• Title/Summary/Keyword: Energy calibration

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Investigation of the optimum condition for the quantitative analysis of Cu sample by Laser induced breakdown spectroscopy (구리 시료의 정량분석을 위한 LIBS의 최적조건 연구)

  • Kim, Seunghyun;Shin, Heesung;Ju, Junesik;Kim, Hodong
    • Analytical Science and Technology
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    • v.22 no.2
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    • pp.141-147
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    • 2009
  • A laser induced breakdown spectroscopy (LIBS) measurement was carried out to derive an optimized measurement condition with a high reproducibility and to grow a plasma sphere to 20 mm high under a 600 mtorr vacuum in order to improve an accuracy of measurement. The measurement of the plasma was taken at a 6.0 mm distance, in the direction of a plasma sphere, from a sample. This location belongs to the outer sphere region in the plasma. The calibration curve of 'Ni' and 'Cu' was acquired by the signal intensity ratio and the atomic ratio for the samples, and linear regression of 'Cu' was $R^2$=0.9886, and the linear regression of 'Ni' was $R^2$=0.9988. The accuracy of LIBS was improved pre-existence as the measurement error of 'Ni' was 0.78%.

Evaluation of Fracture Toughness Characteristics of Pultruded CFRP Spar-Cap Materials with Non-woven Glass Fabric for Wind Blade (유리섬유 부직포가 삽입된 풍력 블레이드 인발 성형 스파캡 소재의 파괴인성 특성 평가)

  • Young Cheol Kim;Geunsu Joo;Jisang Park;Woo-Kyoung Lee;Min-Gyu Kang;Ji Hoon Kim
    • Journal of Wind Energy
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    • v.14 no.3
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    • pp.83-90
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    • 2023
  • The purpose of this study is to evaluate the inter-laminar fracture toughness characteristics of CFRP pultrusion spar cap materials reinforced with non-woven glass fabric. Test specimens were fabricated by the infusion technique. A non-woven glass fabric and artificial defects were embedded on the middle surface between two pultruded CFRP panels. Double cantilever beam (DCB) and End Notched Flexure (ENF) tests were performed according to ASTM standards. Fracture toughness and crack propagation characteristics were evaluated with load-displacement curves and delamination resistance curves (R-Curve). The fracture toughness results were calculated by compliance calibration (CC) method. The initiation and propagation values of Mode-I critical strain energy release rate value GIc were 1.357 kJ/m2 and 1.397 kJ/m2, respectively, and Mode-II critical strain energy release rate values GIIc were 4.053 kJ/m2 for non-precracked test and 4.547 kJ/m2 for precracked test. It was found that the fracture toughness properties of the CFRP pultrusion spar-cap are influenced by the interface between the layers of CFRP and glass fiber non-woven.

Fabrication and Its Characteristics of Ion Energy Spectrometer for Diagnostics of Plasma (플라즈마 진단을 위한 이온에너지 분석장치의 제작 및 특성 조사)

  • Kim, Kye-Ryung;Kim, Wan;Lee, Yong-Hyun;Kang, Hee-Dong
    • Journal of Sensor Science and Technology
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    • v.7 no.3
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    • pp.163-170
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    • 1998
  • An ion energy spectrometer which has the $45^{\circ}$ parallel electrostatic deflection plate was designed and constructed for measuring ion temperature in high temperature plasma. The energy calibration and the energy resolution were studied in detail for a hydrogen ion at the $0.24{\sim}1.92\;keV$ energy using electrostatic accelerator with a duoplasmatron ion source. The voltage of the deflection plate was linearly increased for the decreased ion detector position at the constant ion energy and decreased for the increased ion energy at the fixed ion detector position. The inclination of the deflection plate voltage to the ion energy was between 0.92 and 1.61, and linearly decreased for the increased the ion detector position. The measured energy resolution, which is $4.2%\;{\sim}\;11.6%$ in this experiment region, was improved for the increased ion dector position and ion energy. The relative efficiency was increased for the decreased the ion detector position. The ion energy spectrum of the DC plasma in the multi-purpose plasma generator was measured using this equipment. The ion temperature was 203-205 eV at the discharge voltage 320 V, discharge current 1.7 A.

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An intercomparison of two satellite data-based evapotranspiration approaches (인공위성 데이터 기반의 두 공간 증발산 산정 모형 비교 분석)

  • Sur, Chan-Yang;Choi, Min-Ha
    • Journal of Wetlands Research
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    • v.13 no.3
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    • pp.471-479
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    • 2011
  • Evapotranspiration (ET) including evaporation from a land surface and transpiration from photosynthesis of vegetation is a hydrological factor that has an important role in water cycle. However, there is a limitation to understand it due to heterogeneity of land cover and vegetation. In this study, Mapping EvapoTRanspiration with Internalized Calibration (METRIC) model, one of the energy balance models, and MODerate resolution Imaging Spectroradiometer (MODIS) satellite based well-known Penman-Monteith algorithm were compared. Two ET maps were categorized and compared by land cover classification. The results represented overall applicability of the two models with the highest correlation coefficients in needleleaf and broadleaf forests. This study will be useful to estimate remote sensing based ET maps with high resolution and to figure out spatio-temporal variability and seasonal changes.

A Method for Absolute Determination of the Surface Areal Density of Functional Groups in Organic Thin Films

  • Min, Hyegeun;Son, Jin Gyeong;Kim, Jeong Won;Yu, Hyunung;Lee, Tae Geol;Moon, Dae Won
    • Bulletin of the Korean Chemical Society
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    • v.35 no.3
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    • pp.793-797
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    • 2014
  • To develop a methodology for absolute determination of the surface areal density of functional groups on organic and bio thin films, medium energy ion scattering (MEIS) spectroscopy was utilized to provide references for calibration of X-ray photoelectron spectroscopy (XPS) or Fourier transformation-infrared (FT-IR) intensities. By using the MEIS, XPS, and FT-IR techniques, we were able to analyze the organic thin film of a Ru dye compound ($C_{58}H_{86}O_8N_8S_2Ru$), which consists of one Ru atom and various stoichiometric functional groups. From the MEIS analysis, the absolute surface areal density of Ru atoms (or Ru dye molecules) was determined. The surface areal densities of stoichiometric functional groups in the Ru dye compound were used as references for the calibration of XPS and FT-IR intensities for each functional group. The complementary use of MEIS, XPS, and FT-IR to determine the absolute surface areal density of functional groups on organic and bio thin films will be useful for more reliable development of applications based on organic thin films in areas such as flexible displays, solar cells, organic sensors, biomaterials, and biochips.

Comparison of Air Kerma and Absorbed Dose to Water Based Protocols for High Energy Photon Beams: Theoretical and Experimental Study

  • Shin, Dong-Oh;Kim, Seong-Hoon;Seo, Won-Seop;Park, Sung-Yong;Park, Jin-Ho;Kang, Jin-Oh;Hong, Seong-Eon;Ahn, Hee-Kyung
    • Proceedings of the Korean Society of Medical Physics Conference
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    • 2002.09a
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    • pp.241-243
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    • 2002
  • New types of protocols have been recently in development, all based on an absorbed dose-to-water with the aim of improving the accuracy of measurements of absorbed dose to water. IAEA TRS-277, the air-kerma standard-based present protocol, and IAEA TRS-398 and AAPM TG-51, the absorbed dose-to-water standard-based new one, were studied and compared theoretically and experimentally for photon beams of 6, 10, and 15 MV. NE 2571 and 3 Farmer types of ionization chambers in widely commercial use were used to determine an absorbed dose to water at the reference depth in water. Two different kinds of calibration factors were given respectively for every chamber calibrated in $\^$60/CO gamma ray beams from a Korean Secondary Standard Dosimetry Laboratory (KFDA). This work shows that there is around 1 % of difference of absorbed doses measured between two different types of calibration systems owing to different physical parameters and reference conditions used. We hope this work to help form the basis on development of new type of protocol in Korea.

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A Method for Simultaneous Measurement of Air Kerma, Half Value Layer and Tube Potential in Quality Control Procedure of Diagnostic x ray units

  • Katoh, Tsuguhisa;Saitoh, Hidetoshi;Ohtani, Hiroki;Negishi, Tooru;Myojoyama, Atsushi;Ohno, Yuusuke;Sasaki, Takehito
    • Proceedings of the Korean Society of Medical Physics Conference
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    • 2002.09a
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    • pp.294-297
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    • 2002
  • For the quality control procedure of diagnostic x ray units, a method for simultaneous measurement of air kerma, half value layer and tube potential was developed utilizing a computed radiography system for intraoral radiography and film badge case. The response of average pixel values under the windows were calibrated by x rays generated at tube potentials from 40 to 140 kV with filtration from 1.5 to 3.7 mmAl. The calibration curves for half value layer and tube potential were derived as functions of attenuation factors by the 1.4 mmAl filter and the 0.2 mmCu filter. The energy dependency of the open window response was corrected by the calibration factor as a function of the attenuation factor by the 1.4 mmAl filter. The uncertainty of the estimated half value layer, tube potential and air kerma were 0.2 mmAl, 3.6 % and 5 %, respectively. It was thus suggested that this system could be applied to quality control program to detect the variation of working condition of x ray units in clinical use.

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Probabilistic Calibration of Computer Model and Application to Reliability Analysis of Elasto-Plastic Insertion Problem (컴퓨터모델의 확률적 보정 및 탄소성 압착문제의 신뢰도분석 응용)

  • Yoo, Min Young;Choi, Joo Ho
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.9
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    • pp.1133-1140
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    • 2013
  • A computer model is a useful tool that provides solution via physical modeling instead of expensive testing. In reality, however, it often does not agree with the experimental data owing to simplifying assumption and unknown or uncertain input parameters. In this study, a Bayesian approach is proposed to calibrate the computer model in a probabilistic manner using the measured data. The elasto-plastic analysis of a pyrotechnically actuated device (PAD) is employed to demonstrate this approach, which is a component that delivers high power in remote environments by the combustion of a self-contained energy source. A simple mathematical model that quickly evaluates the performance is developed. Unknown input parameters are calibrated conditional on the experimental data using the Markov Chain Monte Carlo algorithm, which is a modern computational statistics method. Finally, the results are applied to determine the reliability of the PAD.

X-Ray Fluorescence Analysis of $Ta_2O_5,\;Nb_2O_5$ and ZrO_2$ in Tin-Slag Samples using Simple Dilution Method (주석 슬랙중 $Ta_2O_5,\;Nb_2O_5$ZrO_2$의 단일희석법을 이용한 X-선 형광분석)

  • Young-Sang Kim;Hak Je Sung
    • Journal of the Korean Chemical Society
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    • v.28 no.5
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    • pp.293-301
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    • 1984
  • -ray fluorescence analysis of $Ta_2O_5$, $Nb_2O_5$ and $ZrO_2$ in tin-slag samples using the simple dilution method was studied. The method is to correct mathematically the calibration curve to the linear line by the dilution. One synthesized standard having similar composition to the sample and tin slag samples were diluted with anhydrous $Li_2B_4O_7$ at the level of 1%, 2% and 3% of the sample content respectively. The diluted samples were fused at $1150^{\circ}C$ for 30 minutes and these glass beads were finely ground and pelletized. Measuring the X-ray intensities with these pellets, analytical results were calculated by the equation derived from J. Scherman's equation for the characteristic X-ray intensity of an element. Analytical results agreed with the reference values obtained by the standard calibration method within allowable error range and were reproducible.

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SIMULATION OF SHIELDING EFFECTS ON THE TOTAL DOSE OBSERVED IN TDE OF KITSAT-1 (KITSAT-1 TDE의 차폐 효과에 의한 총 축적 방사능양 변화에 대한 연구)

  • 김성준;신영훈;민경욱
    • Journal of Astronomy and Space Sciences
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    • v.18 no.1
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    • pp.71-80
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    • 2001
  • The threshold voltage shift observed in TDE (Total Dose Experiment) on board the KITAT-1 is converted into dose (rad($SiO_2$)) using the result of laboratory calibration with Co-60 gamma ray source in KAERI (Korea Atomic Energy Research Institute). Simulation using the NASA radiation model of geomagnetosphere verifies that the dose difference between RADFET1 and RADFET3 observed on KITSAT-1 comes from the difference in shielding thickness at the position of these RADFETs.

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