• 한국주조공학회지
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• 제44권3호
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• pp.59-69
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• 2024

단결정 초내열합금 CMSX-4의 온도에 따른 인장 특성을 고찰하였다. 열처리된 상태에서는 공정 γ-γ'이 일부 남아 있으며, 대부분의 영역에서는 균일한 입방체 γ'이 관찰되었다. 항복강도와 인장강도는 750℃에서 가장 높았고 온도가 증가함에 따라 감소하였으며 연신율은 650℃에서 가장 낮았다. 연신율이 낮은 시편은 파단 부위 근처에 집중된 변형을 보인 반면, 연신율이 증가한 고온에서는 시편 전체에 걸쳐 변형이 발생하였다. 850℃ 및 950℃에서 인장시험 중 파단 표면 분석을 통해 균열이 주조 결함에서 발생하는 것으로 나타났다. 인장시험 후 수행된 TEM 관찰을 통해 상온에서의 주요 변형 메커니즘이 γ' 상 내의 전위 전단과 관련되어 있음을 알 수 있었다. 그러나 650℃와 적층 결함이 발생한 750℃에서는 γ'상의 전위에 대한 저항이 증가하여 강도가 증가하는 것으로 관찰되었다. 850℃ 이상의 온도에서 열적 활성화 과정으로 인해 전위의 이동이 쉬워지기 때문에 강도가 감소하는것으로 나타났다.

• 영어영문학
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• 제56권2호
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• pp.255-276
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• 2010

Despite some critics' efforts to highlight Shelley's political fruitfulness, they tend to disregard meaningful differences that Shelley has from other Jacobin radicals of his times. Accordingly, the critics tackle his apparent incoherence revealed in A Philosophical View of Reform; the first two sections contain a keen insight into the socio-political injustice prevalent in Britain and the reasons behind it, while the third section withdraws from the previous radical position and settles with a moderate electorate reform. This paper argues that recent developments in post-structuralist and post-Marxist theory help to clearly assess Shelley's political position. Emphasizing that the Jacobin concept of revolution is incompatible with the plurality and opening which a radical democracy requires, post-marxists such as Ernest Laclau and Chantal Mouffee claim that a more viable form of political resistance is to expose repression and force involved in hegemonic articulations. For them, dislocation, a distabilization of a discourse that results from the emergence of events which cannot be domesticated, symbolized, or integrated within the discourse, opens up the possibility of freedom for agents. A Philosophical View of Reform is an attempt to dislocate the discourses of monarchy and paper money by exposing their social and historical constructiveness and their repressive exclusion of alternative discourses. The political goal of this essay is to awaken subjects within a hegemonic structure by decentering the structure and to make them act by stimulating new discoursive constructions.

• 한국분말재료학회지
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• 제5권2호
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• pp.122-128
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• 1998

NiAl based ODS (Oxide Dispersion Strengthened) intermetallic alloys have been produced by mechanical alloying (MA) process and consolidated by hot extrusion. Subsequent thermomechanical treatments have been applied to induce secondary recrystallization in an attempt to improve creep resistance in this material. The creep behavior of secondary recrystallized MA NiAl has been investigated and compared with those of as-extruded condition. Minimum creep rate were shown to be approximately two orders of magnitude lower than that in as-extruded condition. The improvement in creep resistance is believed due to the grain coarsening, restricting of dispersoid coarsening as well as increase in grain aspect ratio. Creep threshold stress behavior, below which no measurable creep rate can be detected, has been discussed on the basis of particle-dislocation interaction theory. The threshold stress becomes negligible after secondary recrystallization in MA NiAl, presumably due to dispersoid coarsening and a decrease in grain boundary area during secondary recrystallization.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제41회 하계 정기 학술대회 초록집
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• pp.132-132
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• 2011

The sheet resistance (Rs) of undoped GaN films on AlN/c-plane sapphire substrate was investigated in which the AlN films were grown by R. F. magetron sputtering method. The Rs was strongly dependent on the AlN layer thickness and semi-insulating behavior was observed. To clarify the effect of crystalline property on Rs, the crystal structure of the GaN films has been studied using x-ray scattering and transmission electron microscopy. A compressive strain was introduced by the presence of AlN nucleation layer (NL) and was gradually relaxed as increasing AlN NL thickness. This relaxation produced more threading dislocations (TD) of edge-type. Moreover, the surface morphology of the GaN film was changed at thicker AlN layer condition, which was originated by the crossover from planar to island grains of AlN. Thus, rough surface might produce more dislocations. The edge and mixed dislocations propagating from the interface between the GaN film and the AlN buffer layer affected the electric resistance of GaN film.

• Archives of Metallurgy and Materials
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• 제67권4호
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• pp.1491-1495
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• 2022

The present research deals with the effect of pre-strain on the hydrogen embrittlement behavior of intercritically annealed medium-Mn steels. A slow strain-rate tensile test was conducted after hydrogen charging by an electrochemical permeation method. Based on EBSD and XRD analysis results, the microstructure was composed of martensite and retained austenite of which fraction increased with an increase in the intercritical annealing temperature. The tensile test results showed that the steel with a higher fraction of retained austenite had relatively high hydrogen embrittlement resistance because the retained austenite acts as an irreversible hydrogen trap site. As the amount of pre-strain was increased, the hydrogen embrittlement resistance decreased notably due to an increase in the dislocation density and strain-induced martensite transformation.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2000년도 춘계학술대회 논문집
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• pp.51-56
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• 2000

Demand for new nondestructive evaluations is growing to detect tensile crack growth behavior to predict long term performance of materials and structure in aggressive environments, especially when they are in non-visible area. Acoustic emission technique is well suited to these problems and has drawn a keen interests because of its dynamic detection ability, extreme sensitivity and location of growing defects. In this study, we analysed acoustic emission signals obtained in tensile test of high strength fire resistance steel for frame structure with time frequency analysis methods. The results obtained are summaries as follows ; In the T and TN specimen consisting of ferrite and pearlite grains, most of acoustic emission events were produced near yield point, mainly due to the dislocation activities during the deformation. However, B specimen under $600^{\circ}C$ - 10min had a two peak which was attribute to the presence of martensite phase. The first peak is before yield point the second is after yield point. The sources of second acoustic emission peak were the debonding of martensite-martensite interface and the micro-cracking of brittle martensite phase. In $600^{\circ}C$-30min to $700^{\circ}C$-60min specimens, many signals were observed from area before yield point and counts were decreased after yield point.

• 열처리공학회지
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• 제18권4호
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• pp.235-241
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• 2005

Thermal creep properties of the advanced zirconium fuel claddings named by HANA alloys which were developed for high burn-up application were evaluated. The creep test of HANA cladding tubes was carried out by the internal pressurization method in temperature range from 350 to $400^{\circ}C$ and in the hoop stress range from 100 to 150 MPa. Creep tests were lasted up to 800 days, which showed the steady-state secondary creep rate. The creep resistance of HANA fuel claddings was affected by final annealing temperature and various factors, such as alloying element, applied stress and testing temperature. From the results the microstructure observation of the samples before and after creep test by using TEM, the dislocation density was increased in the sample of after creep test. The Sn as an alloying element was more effective in the creep resistance than other elements such as Nb, Fe, Cr and Cu due to solute hardening effect of Sn. In case of HANA fuel claddings, the improved creep resistance was obtained by the control of final heat treatment temperature as well as alloying element.

• 한국화재소방학회논문지
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• 제28권5호
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• pp.52-57
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• 2014

구조용 강재는 고온 시 물질 내부의 구성 물질의 결합력 약화로 인하여 내력과 변형이 추가적으로 발생됨으로써, 구조적 성능이 저하되고, 국부 및 연속적 붕괴로 이어질 수 있다. 따라서 강재로 구성된 구조부재는 화재 시 열영향부를 최소화하기 위한 수단이 강구되는 내화설계가 요구된다. 건축용 내화강재(FR 490)는 용접 구조용 강재(SM 490)와 상온시 특성은 동일하나, 고온 시의 내력유지 성능이 우수한 강종으로써 이로 구성된 보부재의 고온 시 내력 평가 자료는 거의 없다. 따라서 본 연구에서는 FR 490강재로 구성된 보부재의 고온 시 거동을 고온 시 재료 특성과 이론적 방법을 통하여 해석적으로 평가하고, 이를 SM 490강재보와 비교함으로써 내화성능을 확인하고자 하였으며, 그 결과 FR 490강재보의 경우 SM 490강재보에 비해서 고온 시 내력유지 성능이 우수하였다.

• Corrosion Science and Technology
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• 제17권5호
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• pp.242-248
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• 2018

Martensitic high-strength steels revealed superior mechanical properties of high tensile strength exceeding 1000 Mpa, and have been applied in a variety of industries. When the steels are exposed to corrosive environments, however, they are susceptible to hydrogen embrittlement (HE), resulting in catastrophic cracking failure. To improve resistance to HE, it is crucial to obtain significant insight into the exact physical nature associated with hydrogen diffusion behavior in the steel. For martensitic steels, tempering condition should be adjusted carefully to improve toughness. The tempering process involves microstructural modifications, that provide changes in hydrogen diffusion/trapping behavior in the steels. From this perspective, this study examined the relationship between tempering condition and hydrogen diffusion behavior in the steels. Results based on glycerin measurements and hydrogen permeation evaluations indicated that hydrogen diffusion/trapping behavior was strongly affected by the characteristics of precipitates, as well as by metallurgical defects such as dislocation. Tempering condition should be adjusted properly by considering required mechanical properties and resistance to HE.

• Applied Microscopy
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• 제46권1호
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• pp.45-50
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• 2016

Iron containing a high amount of chromium is known to be inferior to ductility due to ${\sigma}$ phase formation so that it is generally difficult to apply the plastic deformation process although the alloy possesses a superior characteristics of an excellent corrosion resistance. In this study, Fe-50mass%Cr alloy was melted using high purity powder and the deformation behavior has been investigated by cold rolling and tensile test. The tensile test yielded that the alloy revealed a serration at an early stage of tensile deformation and then the serrated flow vanished to change to a normal work hardening flow at the later stage. The former was governed by twin formation process, the latter by dislocation multiplication one, bringing about a high ductility of 20% or over. The reduction ratio in cold rolling was attained as high as 90%, thus the high corrosion-resistant alloy is able to possess a high ductility.