• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.29 no.2
• /
• pp.101-105
• /
• 2016

The basic characteristics of glass are highly fragile and brittle consequences the ultimate purpose of glass manufacturing is to make a transparent glass with complex shape. In order to solve this problem, mechanical properties of glass can be increased by crystallization of its amorphous glass. However, glass-ceramics has become opaque through crystallization process due to the distracted interface of glass by precipitated particles. This study has been investigated thermal processing conditions of LAS transparent glass-ceramic by using DTA (differential thermal analysis), in order to control size of precipitated particle and then fabricate transparent glass-ceramic. DTA indicated that crystallization peak area was declined with increased nucleation temperature. Subsequently, we have been established optimum temperature for crystallization depending on the nucleation temperature. The transmission and thermal expansion were measured after crystallization, and the size of precipitated particle was identified in range of 20~100 nm by FE-SEM. In addition, by setting the optimized crystallization condition, with high transmission and low thermal expansion glass was synthesized through this experiment.

• Transactions on Electrical and Electronic Materials
• /
• v.13 no.4
• /
• pp.204-207
• /
• 2012

Epoxy nanocomposite was synthesized through the exfoliation of organoclay in an epoxy matrix, which was composed of diglycidyl ether of bisphenol A (DGEBA), 4,4'-methylene dianiline (MDA) and malononitrile (MN). Organoclay was prepared by treating the montmorillonite with octadecyl trimethyl ammonium bromide (ODTMA). The exfoliation of the organoclay was estimated by wide angle X-ray diffraction (WAXD) analysis. In order to measure the cure rate of DGEBA/MDA (30 phr)/MN (5 phr)/organoclay (3 phr), differential scanning calorimetry (DSC) analysis was performed at various heating rates, and the data were interpreted by Kissinger equation. Thermal degradation kinetics of the epoxy nanocomposite were studied by thermogravimetric analysis (TGA), and the data were introduced to the Ozawa equation. The activation energy for cure reaction was 45.8 kJ/mol, and the activation energy for thermal degradation was 143 kJ/mol.

• Structural Engineering and Mechanics
• /
• v.66 no.6
• /
• pp.693-701
• /
• 2018

This paper develops a nonlocal strain gradient plate model for vibration analysis of graphene sheets under thermal environments. For more accurate analysis of graphene sheets, the proposed theory contains two scale parameters related to the nonlocal and strain gradient effects. Graphene sheet is modeled via a two-variable shear deformation plate theory needless of shear correction factors. Governing equations of a nonlocal strain gradient graphene sheet on elastic substrate are derived via Hamilton's principle. Differential quadrature method (DQM) is implemented to solve the governing equations for different boundary conditions. Effects of different factors such as temperature rise, nonlocal parameter, length scale parameter, elastic foundation and aspect ratio on vibration characteristics a graphene sheets are studied. It is seen that vibration frequencies and critical buckling temperatures become larger and smaller with increase of strain gradient and nonlocal parameter, respectively.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 1997.04a
• /
• pp.330-333
• /
• 1997

The thermal impact of mica/epoxy paper(130${\mu}{\textrm}{m}$) is investigated using XRD, DSC and TGL X-ray diffraction(XRD) analysis was performed to know the position and structure of mica crystal in insulation materials. A differential scanning calorimeter(DSC) was used to measure glass transition temperature and excess enthalphy of the composite materials that had been subjected to thermal aging. The glass transition temperature(T$_{g}$) measured by DSC is observed at 95.43$^{\circ}C$ and 113.43$^{\circ}C$, respectively. The T$_{g}$ also increases with increased aging time. Measurements performed by TGA(thermogravimetric analysis) have showed that weight loss profile of sound specimens are lower than those aged.ged.

• Proceedings of the KIEE Conference
• /
• 1989.11a
• /
• pp.211-215
• /
• 1989

This paper presents the thermal analysis of EHV OF cable accessories using FEM. The governing equation about the temperature in the cable accessories is induced by the energy balance equation. Since the temperature distribution is a function of space and time, the weighted residual method is adopted for FEM formulation. The difference approximation is used to treat the time differential term in the element equation. Automatic mesh generation which save time and labor is introduced for the data input process. It will be expected that the following thermal analysis result will be very useful to cable accessories design.

• The Journal of Advanced Prosthodontics
• /
• v.12 no.1
• /
• pp.9-14
• /
• 2020

PURPOSE. The aim of this study was to investigate the effect of different numbers of heat treatments applied to superstructure porcelain on optical, thermal, and phase formation properties of zirconia. MATERIALS AND METHODS. Forty zirconia specimens were prepared in the form of rectangular prism. Specimens were divided into four groups (n = 10) according to the number of firing at heating values of porcelain. Color differences and translucency parameter were measured, and X-ray diffraction (XRD) analysis and differential scanning calorimetry (DSC) were performed. Data were analyzed with analysis of variance (ANOVA). RESULTS. There were no statistically significant differences in ∆E, TP, L, a, and b value changes of the zirconia specimens as a result of repetitive firing processes (P>.05). CONCLUSION. Although additional firing processes up to 4 increase peak density in thermal analysis, additional firing processes up to 4 times can be applied safely as they do not result in a change in color and phase character of zircon frameworks.

• Proceedings of the Korean Institute of Building Construction Conference
• /
• 2022.11a
• /
• pp.197-198
• /
• 2022

Based on the carbonation depth measurement by the indicator for concrete collected from old structures and the quantitative analysis of Ca(OH)₂ and CO₂ in the carbonation section before and after the carbonation depth and in the non-carbonation section, the absorbable CO2 amount and carbonation degree measurement result is as follows 1) The carbonation depth of the 40-year-old reinforced concrete structure was measured to be about 22 mm. (basement interior wall, marble finish, strength 30MPa) 2) The amount of CO₂ absorbed by the concrete was about 4.3% of the sample weight, and the carbonation degree was estimated to be about 53%.

• 한국정보디스플레이학회:학술대회논문집
• /
• 2006.08a
• /
• pp.1193-1197
• /
• 2006

The novel oligomers were synthesized by Grignard reaction, the suzuki coupling reaction, etc. The oligomers were characterized by Infrared (IR), Mass spectrometer (MS). Their thermal properties were investigated by differential scanning calorimetry (DSC) and Thermogravimetric analysis (TGA). The new oligomers showed high thermal stability above $300^{\circ}C$.

• Journal of the Korean Ceramic Society
• /
• v.49 no.1
• /
• pp.111-117
• /
• 2012

Dependencies of thermal properties on the crystallization behavior of $0.9CaMgSi_2O_6-0.1MgSiO_3$ glass-ceramics were investigated as a function of heat-treatment temperature from $750^{\circ}C$ to $950^{\circ}C$. The crystallization behavior of the specimens depended on the heat-treatment temperature, which could be evaluated by differential thermal analysis (DTA), Fourier transform infrared spectroscopy (FT-IR), and X-ray diffraction (XRD) analysis by the Rietveld-reference intensity ratio (RIR) combined procedure. With an increase of the heat-treatment temperature, the thermal conductivity and thermal diffusivity of the heat-treated specimens increased. These results could be attributed to the increase of crystallization with heat-treatment temperature. However, the specific heat capacity of the heat-treated specimens was not affected by the heat-treatment temperature. The thermal conductivities measured from $25^{\circ}C$ to $100^{\circ}C$ were also discussed for application to lighting-emitting diode (LED) packages and substrate materials.

• Journal of IKEEE
• /
• v.23 no.3
• /
• pp.793-799
• /
• 2019

In this study, the diffusion process and the thermal energy distribution gradient of the sensor were confirmed by using the finite element analysis program (COMSOL) of the mesh method to analyze the thermal diffusion in the wearable fabric (Nylon) + MWCNT gas sensor. To analyze the diffusion process of thermal energy, the structure of the gas sensor was modeled in a two dimension plane. The proposed modeling was presented with the characteristic value for the component of the sensor, and the gas sensor designed using the mesh finite element method (FEM) was proposed and analyzed by suggesting the one-way partial differential equation in the governing equation to know the degree of thermal energy diffusion and the thermal energy gradient. In addition, the temperature gradient 10[K/mm] of the anode-cathode electrode layer and the gas detection unit was investigated by suggesting the heat velocity transfer equation.