• Title/Summary/Keyword: Energy dispersive spectrometer

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Experimental Analysis on Particle Growth in TEOS/O2 Plasma Reactor (TEOS/O2용 플라즈마 반응기에서의 미립자 성장에 대한 실험적 분석)

  • Hong, Sung-Taik;Kim, Kyo-Seon
    • Journal of Industrial Technology
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    • v.23 no.A
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    • pp.175-179
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    • 2003
  • A study on the particle growth in $TEOS/O_2$ plasma was performed by observing the particle size and its morphology by TEM. The qualitative chemical analysis of particles was also determined by the EDS (Energy Dispersive X-Ray Spectrometer). The effects of process variables such as the plasma on-time and bubbler temperature on the particle growth were investigated. The particle size becomes larger as the plasma on-time because of the longer coagulation, and also as the bubbler temperature increases because of the faster coagulation between particles.

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The frequency and magnetic characteristics of YIG with the variation of $Al_2O_3$ additions ($Al_2O_3$조성변화에 따른 YIG의 주파수 및 자기특성)

  • 홍기원;김명호;장경욱;이준웅
    • Electrical & Electronic Materials
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    • v.8 no.6
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    • pp.787-794
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    • 1995
  • To improvement the magnetic and frequency properties of YIG(Yttrium-Iron Garnet) in microwave region, it is investigated that the effect of $Al^{3+}$ ions on magnetic and frequency characteristics of YIG, using samples of basic YIG composition( $Y_{3}$F $e_{5}$ $O_{l2}$) added with A1$_{2}$ $O_{3}$ from 0 to 2.5 [mol%]. The measurment is conducted mainly for the structural properties and magnetical properties. The structural properties is measured using SEM(Scanning Electro Microscope), EDX(Energy-dispersive X-ray spectrometer) and XRD(X-ray diffraction equipment). The magnetical properties is measured with B-H curve tracer and impedance analyzer. As a result, it is confin-ned that the effect of eddy current loss is minimized while maintaining high saturation flux density of YIG, when YIG is added with 0.5 [mol%] of A1$_{2}$ $O_{3}$.>.>.

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Evaluation of Microstructure and Mechanical Property of Inconel 600 Degraded under High Temperature (고온 열화된 Inconel 600강의 미세조직 및 기계적 특성 평가)

  • Jung, Kwang-Hu;Kim, Seong-Jong
    • Journal of the Korean institute of surface engineering
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    • v.50 no.6
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    • pp.492-497
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    • 2017
  • In this study, we investigated the effect of thermal aging on mechanical characteristics of Inconel 600 nickel-based alloy. The thermal aging was conducted up to 1000 hours at an atmosphere of $650^{\circ}C$. The microstructure of thermally aged specimens was investigated by an optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectrometer (EDS). In addition, tensile test (strain rate: 2 mm/min) and micro Vickers hardness test were conducted to evaluate mechanical properties with time. As a result of the experiment, Cr-rich carbide continuously precipitated during thermal aging, leading to the change of the mechanical characteristics and fracture mode. With the increase of aging time, tensile strength, yield strength, and hardness gradually decreased. The fracture mode changed from ductile to brittle with the increase of grain boundary carbide.

Corrosion of Quartz Crystal Marine Sensors in Sea Water (항만센서용 수정진동자의 해수에 의한 부식)

  • 최광재;장상목;김영한
    • Journal of Korean Port Research
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    • v.12 no.2
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    • pp.323-328
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    • 1998
  • A quartz crystal analyzer is utilized to monitor the corrosion process of an aluminum surface of a quartz crystal for marine sensor by sea water. A quartz crystal having 2000 $\AA$ of aluminum layer is installed in a specially designed cell and is in contact with sea water imitated electrolyte solution. While a constant potential is applied to the cell, the resonant frequency and resonant resistance are simultaneously measured using the quartz crystal analyzer. In addition, surface topographs are taken with an atomic force microscope(AFM) and the element analysis of the surface is conducted using an energy dispersive X-ray spectrometer(EDX). The simultaneous measurement of resonant frequency and resonant resistance during the corrosion process explains the change of surface structure caused by the corrosion. The variation of resonant frequency addresses the amount surface metal dissolution. As a conclusion, it is found that a simple measurement using the quartz crystal analyzer can replace the complex monitoring employing large equipments in the investigation of a corrosion process of sensor surface.

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A Study on Property of Microstructuree for Ba System of Perovskite Structure (페로브스카이형 Ba계열의 미세구조 특성)

  • Song, Min-Jong;Dong, Kyung-Rae;Kim, Chang-Bok;Choi, Seong-Kwan;Park, Yong-Soon
    • Korean Journal of Digital Imaging in Medicine
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    • v.13 no.4
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    • pp.185-189
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    • 2011
  • To assess the prevalence of various radiological reduction methods for childhood intussusception in training hospitals by means of a nationwide phone survey, and to demonstrate recent trends in this area by comparing the findings with those obtained in a survey conducted. $BaTiO_3$ system was prepared by using fabrication of classical conditioning ceramics. Polycrystalline and surface structure characteristics of the specimens were measured by X-ray diffraction, SEM(Scanning Electron Microscopy) and EDAX (Energy Dispersive Spectrometer), respectively.

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The Characteristics of Hetero Junction Using NiCuZn Ferrite and Dielectric for LTCC (LTCC를 위한 NiCuZn 페라이트계와 유전체의 이종접합의 특성)

  • Kim, Nam Hyun;Park, Hyun;Kim, Kyung Nam
    • Journal of the Korean institute of surface engineering
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    • v.45 no.5
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    • pp.188-192
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    • 2012
  • The hetero junction on dielectrics and ferrite for LTCC was prepared by using NiCuZn ferrite. The shrinkage behaviour of ferrite tapes in combination with a dielectric tape was investigated. The characteristics of NiCuZn ferrite were investigated using XRD (X-ray diffractometer), Dilatometer, FE-SEM (Field emission scanning electron microscope), EDS (Energy dispersive spectrometer). NiCuZn ferrite calcined at $700^{\circ}C$ had a good apparent density and initial permeability of magnetic properties. The shrinkage rate of the NCZF700 ferrite and dielectric material was similar. The multilayer revealed dense, uniform morphologies with excellent interface quality. Diffusion of hetero junction such as dielectric and ferrite was not occuring at $900^{\circ}C$.

Analysis of Deposited Dust Particles using SEM/EDX (SEM/EDX 분석법을 이용한 침착먼지에 대한 분석사례)

  • Ha, Eun-Ji;Park, Jeong-Ho
    • Journal of Environmental Science International
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    • v.30 no.3
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    • pp.279-287
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    • 2021
  • In this study, the composition and morphology of deposited dust particles with size ranging from a few to tens ㎛ were investigated using SEM/EDX (scanning electron microscopy with energy dispersive x-ray spectrometer). Then deposited dust particles were classified into 8 groups: quartz, aluminosilicates, ca-rich, Fe/Ti oxide, carbon-rich, industrial particle, Fe-rich, and biogenic particle. The sources of deposited dust were high in the order of aluminosilicates 41% > biogenic 18% > Fe-rich 11% > quartz and C-rich 8% > industrial 7% > Fe/Ti oxide 5% > Ca-rich 1%. In particular, the ratio of biogenic particles was relatively high due to influence of pollen. The ratio of carbon-rich was 11% at YM site, 10% at MD site, and 4% at MO site, and the site close to the large emission source was high.

Ni Nanoparticles-hollow Carbon Spheres Hybrids for Their Enhanced Room Temperature Hydrogen Storage Performance

  • Kim, Jin-Ho;Han, Kyu-Sung
    • Transactions of the Korean hydrogen and new energy society
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    • v.24 no.6
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    • pp.550-557
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    • 2013
  • A glucose hydrothermal method is described for preparing hollow carbon spheres (HCS), which have a regular morphology and a high Brunauer-Emmett-Teller surface area of 28.6 m2/g. Scanning electron microscopy shows that they have thin shells and diameter between 2 and 8 ${\mu}m$. The HCSs were modified for the enhanced room temperature hydrogen storage by employing Ni nanoparticles on their surface. The Ni-decorated HCSs were characterized by X-ray diffraction, transmission electron microscopy coupled with an energy dispersive spectroscope, and an inductively coupled plasma spectrometer, indicating that fine and well-distributed Ni nanoparticles can be accomplished on the HCSs. The hydrogen uptake capacity in HCSs with and without Ni loading was evaluated using a high-pressure microbalance at room temperature under a hydrogen pressure upto 9 MPa. As much as 1.23wt.% of hydrogen can be stored when uniformly distributed Ni nanoparticles are formed on the HCSs, while the hydrogen uptake capacity of as-received HCSs was 0.41 wt.%. For Ni nanoparticle-loaded HCSs, hydrogen molecules could be easily dissociated into atomic hydrogen and then chemically adsorbed by the sorbents, leading to an enhanced capacity for storing hydrogen.

Study of Growth and Temperature Dependence of SnS Thin Films Using a Rapid Thermal Processing (황화급속열처리를 이용한 SnS 박막성장 및 온도의존성 연구)

  • Shim, Ji-Hyun;Kim, Jeha
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.29 no.2
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    • pp.95-100
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    • 2016
  • We fabricated a tin sulfide (SnS) layer with Sn/Mo/glass layers followed by a RTP (rapid thermal processing), and studied the film growth and structural characteristics as a function of annealing temperature and time. The elemental sulfur (S) was cracked thermally and applied to form SnS polycrystalline film out of the Sn percursor at pre-determined pressures in the RTP tube. The sulfurization was done at the temperature from $200^{\circ}C$ to $500^{\circ}C$ for a time period of 10 to 40 min. At ${\leq}300^{\circ}C$, 20 min., p-type SnS thin films was grown and showed the best composition of at.% of [S]/[Sn] $${\sim_=}$$ 1 and [111] preferred orientation as investigated from using XRD (X-ray diffraction) analysis and EDS (energy dispersive spectroscopy) and SEM (scanning electron microscopy), and optical absorption by a UV-VIS spectrometer. In this paper, we report the details of growth characteristics of single phase SnS thin film as a function of annealing temperature and time associated with the pressure and ambient gas in the RTP tube.

Identification of Diachea leucopodia on Strawberry from Greenhouse in Korea

  • Lee, Jung-Han;Han, Ki-Soo;Bae, Dong-Won;Kim, Dong-Kil;Kim, Hee-Kyu
    • Mycobiology
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    • v.36 no.3
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    • pp.143-147
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    • 2008
  • We have detected the slime mold, Diachea leucopodia (GNU06-10) in a strawberry greenhouse located in Sancheong-gun, Gyeongnam. Typical fruiting bodies had developed gregariously on the strawberry leaves, petioles, and plant debris on ground soil habitat, and also surprisingly on plastic pipes and a vinyl covering. Field samples were examined via stereomicroscopy, light microscopy, and SEM for the determination of morphological characteristics. Dark-brown to black spores formed gregariously within the stipitate cylindrical sporangium, and were covered by an iridescent peridium, which may be intact at maturity, or may have disintegrated. The upper portion of the peridium generally breaks up to expose the spores, whereas the lower portion was usually persistent. The results of energy dispersive X-ray spectrometer (EDS) analysis showed that lime was present in the stalk and columella but absent from the spores, capillitium, and peridium. The above characteristics confirm its taxonomic position in the genus Diachea. However, this genus is intermediate in character between the Physarales and Stemonitales of the Myxogastromycetidae. Hence, this genus had been classified as a member of the Stemonitales until the mid-1970's, on the basis of its iridescent peridium and noncalcareous capillitial system, similar to Comatricha of the Stemonitaceae. By way of contrast, emphasis on morphological characteristics, most notably the calcareous stalk and typical columella, places Diachea within the order Physarales. The presence of a phaneroplasmodium during the trophic stage and lime deposition in its sporophores, as was confirmed in this work, supported the inclusion of Diachea in the Physarales, and the noncalcareous capillitial system verified its identification as a member of the Didymiaceae. Further characteristics of the species D. leucopodia include the following: phaneroplasmodium, spore globose 7.5 ${\mu}m$ in diameter, very minutely roughened; sporangia $500{\mu}m\times1mm$, more or less cylindrical, gregarious, stalked 1.2mm; stalk and columella white.