• Journal of the Korean Society of Food Science and Nutrition
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• 제38권1호
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• pp.111-115
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• 2009

Carrots were dried using 30, 50, and 80% polyethylene glycol (PEG) or maltodextrin as a dehydrating agent, and the dried carrots were compared with the freeze dried and hot-air dried in terms of rehydration ratio, color, carotene content, and sensory evaluation. The amount of moisture loss during drying of carrots using PEG or maltodextrin increased with increasing concentration of dehydrating agent. Rehydration ratio as well as carotene content of the PEG-treated carrots were greater than those of freeze-dried or hot-air dried carrots. Regarding color and sensory evaluation of the dried carrots, the PEG-treated and maltodextrin-treated carrots were better than freeze-dried or hot-air dried carrots. These results suggest that drying of carrots using PEG or maltodextrin is a very efficient method because of its good rehydration capacity and minimal destruction of nutrients and cell structure.

• Polymer(Korea)
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• 제24권1호
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• pp.72-81
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• 2000

Benzoic acid polyester/lactone polyol were synthesized by polycaprolactone 0201 as diol, trimethylolpropane as triol, adipic acid as dibasic acid, and benzoic acid as monobasic acid. Polyisocyanate prepolymer Desmodur N-100 of HDI-biuret type was used in this study. Two-component polyurethane coatings were prepared by blending benzoic acid polyester/polycaprolactone, polyisocyanate, wetting/dispersing agent, white pigment, and flowing agent. Various properties were examined on the film coated with the prepared polyurethane. They showed excellent physical properties such as abrasion resistance, accelerated weathering resistance, and yellowness index. They also showed good physical properties such as flexibility, impact resistance, 60$^{\circ}$ specular gloss, cross hatch adhesion, hydrocarbon resistance, and lightness index difference. Hardness of coating showed a little poor character. The introduction of polycaprolactone 0201 as diol in the polyurethane coatings improved the hydrocarbon resistance, impact resistance, and flexibility of coatings. According to the drying and curing behavior with the contents of benzoic acid, they seem to have reasonable coating properties such as drying time of 2 to 4 hours and pot-life time of 20 to 37 hours.

• Bulletin of the Korean Chemical Society
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• 제34권2호
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• pp.622-628
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• 2013

Nanocrystalline spinel lithium manganese oxide ($LiMn_2O_4$) powders with narrow-size-distribution, pure-phase particles, and high crystallinity with an average crystallite size of about 70 nm were synthesized at $600^{\circ}C$ for 6 h in air by freeze drying method. Spinel $LiMn_2O_4$ is also prepared by sol-gel using citric acid as a chelating agent. The influence of different parameters such as pH conditions, solvent, molar ratio of citric acid to total metal ions, calcination temperature, starting material on the structure, morphology and purity of this oxide was investigated. The results of sol-gel method show that pure $LiMn_2O_4$ with average crystallite size of about 130 nm can be produced from nitrate salts as starting materials at $800^{\circ}C$ for 6 h in air. The optimum pH and molar ratio of chelating agent to total metal ions are $4{\leq}pH{\leq}6$ and 1.0, respectively. A possible mechanism on the formation of the nanocrystallines synthesized by sol-gel was also discussed. At the end a comparison of the differences between two methods was made on the basis of x-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared spectroscopy (FTIR), and thermogravimetric analysis (TGA) tests.

• Journal of Pharmaceutical Investigation
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• 제6권1호
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• pp.26-32
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• 1976

Dicalcium phosphate dihydrate (DCPD) is the most widely-used dentifrice abrasive in non-therapeutic tooth-paste requiring, low abrasive level, high stability and excellent compatibility with other formulation ingredients. One of the difficulties encountered in the use of this material in tooth-paste is that unless storage of the product is maintained at a relative low temperature there is a distinct tendency to lose water of crystallization. Another difficulty which has been encountered is that there is a tendency for the product to become lumpy. Various means have been proposed for increasing the stability and overcoming the lumping tendency, most of which means comprise the addition of stabilizing agent. But there is not any report about the relationships between the mechanism of dehydration, physical properties, structure and manufacturing condition. In this experiment, DCPD were manufactured by methods of Moss' patent, its two varied and J.P.VIII, these were studied by means of stability test, IR spectra, and DTA. According to the manufacturing conditions, DCPD has different physical properties and structures, i. e., monoclinic system of low drying temperature, triclinic system of high drying temperature. Dehydration of DCPD may be supposed one step debydration at about $100^{\circ}$ and it finaly converts to ${\gamma}-pyrophosphate$ at about $465^{\circ}$ and if the drying temperature is high it becomes DCP anhydrous. DCPD made by Moss' patent is thought of the best polishing agent of tooth-paste.

• Journal of the Korea institute for structural maintenance and inspection
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• 제23권1호
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• pp.45-53
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• 2019

Slump flow, compressive strength, flexural strength and drying shrinkage were measured to evaluate workability and mechanical performance of geopolymer. Experimental parameters include the addition of gypsum, blending ratio of blast furnace slag and fly ash and addition of shrinkage reducing agent. Geopolymer using blast furnace slag mixed with gypsum showed larger slump flow than blast furnace slag without gypsum. The slump flow when blending ratio of blast furnace slag and fly ash is 5:5 tended to be larger than the slump flow when blending ratio is 8:2. Geopolymer using blast furnace slag without gypsum showed higher compressive strength and flexural strength than blast furnace slag mixed with gypsum. Compressive strength and flexural strength tended to be higher when blending ratio of blast furnace slag and fly ash was 8:2 than when blending ratio was 5:5. Drying shrinkage decreased with increasing fly ash and blast furnace slag without gypsum, and it was found that shrinkage reducing agent is effective to reduce drying shrinkage of geopolymer.

• Proceedings of the Korean Institute of Building Construction Conference
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• 한국건축시공학회 2016년도 추계 학술논문 발표대회
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• pp.32-33
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• 2016

This purpose of this study is to find the properties of pore structure and length change of blast furnace slag cement added alkali powder stimulant on shrinkage reducing agent presence. In length change, the specimen added alkaline stimulant was smaller than normal blast furnace slag concrete. And the specimen added shrinkage reduction agent was confirmed to show smaller rate of length change than the length. In MIP analysis of 1day-age, 0.1㎛ subsequent pore amount of the specimen added alkaline stimulant was significantly smaller value the normal blast furnace slag concrete specimen.

• Proceedings of the Korean Institute of Building Construction Conference
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• 한국건축시공학회 2008년도 추계 학술논문 발표대회
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• pp.27-30
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• 2008

This study investigated the application of red muds, which were industrial wastes fired at 800℃, with a coloring agents. The results were summarized as following. The slumpflow, air content and unit weight volume were satisfied with each target values. The setting time was shortened on the case that 3 % of the red coloring agent and fired red mud were simultaneously replaced about 1 hour compared with the previous study which was 6 % of the red coloring agent was individually used. For the length change ratio caused by drying shrinkage and depth of neutralization on hardened concrete, they were declined when 3 % of the red coloring agent and fired red mud were simultaneously replaced compared with the previous study. On the measurement of forming colors, the case that 3 % of the red coloring agent and fired red mud were simultaneously replaced was similar to the previous study.

• Proceedings of the Korean Institute of Building Construction Conference
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• 한국건축시공학회 2003년도 학술.기술논문 발표회
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• pp.113-117
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• 2003

In this study is investigated the various properties of concrete with the kinds of stabilizing agent of recycling water and solid content in order to suggest a practical use of recycling water. According to the results, fluidity and air content varies slightly with the kinds of stabilizing agent and solid content, but does not make a big difference. Setting time does not differ remarkably from plain concrete at 20℃, but is shortened with an increase of solid content. Bleeding is reduced more largely in the case of S than in the case of R, and is not influenced by solid content. Compressive strength is equal or decreases in comparison with plain concrete at solid content of I and 50%, and shows the highest value at solid content of 3%. Length change by drying shrinkage is larger than plain concrete at solid content of 5%, and decreases at solid content of I and 3%. Therefore, it proves that the influence of the kinds of stabilizing agent is minute, and solid content is most effective at 3%.

• Proceedings of the Korean Institute of Building Construction Conference
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• 한국건축시공학회 2003년도 학술.기술논문발표회
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• pp.113-117
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• 2003

In this study is investigated the various properties of concrete with the kinds of stabilizing agent of recycling water and solid content in order to suggest a practical use of recycling water According to the results. fluidity and air content varies slightly with the kinds of stabilizing agent and solid content, but does not make a big difference. Setting time does not differ remarkably from plain concrete at 2$0^{\circ}C$, but is shortened with an increase of solid content. Bleeding is reduced more largely in the case of S than in the case of R, and is not influenced by solid content. Compressive strength is equal or decreases in comparison with plain concrete at solid content of 1 and 5%, and shows the highest value at solid content of 3%. Length change by drying shrinkage is larger than plain concrete at solid content of 5%, and decreases at solid content of 1 and 3%. Therefore, it proves that the influence of the kinds of stabilizing agent is minute, and solid content is most effective at 3%.

• Ultrasonography
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• 제32권1호
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• pp.59-65
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• 2013

Purpose: The purpose of this study is to establish the methodology regarding synthesis of ultrasound contrast agent imaging, and to evaluate the characteristics of the synthesized ultrasound contrast agents, including size or degradation interval and image quality. Materials and Methods: The ultrasound contrast agent, composed of liposome and SF6, was synthesized from the mixture solution of $21{\mu}mol$ DPPC (1, 2-Dihexadecanoyl-sn-glycero-3-phosphocholine, $C_{40}H_{80}NO_8P$), $9{\mu}mol$ cholesterol, $1.9{\mu}mol$ of DCP (Dihexadecylphosphate, $[CH_3(CH_2)_{15}O]_2P(O)OH$), and chloroform. After evaporation in a warm water bath and drying during a period of 12-24 hours, the contrast agent was synthesized by the sonication process by addition of buffer and SF6 gas. The size of the contrast agent was controlled by use of either extruder or sonication methods. After synthesis of contrast agents, analysis of the size distribution of the bubbles was performed using dynamic light scattering measurement methods. The degradation curve was also evaluated by changes in the number of contrast agents via light microscopy immediate, 12 hours, 24 hours, 36 hours, 48 hours, 60 hours, 72 hours, and 84 hours after synthesis. For evaluation of the role as an US contrast agent, the echogenicity of the synthesized microbubble was compared with commercially available microbubbles (SonoVue, Bracco, Milan, Italy) using a clinical ultrasound machine and phantom. Results: The contrast agents were synthesized successfully using an evaporation-drying-sonication method. The majority of bubbles showed a mean size of 154.2 nanometers, and they showed marked degradation 24 hours after synthesis. ANOVA test revealed a significant difference among SonoVue, synthesized contrast agent, and saline (p < 0.001). Although no significant difference was observed between SonoVue and the synthesized contrast agent, difference in echogenicity was observed between synthesized contrast agent and saline (p < 0.01). Conclusion: We could synthesize ultrasound contrast agents using an evaporation-drying-sonication method. On the basis of these results, many prospective types of research, such as anticancer drug delivery, gene delivery, including siRNA or microRNA, targeted molecular imaging, and targeted therapy can be performed.