• 한국치위생학회지
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• 제19권6호
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• pp.1067-1075
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• 2019

Objectives: The present study aimed to compare the accuracy of removable partial denture (RPD) frameworks fabricated by selective laser sintering (SLS) before and after electropolishing. Methods: A partially edentulous mandibular model was used as the working model. Scanning of the model was performed using a dental scanner. The framework was designed using CAD software. The metal framework was formed using an SLS 3D printer. 3D scans of the two fabricated prototypes produced before and after electropolishing were overlapped with reference data. The fit was calculated based on Root Mean Square (RMS). Fabrication accuracy was verified using the paired t-test to compare the discrepancy before and after electropolishing. Results: The mean (SD) values of RMS before and after electropolishing were 126.6 (34.19) and 75.86 (21.36), respectively. There was a statistically significant difference before and after electropolishing (p<0.05). Conclusions: Metal frameworks made with SLS 3D printers showed clinically acceptable fit after electropolishing.

• Corrosion Science and Technology
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• 제21권4호
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• pp.314-324
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• 2022

The objective of this investigation was to indentify major factors affecting surface roughness among various parameters of electropolishing process using the design of an experiment method (full factorial design) for UNS S31603. Factors selected included electrolyte composition ratio, applied current density, and electrolytic polishing time. They were compared through analysis of variance (ANOVA). Results of ANOVA revealed that all parameters could affect surface roughness, with the influence of electrolyte composition ratio being the highest. As a result of surface analysis after electropolishing, the specimen with the deepest surface damage was about 35 times greater than the condition with the smallest surface damage. The largest value of surface roughness after electropolishing was higher than that of mechanical polishing due to excessive processing. On the other hand, the smallest value of surface roughness after electropolishing was 0.159 ㎛, which was improved by more than 80% compared to the previous mechanical polishing. Taken all results together, it is the most appropriate to perform electrolytic polishing with a sulfuric acid and phosphoric acid ratio of 3:7, an applied current density of 300 mA/cm², and anelectrolytic polishing time of 5 minutes.

• 센서학회지
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• 제26권2호
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• pp.122-127
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• 2017

Graphene grown on copper-foil substrates by chemical vapor deposition (CVD) has been attracting interest for sensor applications due to an extraordinary high surface-to-volume ratio and capability of large-scale device fabrication. However, CVD graphene has a polycrystalline structure and a high density of grain boundaries degrading its electrical properties. Recently, processes such as electropolishing for flattening copper substrate has been applied before growth in order to increase the grain size of graphene. In this study, we systemically analyzed the effects of the process condition of electropolishing copper foil on the quality of CVD graphene. We observed that electropolishing process can reduce surface roughness of copper foil, increase the grain size of CVD graphene, and minimize the density of double-layered graphene regions. However, excessive process time can rather increase the copper foil surface roughness and degrade the quality of CVD graphene layers. This work shows that an optimized electropolishing process on copper substrates is critical to obtain high-quality and uniformity CVD graphene which is essential for practical sensor applications.

• 마이크로전자및패키징학회지
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• 제15권1호
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• pp.45-50
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• 2008

Through via 3D SiP의 평탄화 공정에 적용하기 위해 전기도금법을 이용하여 직경 $50{\mu}m$와 $20{\mu}m$ via를 구리로 채운 후 전해연마를 실시하여 전해액 종류와 첨가제에 따른 특성을 분석하였다. 전해연마시 양극과 음극의 전위차 변화를 측정하여 평탄화 공정의 종료 시점을 판단하였다. 인산에 가속제인 acetic acid와 억제제인 glycerol을 첨가한 전해액으로 전해연마를 실시하여 via 형상 안팎의 단차를 제거하면서 평탄화를 이를 수 있었고, 양극과 음극의 전위차가 급격히 증가하는 시점에서 공정을 종료하여 via 위에 과도금된 구리만을 제거할 수 있었다.

• 한국표면공학회지
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• 제49권5호
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• pp.447-453
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• 2016

In this study, we intended to extend the life of electropolishing solution through the reduction of electric resistance by improving the electrolysis efficiency. The optimum conditions were obtained by half round bus bar and Taguchi method. As the main control factors in the electropolishing process, current density, polishing time, electrolyte temperature and flow rate were selected. The electrolyte temperature was the most significant to the electrolysis efficiency. The optimum conditions for the life extension of electropolishing solution were as follows: current density, $45A/dm^2$; polishing time, 6 min; electrolyte temperature, $70^{\circ}C$; flow rate, 11 L/min. As a results of ANOVA of SN ratios, it was found that the electrolyte temperature was significant factor at the 90% confidence level.

• Corrosion Science and Technology
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• 제21권2호
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• pp.158-169
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• 2022

The objective of this study was to investigate the electrochemical behavior and damage degree of metal surface under different conditions by performing a potentiodynamic polarization experiment using an electropolishing solution for UNS S31603 based on initial delay time and surface roughness (parameters). A second anodic peak occurred at initial delay time of 0s and 100s. However, it was not discovered at 1000s and 3600s. This research referred to an increase in current density due to hydrogen oxidation reaction among various hypotheses for the second anodic peak. After the experiment, both critical current density and corrosion current density decreased when the initial delay time (immersion time) was longer. As a result of surface analysis, characteristics of the potentiodynamic polarization behavior were similar with roughness, although the degree of damage was clearly different. With an increase in surface roughness value, the degree of surface damage was precisely observed. As such, electrochemical properties were different according to the immersion time in the electropolishing solution. To select electropolishing conditions such as applied current density, voltage, and immersion time, 1000s for initial delay time on the potentiodynamic polarization behavior was the most appropriate in this experiment.

• 한국전기전자재료학회논문지
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• 제13권12호
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• pp.983-988
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• 2000

The leadframe of thin plate fabricated by stamping method generates a lot of burr and stress in the processing surface because of the mold. The electropolishing equipment was produced in order to increase accuracy and surface roughness for 42%Ni-Fe leadframe. An electrolyte consisted of phosphoric acid, ethylene glycol and deionized water. Experiments were accomplished as polishing conditions were changed such as current density, polishing time, electrode gap and sample shape. The burr from the cutting was eliminated and surface characteristics of high flatness and high luster wre obtained after electropolishing. In addition, the electroplishing had good characteristic in 1.0 A current density and 4㎜ of electrode spaces, and it was affected by the composition of electrolyte and the sample shape.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 2003년도 추계학술대회
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• pp.71-76
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• 2003

This paper describes the characteristic of a large-diameter pipe to obtain smooth surface using Electropolishing after grinding using a non-woven fabric. Grinding using a non-woven fabric is possible under lower load and fine effect comparing with Wheel grinding. Also, the ion from the surface of the metal is eliminated by means of an electrical potential and current in Electropolishing. Electropolishing is used for leveling the surface, improving the physical appearance of the part, promoting corrosion properties and reducing contamination and adhesion of the surface. Therefore, the aim of the present study is to investigate the internal machining of a large-diameter pipe for semiconductor using experimental design method.

• 열처리공학회지
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• 제23권3호
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• pp.137-141
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• 2010

The Co-Cr alloys have clinical histories in dental and orthopaedic implants, and recently in cardiovascular stent applications because the alloys exhibit a high elastic modulus and radiopacity. In order to improve mechanical property of the Co-Cr alloys, electropolishing is employed as the final process. Electropolishing, an anodic dissolution process in the transpassive state, is sensitively affected by process conditions such as current density, machining time, electrode gap. In this study, the effect of heat treatment conditions on surface roughness and inclusion analysis is investigated in Co-Cr alloy (L605). The most smooth surface of Co-Cr alloy is obtained when electropolishing is performed at 15-20 V for 15-30 sec with a electrode gap of 3.5 mm.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2007년도 춘계학술대회 논문집
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• pp.273-274
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• 2007