• 제목/요약/키워드: Extraction methods

검색결과 3,457건 처리시간 0.047초

참외 시설재배 토양에 대한 유효규산 추출방법 비교 (Evaluation of Available Soil Silicon Extracting Procedures for Oriental Melon)

  • 조현종;최희열;이용우;정종배
    • 한국토양비료학회지
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    • 제37권4호
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    • pp.251-258
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    • 2004
  • 밭작물에 대한 규산질 비료의 시용이 널리 이루어지고 있으나 적정시용수준이 밝혀져 있지 못하며 또한 밭토양에서의 유효규산 측정방법이 구명되어있지 못한 실정이다. 본 연구는 참외 시설재배지 토양에 대하여 유효규산 측정방법을 구명하기 위해 수행되었다. 경북 성주지역의 참외 시설재배지,10개소의 토양과 참외 잎 시료를 채취하여 가용성 토양 규산 함량과 잎 중의 총 규산 함량을 분석하였다. 가용성 토양 규산은 0.5 N HCI, 1 N sodium acetate buffer (pH 4.0). citric acid 1%, water, Tris buffer (pH 7.0), 그리고 1주간 담수하는 방법 등으로 추출하였으며, 식물체 규산은 autoclave 방법으로 추출하였다. 추출액중의 가용성 규산은 비색법으로 정량하였다. 각 추출방법별로 가용성 토양규산 함량과 식물체규산 함량과의 관계를 비교하였는데, 1 N sodium acetate buffer 방법이 토양 규산과 식물체 규산 관계를 가장 뚜렷한 포화곡선으로 나타내었다. 포화곡선으로부터 산출된 참외 잎 중의 포화 규산 함량은 약 $14g\;SiO_2\;kg^{-1}$이었고 1 N sodium acetate buffer 방법으로 추출할 경우토양 규산 함량 $120mg\;SiO_2\;kg^{-1}$이 참외에 적정한 수준인 것으로 나타났다. 특히 1 N sodium acetate buffer방법의 경우 참외 잎 중의 규산 함량이 포화되는 수준 이하의 토양 규산 함량 범위에서는 토양 규산 함량과 식물체 규산 함량 사이에 유의성 있는 상관관계가 있었다. 따라서 현재 우리나라에서 논토양의 유효규산 측정방법으로 널리 사용퇴고 있는 1 N sodium acetate buffer를 이용한 유효규산 추출방법이 밭토양에도 적용될 수 있을 것으로 판단되나 앞으로 다양한 작물과 토양을 대상으로 계속적인 연구가 요구된다.

하악 제3대구치 발치를 위한 예방적 항생제의 효용성 (THE EFFICACY OF PROPHYLACTIC ANTIBIOTICS FOR MANDIBULAR THIRD MOLAR EXTRACTION)

  • 강상훈;김정인;박원서;이충국;이상휘
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • 제34권3호
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    • pp.365-369
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    • 2008
  • This study analyzed the incidence of wound infection after the operation of mandibular third molar extraction in relation with antibiotic prophylaxis with the object of young and healthy patients. The study object was 1,177 mandibular third molars of 850 men of 20 to 25 years old without any specific systemic disease. Three methods of preventive antibiotic medication were selected according to the preventive antibiotic medication previously reported; three experimental groups were selected based on them, and the antibiotic used was amoxicillin($^{(R)}Kymoxin$, Yuhanyanghaeng, Seoul). The group 1 includes the patients that took the antibiotic orally before the operation(one hour earlier, 500mg) and for three days after the operation(250mg per time, three times/day), the group 2 is the ones that took the same antibiotic orally only once about one hour before the operation(500mg), and the group 3 did not take any antibiotics before and after the operation. And to compare the difficulties and the degrees of extraction during operations which can be possibly related to the wound infection after the operations, the mandibular third molars' impacted depths and extraction methods were investigated as well. To check if the wound was infected, observations with an internal of one week were performed twice after the operation, and the meaningfulness of the infection incidence was verified through Chi-square test using SPSS program(SPSS Inc., IL, USA). There was no statistically significant difference between the antibiotic medication methods and the wound infection incidence after the operation among the experimental groups. As examining the relations between the mandibular third molar operation methods and the wound infection incidence after the operation, there existed a statistically meaningful difference in the infection incidence according to the operation methods(p=0.020). And there was no statistically significant difference in the wound infection incidence according to the impacted depth of the mandibular third molar. Therefore, it is thought that there exists little necessity of prophylatic antibiotics medication when extracting the mandibular third molar of young and healthy men without any systemic disease in general; however, in case when it is expected that the possibility of infection will be high or the wound on the tissue will be severe, it is sure that the prophylactic antibiotics medication will be necessary.

추출조건에 따른 해조류의 알긴산 수율과 점도 (Comparison of Alginic Acid Yields and Viscosity by Different Extraction Conditions from Various Seaweeds (Laminaria religiosa, Hizikia fusiforme, and Undaria pinnatifida))

  • 윤미옥;이승철;임종환;김정목
    • 한국식품영양과학회지
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    • 제33권4호
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    • pp.747-752
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    • 2004
  • HWEM(hot-watele material ), WSA(water soluble alginate), ASA(alkali soluble alginate), AASA(acid alkali soluble alginate)의 네 가지 알긴산 추출방법을 이용해서 다시마(Laminaria religiosa), 미역(Undaria pinnatifida), 톳(Hizikia fusiforme)의 3가지 시료를 가지고 알긴산을 추출하여 수율을 알아본 결과 사용된 시료 중에서 AASA추출방법에 의한 미역에서의 알긴산 함량이 39.6%로 가장 우수하게 나타났으며 HWEM은 10.2∼18.6% 정도의 수율로 AASA 방법으로 얻은 수율보다 절반밖에 미치지 못하였다. 제조된 알긴산 분말의 색도는 다시마로부터 WSA추출법을 이용해서 제조한 알긴산의 ΔE값이 20.63으로 가장 밝게 나왔으며 추출에 사용된 모든 시료들에 있어서 WSA추출방법에 의한것이 밝은 색도를 가지며 ASA 추출방법을 이용해서 얻은 알긴산의 색도는 ΔE값이 75.31로 다른 것에 비해 어두운 색의 알긴산이 제조되었다. AASA 추출방법에서 3% $Na_2$CO$_3$ 농도에서 37.1%로 높은 수율을 얻을 수 있었으며, H$_2$SO$_4$의 농도를 0.1, 0.2, 0.4 N로 변화시켜서 추출한 결과는 0.4 NH$_2$SO$_4$에서 34.9%의 높은 수율을 나타냈다. 톳에서 추출한 알긴산의 점도는 상업용에 비해 훨씬 낮은 점도를 나타내었으며 ASA추출 방법에 의해 얻어진 알긴산의 점도가 WSA에 의한 것보다 높은 점성을 나타내었다.

사용자 인터페이스 에이전트를 통한 정보추출 규칙의 자동 생성 (Automatic Generation of Information Extraction Rules Through User-interface Agents)

  • 김용기;양재영;최중민
    • 한국정보과학회논문지:소프트웨어및응용
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    • 제31권4호
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    • pp.447-456
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    • 2004
  • 정보추출은 한 문서에서 그 문서의 중심적 의미를 나타내는 특정 구성요소를 인식하여 추출하는 작업으로서, 이질적인 여러 정보소스로부터 균일화된 정보추출을 수행하기 위해서는 각 정보소스에 맞는 정보추출 규칙을 생성해야 한다. 기존 정보추출 규칙의 생성 방법에는 전문가에 의한 수동 생성 방법과 에이전트 프로그램에 의한 자동 생성 방법이 있는데, 수동 생성은 규칙의 정확성은 보장되나 확장성과 효율성에 문제가 있고, 자동 생성은 확장성은 있으나 규칙 생성 자체의 어려움과 생성된 규칙의 신뢰성이 문제점으로 대두된다. 본 논문에서는 이러한 두 가지 방법의 문제점을 보완하여 추출 규칙의 정확성과 확장성을 동시에 제공하기 위해 지도 학습(supervised teaming)을 적용한 정보추출 규칙 생성 기법을 제안한다. 본 논문에서 제시하는 방법은 사용자 인터페이스 에이전트를 사용하여 정보추출 규칙 생성을 위한 단서 정보를 사용자로부터 받고 이 정보를 바탕으로 에이전트가 XML로 표현된 규칙을 생성하는 것이다. 결과적으로 정보추출 규칙의 수동 생성과 자동 생성을 혼합한 형태가 된다. 사용자 인터페이스 에이전트는 규칙의 생성 뿐 아니라 기존의 규칙을 수정하거나 확장하는데도 이용된다. 구인 광고와 논문모집 공고와 관련된 정보소스에 대해 이 방법을 테스트한 결과 다른 기법에서 추출하지 못했던 정보를 추출할 수 있었고, 성능 면에서도 80% 이상의 정확도와 재현 율을 보였다. 본 시스템은 추후 정보 중재자 에이전트와 같은 응용 분야에 적용시킬 수 있을 것으로 기대한다.

Phytochemical analysis of Panax species: a review

  • Yang, Yuangui;Ju, Zhengcai;Yang, Yingbo;Zhang, Yanhai;Yang, Li;Wang, Zhengtao
    • Journal of Ginseng Research
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    • 제45권1호
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    • pp.1-21
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    • 2021
  • Panax species have gained numerous attentions because of their various biological effects on cardiovascular, kidney, reproductive diseases known for a long time. Recently, advanced analytical methods including thin layer chromatography, high-performance thin layer chromatography, gas chromatography, high-performance liquid chromatography, ultra-high performance liquid chromatography with tandem ultraviolet, diode array detector, evaporative light scattering detector, and mass detector, two-dimensional high-performance liquid chromatography, high speed counter-current chromatography, high speed centrifugal partition chromatography, micellar electrokinetic chromatography, high-performance anion-exchange chromatography, ambient ionization mass spectrometry, molecularly imprinted polymer, enzyme immunoassay, 1H-NMR, and infrared spectroscopy have been used to identify and evaluate chemical constituents in Panax species. Moreover, Soxhlet extraction, heat reflux extraction, ultrasonic extraction, solid phase extraction, microwave-assisted extraction, pressurized liquid extraction, enzyme-assisted extraction, acceleration solvent extraction, matrix solid phase dispersion extraction, and pulsed electric field are discussed. In this review, a total of 219 articles published from 1980 to 2018 are investigated. Panax species including P. notoginseng, P. quinquefolius, sand P. ginseng in the raw and processed forms from different parts, geographical origins, and growing times are studied. Furthermore, the potential biomarkers are screened through the previous articles. It is expected that the review can provide a fundamental for further studies.

지상 레이저 스캐닝 기술을 이용한 도로 기하정보 추출 (Extraction of Geometric Information on Highway Using Terrestrial Laser Scanning Technology)

  • 이종출;이병걸;김진수
    • 한국측량학회:학술대회논문집
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    • 한국측량학회 2007년도 춘계학술발표회 논문집
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    • pp.379-382
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    • 2007
  • Laser scanning technology with high positional accuracy and high density automation will be widely applied in vast range of fields including geomatics. Especially, the development of laser scanning technology enabling long range information extraction is increasing its full use in civil engineering. The purpose of this study is to extract accurate highway geometric information taking the advantages of scanning technology. Fulfilling this goal, the information of target highway's three-dimensional data was obtained through terrestrial laser scanning technology. In accordance with the result from target highway's geometric information extraction using the information above, laser scanning technology showed faster speed and better accuracy on highway geometric information extraction with reduced cost compared to traditional methods.

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양파껍질과 양파육질의 용매추출물에 따른 항산화 효과 (Antioxidant Effects on various solvent extracts from Onion Peel and Onion Flesh)

  • 조정순;방현아
    • 대한영양사협회학술지
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    • 제4권1호
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    • pp.14-19
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    • 1998
  • This study was designed to investigate the role of onion as a natural antioxidant. Onion was distinguished as yellow onion peel and onion flesh. Onion samples were extracted with 5 different kinds of solvents such as water, 70% ethanol, 99.9%ethanol, 99.9% methanol, and 96% butanol in order to select optimal extraction solvents, In this part of study linoleic acid was used s an model system for the purpose of determining the antioxidant activities. The optimal extraction rate of various solvents containing onion samples was determined by measuring extraction yield, electron donating ability(EDA), thiobarbituric acid(TBA), and thiocyanate, which are common methods for measuring activity. As a result 70% ethanol was shown as the most effective solvent.

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Applications of carbon-based materials in solid phase micro-extraction: a review

  • Guo, Jian;Park, Soo-Jin;Meng, Long-Yue;Jin, Xinghua
    • Carbon letters
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    • 제24권
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    • pp.10-17
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    • 2017
  • With continuous development in the field of sample preparation technology, solid phase micro-extraction (SPME) has been widely used in analytical chemistry for high extraction efficiency and convenient operation. Different materials lead to different extraction results. Among existing materials, carbon-based materials are still attracting attention from scientists due to their excellent physical and chemical properties as well as their modifiable surfaces, which could enhance the adsorption effects of SPME fiber. This review introduces the preparation methods and applications of different kinds of carbon-based material coatings on fibers. In addition, directions for future research on carbon material composites are discussed.

휴대폰과 스마트폰의 모바일 포렌식 추출방법 연구 (A Study on Mobile Forensic Extraction Methods of Cellular and Smart Phone)

  • 이정훈;박대우
    • 디지털산업정보학회논문지
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    • 제6권3호
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    • pp.79-89
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    • 2010
  • Cellular and Smart phone through the business and real life is associated with an increasing number of information processing, Breaches associated with mobile terminal Tile has occurred and cause Crime and damage. In this paper, Cellular and Smart phone for mobile forensics SYN scheme and JTAG scheme to target Cellular and Smart phone for the extraction of forensic data will be studied. SYN, JTAG approach to forensic analysis indicate with the process, Every Smart phone's OS specific performance and data extraction were compared. In the laboratory, Cell and smart phone with the SYN scheme and JTAG scheme to extract forensic data Improvement compared to the extraction is presented.

ICP-AES를 이용한 전처리방법에 따른 환경시료내 Pb, Cd의 측정 비교 연구 (A comparative measurement study of Pb, Cd using ICP-AES with different pretreatment methods)

  • 권태영;윤춘경;전지홍
    • 한국농공학회:학술대회논문집
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    • 한국농공학회 1998년도 학술발표회 발표논문집
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    • pp.513-520
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    • 1998
  • The evaluation of uncertainty in environmental elemental analysis can be difficult because of the wide variety of analytical sample and objectives. for the specification of measured, elemetal analysis need certain method and high pretreatment technique. The sample of Pb, Cd in paddy soil and sewage sludge were analyzed by same ICP-AES, but each using four different pretreatment technique ; 0.1N HCl extraction, AB-DTPA extraction and two Mixture Acid Digestion. The four technique gave comparable results for the analysis of lead and cadmium. Concentrations determined by Mixture Acid Digestion were more higher than those by 0.1NHCI extraction and AB-DTPA extraction.

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