• 한국구조물진단유지관리공학회 논문집
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• 제24권5호
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• pp.95-102
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• 2020

이 연구에서는 입경이 큰 골재를 사용하면서 2% 이상의 인장변형률 성능을 나타내는 고연성 PE 섬유보강 시멘트 복합체 개발을 목적으로 골재의 크기와 입도분포에 따른 고연성 섬유보강 시멘트 복합체의 인장거동 특성을 살펴보고자 하였다. 0.6 mm 이하의 입경들로 구성된 규사를 사용한 배합을 기준으로 최대입경 2.36 mm, 4.75 mm, 5.6 mm, 6.7 mm의 강모래 및 강자갈을 사용한 배합을 비교하여 성능평가를 실시하였다. 골재의 입도분포는 수정 A&A 모델에 기반한 최적입도분포곡선에 가깝도록 세분화된 입경별 혼합비율을 조절하였다. 직접인장실험을 통해 구한 인장거동은 모든 배합에서 뚜렷한 인장변형률 경화 거동을 보였다. 골재 입경별 혼합비율을 조절하여 입도분포가 최적곡선에 가깝도록 한 경우에는 모든 배합에서 규사를 사용한 경우보다 높은 인장변형률 성능을 나타내었다. 또한 골재의 최대입경이 커서 입도분포가 넓을수록 높은 인장변형률 성능을 보였으며, 최대입경 5.6 mm, 6.7 mm의 굵은 골재를 포함하는 경우 각각 4.83%와 5.89%의 매우 높은 인장변형률 성능을 나타내었다. 이 연구를 통해 적절한 입도분포 조절을 통해 굵은 골재를 사용하면서도 고연성 섬유보강 시멘트 복합체의 제조가 가능함을 보였다.

• 대한기계학회논문집B
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• 제25권1호
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• pp.9-17
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• 2001

A numerical study has been carried out on the evolution of the particle size distribution for unipolar charged particles that experience coagulation in an alternating electric field. The collision frequency function of charged particles was analytically derived. The log-normal size distribution function is utilized for representing a poly-disperse size distribution and the moments of the particle size distribution are used to solve the general dynamic equation considering only AC electric force effect. The results are compared with the effects of brownian coagulation.

• 공업화학
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• 제21권3호
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• pp.311-316
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• 2010

본 연구는 높은 분산 안정성을 유지하는 antimony-doped tin oxide (ATO) 분산액을 제조하기 위하여, 습식 볼밀법으로 분쇄시간에 따른 ATO의 입자크기, 입도분포, 분산성의 변화를 고찰하였다. 또한 각각의 습식 볼밀 처리된 ATO 분산액의 pH를 변화시켜 ATO 분산액의 분산 특성을 고찰하였다. 습식 볼밀 분쇄 조건에 의하여 ATO의 입자크기 및 입도 분포 변화는 레이저회절 입도분석기와 주사전자현미경을 이용하여 평가하였고, 습식 볼밀 분쇄 시간 및 pH조건에 따른 ATO 입자의 분산성은 제타전위 측정법과 다중광산란(multiple light scattering)법을 이용하여 평가하였다. 분쇄 조건 중 60 min 동안 처리된 ATO 입자 크기는 30% 이하로 작아지고, $1{\sim}35{\mu}m$에서 $0.1{\sim}5{\mu}m$로 입도분포를 갖는 균일한 입자를 얻을 수 있었다. 그러나 분쇄조건을 60 min 이상 처리한 것은 역분쇄 및 재응집 현상의 발생으로 인하여 한계 분쇄 시간이 나타나는 것을 알 수 있었다. 이러한 결과로부터 ATO 분산액은 습식 볼밀 분쇄 시간을 증가시킬수록 입자 크기가 감소하고 표면 에너지가 증가하여 입자간의 반발력이 커지게 됨을 알 수 있었고, 또한 용액의 pH를 증가시킬수록 입자의 표면 이온화도가 커짐으로 인하여 ATO 분산액의 분산성이 향상되는 것을 알 수 있었다.

• 한국결정성장학회지
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• 제24권3호
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• pp.111-119
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• 2014

A novel pulsed laser ablation process in liquid was investigated to prepare scheelite-type ceramic [calcium tungstate ($CaWO_4$) and calcium molybdate ($CaMoO_4$)] nanocolloidal particles. The crystalline phase, particle morphology, particle size distribution, absorbance and optical band-gap were investigated. Stable colloidal suspensions consisting of well-dispersed $CaWO_4$ and $CaMoO_4$ nanoparticles with narrow size distribution could be obtained without any surfactant. Particle tracking analysis using optical microscope combined with image analysis was applied for a fast determination of particle size distribution in the prepared nanocolloidal suspensions. The mean nanoparticle size of $CaWO_4$ and $CaMoO_4$ colloidal nanoparticles were 16 nm and 30 nm, with the standard deviations of 2.1 and 5.2 nm, respectively. The optical absorption edges showed blue-shifted values about 60~70 nm than those of reported in bulk crystals. And also, the estimated optical energy band-gaps of $CaWO_4$ and $CaMoO_4$ colloidal particles were 5.2 and 4.7 eV. The observed band-gap widening and blue-shift of the optical absorbance could be ascribed to the quantum confinement effect due to the very small size of the $CaWO_4$ and $CaMoO_4$ nanocolloidal particles prepared by pulsed laser ablation in liquid.

• 대한기계학회논문집B
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• 제22권12호
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• pp.1691-1701
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• 1998

Fly ash produced in coal combustion is a fine-grained material consisting mostly of spherical, glassy, and porous particles. A study on the formation mechanism of the fly ash from coal particles in the pulverized coal power plant is investigated with a physical, morphological, and chemical characteristic analysis of fly ash collected from the Samchonpo power plant. This study may contribute to the data base of domestic fly ash, the improvement of combustion efficiency, fouling phenomena and ash collection in the electrostatic precipitator. The physical property of fly ash is determined using a particle counter for the measurement of ash size distribution. Morphological characteristic of fly ash is performed using a scanning electron micrograph. The chemical components of fly ash are determined using an inductively coupled plasma emission spectrometry(ICP). The distribution of fly ash size was bi-modal and ranged from 12 to $19{\mu}m$ in mass median diameter. Exposure conditions of flue gas temperature and duration within the combustion zone of the boiler played an important role on the morphological properties of the fly ash such as shape, particle size and chemical components. The evolution of ash formation during pulverized coal combustion has revealed three major mechanisms by large particle formation due to break-up process, gas to particle conversion and growth by coagulation and agglomeration.

• Computers and Concrete
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• 제26권2호
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• pp.175-183
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• 2020

Fly ash has become an important component of concrete as supplementary cementitious material with the development of concrete technology. To make use of fly ash efficiently, four types of fly ash with particle size distributions that are in conformity with four functions, namely, S.Tsivilis, Andersen, Normal and F distribution, respectively, were prepared. The four particle size distributions as functions of the strength and pore structure of concrete were thereafter constructed and investigated. The results showed that the compressive and flexural strength of concrete with the fly ash that conforming to S.Tsivilis, Normal, F distribution increased by 5-10 MPa and 1-2 MPa, respectively, compared to the reference sample at 28 d. The pore structure of the concrete was improved, in which the total porosity of concrete decreased by 2-5% at 28 d. With regarding to the fly ash with Andersen distribution, it was however not conducive to the strength development of concrete. Regression model based on the grey multiple linear regression theory was proved to be efficient to predict the strength of concrete, according to the characteristic parameters of particle size and pore structure of the fly ash.

• Asian-Australasian Journal of Animal Sciences
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• 제5권1호
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• pp.13-18
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• 1992

Three cattle, a sheep and a goat were slaughtered to determine the distribution of digesta particles and mean size of digesta particles. Aliquot samples of digesta in the diverse sites of the digestive tracts were fractionated by a wet sieving technique. Fractionated particles were analyzed by the magnetic grid analyzer system constructed by authors. Results showed that the proportion of particles in digesta was similar among the omasum, abomasums cecum, colon and rectum, but that for the reticulo-ruminal digesta was different from the others. The pattern of the mass base frequency distribution of particles was also similar in the post-ruminal digesta. Average Heywood's diameter (the diameter equivalent to that of a circle with equal area to a projected area of a given particle) was about 1.2 mm in the reticulo-ruminal digesta and decreased to 0.65 mm for cattle or to about 0.35 mm for sheep and goat in the omasal digesta. Average Heywood's diameter was about the same in the post-ruminal digesta. It is concluded that mean particle size and particle distribution in digesta of the rectum or feces reflect those in digesta of the omasum.

• 한국재료학회지
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• 제30권5호
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• pp.223-230
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• 2020

As a case study on aspect ratio behavior, Kaolin, zeolite, TiO₂, pozzolan and diatomaceous earth minerals are investigated using wet milling with 0.3 mm media. The grinding process using small media of 0.3 pai is suitable for current work processing applications. Primary particles with average particle size distribution D₅₀, ~6 ㎛ are shifted to submicron size, D₅₀ ~0.6 ㎛ after grinding. Grinding of particles is characterized by various size parameters such as sphericity as geometric shape, equivalent diameter, and average particle size distribution. Herein, we systematically provide an overview of factors affecting the primary particle size reduction. Energy consumption for grinding is determined using classical grinding laws, including Rittinger's and Kick's laws. Submicron size is obtained at maximum frictional shear stress. Alterations in properties of wettability, heat resistance, thermal conductivity, and adhesion increase with increasing particle surface area. In the comparison of the aspect ratio of the submicron powder, the air heat conductivity and the total heat release amount increase 68 % and 2 times, respectively.

• 한국대기환경학회지
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• 제2권3호
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• pp.34-44
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• 1986

Particle size distribution of airborne suspended particulate concentrations according to particle size in the events of yellow sand phenomena, have been measured and analyzed by using Andersen air sampler for four years, January 1982 through December 1985. The conclusions are as follows: 1. Yellow sand phenomena, generally, occur between March and May. 2. The frequent occurrences of yellow sand were observed during March and April and airborne suspended particulate concentrations in the cases of yellow sand appeared to be 2 $\sim$ 3.4 times higher than those of normal conditions. 3. Geometric mean particle diameter and its geometric mean standard deviation by logarithmic normal distribution sheet, were quite close to each other and log-distribution curves showed similar shapes. 4. Analysis by particle size distribution curve showed bi-modal distribution. 5. Concentrations of coarse particles in normal conditions were 1.2 $\sim$ 2 times higher than those of fine particles and, similarly, coarse particle concentrations in yellow sand cases were 1.3 $\sim$ 2.5 times higher than those of fine particles. 6. Concentrations of coarse particles in yellow sand cases were 2 $\sim$ 3.6 times higher than those in normal conditions and those of fine particles were 1.7 $\sim$ 3.5 times higher.

• 한국재료학회지
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• 제11권10호
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• pp.869-878
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• 2001

Alumina $(Al_2O_3)$ green bodies were fabricated by gel-casting using three kinds of alumina with different particle size (mean particle size: 4.6 $\mu\textrm{m}$, 0.32 $\mu\textrm{m}$, 10nm). The effects of particle size on gel-casting process and green microstructure were investigated. The optimum dispersion conditions using ammonium salt (D-3019) as dispersant were 0.2 wt% (4.63 $\mu\textrm{m}$), 0.5 wt% (0.32 $\mu\textrm{m}$), and 5.0 wt% (10 nm), in high solid loading. The optimum solid loading of each starting material for gel-casting was obtained as 59 vol% (4.63 $\mu\textrm{m}$), 57 vol% (0.32 $\mu\textrm{m}$), 15 vol% (10 nm), depending on particle size, indicating that nano-size particle (10 nm) represent lower solid loading as high specific surface area than those of other two starting materials. The drying at ambient conditions (humidity; $\thickapprox$90%) was performed more than 48hrs to enable ejection of the part from the mold and then at $120^{\circ}C$ for 2hrs in an air oven, showing no crack and flaw in the dried green bodies. The pore size and distribution of the gelcast green bodies showed the significant decrease with decreasing particle size. Green microstructure was dependent on the pore size and distribution due to the particle size, and on the deairing step. The green density maximum obtained was 58.9% (4.63 $\mu\textrm{m}$), 60% (0.32 $\mu\textrm{m}$), 47% (10 nm) theoretical density (TD), and the deairing step applied before gel-casting did not affect green density.