, were 7.1 MPa, 7.5 MPa, and 1090 MPa, respectively.

• Elastomers and Composites
• /
• v.47 no.2
• /
• pp.121-128
• /
• 2012

Waste EPDM(W-EPDM) collected from the automotive weather strip and the gasket of a laundry machine has not been effectively recycled. Using this W-EPDM powder and other ingredients, i.e., binder(polyolefin resin, polyolefin elastomer, etc.), filler and additives, various economic rubber composites were made by extrusion. In advance of main experiments, the effects of ultrasonic treatment of W-EPDM on the property of rubber composites, comparison in the property of the composites of W-EPDM with those of virgin and devulcanized EPDM, and waste tire rubber were investigated. Also, the properties of the rubber composites extruded with a 12-screw extruder were compared with those extruded with twin-screw extruder. Various W-EPDM composites for synthetic turf filler and car mat were extruded and injection molded, and 3 main properties of tensile strength, elongation and hardness were investigated to develop economical and proper recipes of the rubber composites.

• Journal of the Korea institute for structural maintenance and inspection
• /
• v.23 no.7
• /
• pp.104-112
• /
• 2019

The material properties of the 3D printing cement composite mortar were evaluated, and the performance range in which printing was possible was calculated using the void ratio in a fresh state as a single index. As a results of the tests, as the water-binder ratio (W/B) increased, the mortar flow value increased and the density and strength decreased. As the sand-binder ratio (SS/B) increased, the mortar flow value decreased. However, strength and density increased and decreased up to a certain SS/B. As admixture-binder ratio (Ad/B) increased, mortar flow value, density, and strength decreased. These trends make it difficult to mix-design to meet the target performances of 3D printing mortars, represented by extrudability and buildability. The value of mortar flow increased proportionally with the void ratio, while the density and strength apparently decreased as the void ratio increased. This indicates that void ratio can be utilized as a single index for controlling the material properties in the design of mortar mixtures. It was found that mortar mixture could be printed by a 3D printer when the void ratio was in the range from 0.6 to 0.7. This was verified by printing a mortar which has the void ratio of 0.634. The mortar was produced with the mixture design of W/B 35.0%, SS/B 60.0%, and Ad/B 0.1%. Further research applying diverse admixtures is needed to improve the quality of 3D printing output mortars.

• Clean Technology
• /
• v.24 no.2
• /
• pp.119-126
• /
• 2018

This study introduced a treatment process that was developed to treat Indonesian low-rank coal with high-ash content, which has the same characteristics as residual coal from the biosolubilization process. The treatment process includes separation of ash, solid-liquid separation, pelletizing, and drying. To reduce the ash content, flotation was performed using 4-methyl-2-pentanol (MIBC) as frother, and kerosene, waste oil, and cashew nut shell liquid (CNSL) as collectors. The increasing amount of collector had an effect on combustible coal recovery and ash reduction. After flotation, a filter press, extruder, and an oven drier were used to make a dried coal pellet. Then another coal pellet was made using asphalt as a binder. The compressive strength and friability of the coal pellets were tested and compared.

• KIEAE Journal
• /
• v.12 no.3
• /
• pp.107-114
• /
• 2012

This is a study that surveyed and analyzed the present status of producing loess construction materials in Korea from 2006 to 2011. The findings are as follows. 1) More than 70% of loess construction material manufacturers are distributed in the capital area. Chungcheong-do and Gyeonggi-do are grown by about 20% on the annual average. 2) Shape of loess brick is possessed mostly by a rectangular parallelepiped. A hole shape, which has 1~5 holes among these things, is possessing a majority. 3) It was indicated to be 42 days as material age for the compressive strength, to be about 2.7Mpa for both extrusion and compression, and to be about 30% for absorptance. 4) Among the whole loess material manufacturers, it accounts for 87 for loess brick 66% for loess mortar and more than 39% for loess paint, but within 10%~15% for other loess products. 5) The main specifications of loess brick are $300{\times}150{\times}150,\;300{\times}150{\times}100,\;300{\times}200{\times}150,\;300{\times}150{\times}200$ in order of the output of 74kinds of loess bricks. 6) In order to improve the strength of building materials, mortar and concrete used loess, it is necessary to examine closely about the effect of ceramic binder and cement on loess products.

• Journal of Korean Society of Occupational and Environmental Hygiene
• /
• v.30 no.2
• /
• pp.153-162
• /
• 2020

Objectives: 3D printing technologies have become widely developed and are increasingly being used for a variety of purposes. Recently, the evaluation of 3D printing operations has been conducted through chamber test studies, and actual workplace studies have yet to be completed. Therefore, the objective of this study was to determine the emission of volatile organic compounds(VOCs), metals, and particles from printing operations at a workplace. This included monitoring conducted at a commercial 3D printing service workplace where the processes involved material extrusion, material jetting, binder jetting, vat photo polymerization, and powder bed fusion. Methods: Area samples were collected with using a Tenax TA tube for VOC emission and MCE filter for metals in the workplace. For particle monitoring, Mini Particle Samplers(MPS) were also placed in the printer, indoor work area, and outdoor area. The objective was to analyze and identify particles' size, morphology, and chemical composition using transmission electron microscopy with energy dispersive spectroscopy(TEM-EDS) in the workplace. Results: The monitoring revealed that the concentration of VOCs and metals generated during the 3D printing process was low. However, it also revealed that within the 3D printing area, the highest concentration of total volatile organic compounds(TVOC) was 4,164 ppb at the vat photopolymerization 3D printing workplace, and the lowest was 148 ppb at the material extrusion 3D printing workplace. For the metals monitoring, chromium, which, is carcinogenic for humans, was detected in the workplace. As a characteristic of the particles, nano-sized particles were also found during the monitoring, but most of them were agglomerated with large and small particles. Conclusions: Based on the monitoring conducted at the commercial 3D printing operation, the results revealed that the concentration of VOCs and metals in the workplace were within Korea's occupational exposure limits. However, due to the emission of nano-sized particles during 3D printing operations, it was recommended that the exposure to VOCs and metals in the workplace should be minimized out of concern for workers' health. It was also shown that the characteristics of particles emitted from 3D printing operations may spread widely within an indoor workplace.

• Korean Journal of Materials Research
• /
• v.16 no.3
• /
• pp.188-192
• /
• 2006

The microstructures and mechanical properties of continuously porous $SiC-Si_3N_4$composites fabricated by multi-pass extrusion were investigated at different Si levels added. Si-powder with different weight percentages (0%, 5%, 10%, 15%, 20%) was added to the SiC powder to make the raw mixture powders, with $6wt%Y_2O_3-2wt%Al_2O_3$ as sintering additives, carbon ($10-15{\mu}m$) as a pore-forming agent, ethylene vinyl acetate as a binder and stearic acid ($CH_3(CH_2)_{16}COOH$) as a lubricant. In the continuously porous $SiC-Si_3N_4$ composites, $Si_3N_4$ whiskers like the hairs of nostrils were frequently observed on the wall of the pores. In this study, the morphology of the $Si_3N_4$ whiskers was investigated with the silicon addition content. In the composites containing of 10 wt% Si, a large number of $Si_3N_4$ whiskers was found at the continuous pore regions. In the sample to which 15 wt% Si powder was added, maximum values of about 101 MPa bending strength and 57.5% relative density were obtained.