• International Journal of Precision Engineering and Manufacturing
• /
• 제3권2호
• /
• pp.78-86
• /
• 2002

In general, X-ray diffraction method detects the changes of crystal lattice under material surface using the angle of diffraction 2$\theta$. This technique which deals with in the presented paper can be applied to a behavior on the slipped band or the micro crack cause to material degradation. The relation between half-value breadth and cycle numbers shows three stages, which consist of rapid decrease in the initial cycle, slight decrease in the middle cycle, and then rapid decrease in the final cycle. The ratio of half-value breadth has a constant value on B/B$\_$0/ - N diagram under the loading condition except early part of fatigue life. The ratio of half-value breadth B/B$\_$0/ - log N$\_$f/ with respect to number of cycle to failure N$\_$f/ has linear behavior on B/B$\_$0/ - log N$\_$f/ diagram. Therefore, the evaluation of fatigue life by the average gradient has much less mean error than the estimation of fatigue life by log B/B$\_$0/ - log N/N$\_$f/ relation.

• Fibers and Polymers
• /
• 제6권3호
• /
• pp.186-199
• /
• 2005

A selection of commercially available poly(ethy1ene terephtha1ate) fibers with different degrees of molecular alignment and crystallinity have been investigated utilizing a wide range of techniques including optical microscopy, infrared spectroscopy together with thermal and wide-angle X-ray diffraction techniques. Annealing experiments showed increased molecular alignment and crystallinity as shown by the increased values of birefringence and melting enthalpies. Crystallinity values determined from thermal analysis, density, unpolarized infrared spectroscopy and X-ray diffraction are compared and discussed in terms of the inherent capabilities and limitations of each measurement technique. The birefringence and refractive index values obtained from optical microscopy are found to decrease with increasing wavelength of light used in the experiments. The wide-angle X-ray diffraction analysis shows that the samples with relatively low orientation possess oriented non-crystalline array of chains whereas those with high molecular orientation possess well defined and oriented crystalline array of chains along the fiber axis direction. X-ray analysis showed increasing crystallite size trend with increasing molecular orientation. SEM images showed micro-cracks on low oriented fiber surfaces becoming smooth on highly oriented fiber surfaces. Excellent bending characteristics were observed with knotted fibers implying relatively easy fabric formation.

• 한국정밀공학회지
• /
• 제17권1호
• /
• pp.145-152
• /
• 2000

X-ray diffraction method detects change of crystal lattice distance under material surface using diffraction angle 2$\theta$. This technique can be applied to the behavior on slip band and micro crack due to material degradation. The relation between half-value breadth and number of cycle has three stages which constitute rapid decrease in initial number of cycles, slight decrease in middle number of cycles and rapid decrease in final number of cycles. The ratio of half-value breadth takes a constant value on B/B$_{0}$-N diagram with loading condition except early part of fatigue life. The ratio of half-value breadth B/B$_{0}$ with respect to number of cycle to failure N$_{f}$ has linear behavior on B/B$_{0}$-log N$_{f}$ diagram. Therefore, in this paper the estimation of fatigue life by average gradient method has much less estimated mean error than the estimation of fatigue life by log B/B$_{0}$-log N/N$_{f}$ relation.elation.ation.

• 한국정밀공학회지
• /
• 제23권8호
• /
• pp.72-79
• /
• 2006

We measured grating pitch standards using optical diffractometry and analyzed measurement uncertainty. Grating pitch standards have been used widely as a magnification standard for a scanning electron microscope (SEM) and a scanning probe microscope (SPM). Thus, to establish the meter-traceability in nano-metrology using SPM and SEM, it is important to certify grating pitch standards accurately. The optical diffractometer consists of two laser sources, argon ion laser (488 nm) and He-Cd laser (325 nm), optics to make an incident beam, a precision rotary table and a quadrant photo-diode to detect the position of diffraction beam. The precision rotary table incorporates a calibrated angle encoder, enabling the precise and accurate measurement of diffraction angle. Applying the measured diffraction angle to the grating equation, the mean pitch of grating specimen can be obtained very accurately. The pitch and orthogonality of two-dimensional grating pitch standards were measured, and the measurement uncertainty was analyzed according to the Guide to the Expression of Uncertainty in Measurement. The expanded uncertainties (k = 2) in pitch measurement were less than 0.015 nm and 0.03 nm for the specimen with the nominal pitch of 300 nm and 1000 nm. In the case of orthogonality measurement, the expanded uncertainties were less than $0.006^{\circ}$. In the pitch measurement, the main uncertainty source was the variation of measured pitch values according to the diffraction order. The measurement results show that the optical diffractometry can be used as an effective calibration tool for grating pitch standards.

• 한국인터넷방송통신학회논문지
• /
• 제22권5호
• /
• pp.123-128
• /
• 2022

정확한 모드전송선로 이론 (MTLT)을 적용하여 원추형 광 입사에서 공진 회절격자의 특성을 조사하였다. 원추형 구성에서 공진 회절과 관련된 모드 벡터가 전형적이 구조의 회절격자와 관련된 것보다 입사각에 따라 작게 변한다는 것을 보여주었다. 더욱이, 소멸하는 회절파가 공진 효과를 담당하는 누설 모드를 구동함에 따라, 원추형 장착은 기존 회절격자보다 더 큰 각도 허용 오차를 회절격자에 부여함을 보였다. 이에 기초하여, 수치 계산을 통하여 원추형 입사에서 발견된 스펙트럼을 사용하여, 원추형 및 클래식 구성에서 공진 회절격자의 각도-스펙트럼과 파장-스펙트럼 성능을 정량화하였다. 이러한 결과는 효율적이고 물리적으로 희소한 공진 회절격자를 요구하는 다양한 응용 분야에서 유용할 것이다.

• 한국전기전자재료학회논문지
• /
• 제21권9호
• /
• pp.829-834
• /
• 2008

Two-dimensional photonic quasicrystal (PQCs) template patterns have been fabricated on a 1.1 ${\mu}m$-thick DMI-150 photoresist using a multiple-exposure holographic method. A 442-nm HeCd laser was utilized as a light source and the holographic exposure was carried out at a fixed angle of ${\theta}$ = 6$^{\circ}$. After the first holographic exposure, the sample was rotated to a proper angle and the second exposure was performed to the same manner. This exposure process was repeated n/2 times to obtain n-fold symmetric PQC patterns and then the sample was developed. The diffraction patterns of the fabricated PQC template were observed using a 632.8-nm HeNe laser. The fabricated PQCs exhibited 8, 10 and 12-fold rotational symmetry, which was in a good agreement with the interference simulation results. In addition, the diffraction patterns with n-rotation symmetry were observed for the corresponding n-fold PQCs. We believe that the multiple-exposure holography is a good method to fabricate the mesoscale PQCs with a high rotational symmetry.

• 한국분말야금학회:학술대회논문집
• /
• 한국분말야금학회 2000년도 추계학술대회 및 발표대회 강연 및 발표논문 초록집
• /
• pp.11-12
• /
• 2000

Non-stoichiometric ceramics of $Ni_{x}ZnO_{1-x}Fe_{2}O_{4}$ were prepared by self-propagating high temperature synthesis reaction with various processing conditions and their stoichometric numbers were determined by neutron diffraction. The neutron diffraction patterns were measured at room temperature using monochromatic neutrons with a wave length of 0.18339 nm from a Ge(331) mocochromator at a 90 degree take off angle. The Rietveld refinement of each pattern converged to good agreement (x2=1.88-2.24). The neutron diffraction analysis revealed the final stoichiometries of the ferrites were $Ni_{0.38}Zn_{0.62}Fe_{2}O_{4}$ and $Ni_{0.33}Zn_{0.67}Fe_{2}O_{4]$, respectively. This supports that final stoichiometric number of the self-propagating high temperature synthesis product can be controlled by the processing parameters during the combustion reaction.

• 한국환경보건학회지
• /
• 제29권4호
• /
• pp.48-54
• /
• 2003

This study investigated retrogradation properties of Jeungpyun substituted for cereals with dietary fibers of 60% of brown rice, and barley. Quality changes during storage periods of the functional Jeungpyun, were studied using $\alpha$-amylase iodine enzyme digestion methods, X-ray diffraction patterns, and differential scanning calorimetry (DSC). The barley substituted samples showed significantly lower retrogrdation rates than those of control when examined by $\alpha$-amylase method. The Relative crystallity by X-ray diffraction patterns had typical A type in all samples with appealing big crystallity around its diffraction angle 23$^{\circ}$degrees as storage periods were increased. The brown rice and barley Jeunpyun made smaller crystallity than that of control, representing slower retrogradation rates. The batter controls had significantly lower ΔH than the other compared samples when measured by DSC, but had significantly higher ΔH after 30 days of storage, implying that the control required more energy for regelatinization after the 30 days of storage.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 1999년도 춘계학술대회 논문집
• /
• pp.87-90
• /
• 1999

The dependence of diffraction efficiency as a funct~on of film thickness and incident angle has been investigated in amorphous chalcogenide thin films, which act as a polarization holographic materials. Especially a-(Se, S) based films exhibit a number of photoinduced phenomena not observed in other types of amorphous thin films. Holographic gratings in amorphous As-Ge-Se-S thin films have been formed using the mutual perpendicular polarized(linearly) He-Ne laser light. We could obtain the optimum condition to get high diffraction efficiency.

• 대한전기학회:학술대회논문집
• /
• 대한전기학회 1986년도 하계학술대회논문집
• /
• pp.591-594
• /
• 1986

An asymptotic solution of electro-magnetic waves diffracted by a dielectric wedge of the angle larger than $180^{\circ}$ is obtained in case of the incidence of a E-polarized plane wave. Based on the dual integral equation in the spectral domain, physical optics approximation is supplemented by correction currents distributed along the interfaces. Those currents are expanded in a series of Bessel functions, known as Neumann's expansion of which fractional order is chosen to satisfy the static edge condition as the limiting value of dynamic case. Numerical results of edge diffraction patterns and field patterns are presented for some typical cases.