• Title/Summary/Keyword: Diamond Analysis

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Improvement of Coating Properties of Metal/diamond Composite Through Ni Coated Diamond in the Kinetic Spraying Process (저온 분사 공정에서 니켈이 코팅된 다이아몬드 적용을 통한 금속/다이아몬드 복합재료의 코팅성 향상)

  • Na, Hyun-Taek;Bae, Gyu-Yeol;Kang, Ki-Cheol;Kim, Hyung-Jun;Lee, Chang-Hee
    • Journal of the Korean institute of surface engineering
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    • v.41 no.6
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    • pp.255-263
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    • 2008
  • Generally, deposition mechanism of diamond particle is mainly embedding effect in the kinetic spray process. Accordingly, in spite of high cost, helium gas was employed as process gas to get high diamond fraction in the composite coating. In this study, the deposition behavior of bronze/diamond by kinetic spray process was compared using different process gas (helium and nitrogen). Bare (mean size of $5{\mu}m$, $20{\mu}m$) and nickel coated diamond (mean size of $26{\mu}m$) were deposited on Al 6061-T6 substrate with fixed process temperature and pressure. For comparison with experimental results, plastic deformation behavior of nickel layer was simulated by finite element analysis (using ABAQUS/Explicit 6.7-2). The size, broken ratio, and fraction of diamond in the composite coating were analyzed through scanning electron microscopy and image analysis method. The uniform distribution and deposition efficiency of diamond particles in the coating layer could be achieved by tailoring the physical properties of the feedstock.

A Study on New Twist-Diamond Wire Characteristics for Improving Processing Performance (트위스트 다이아몬드 와이어의 성능향상을 위한 특성평가에 관한 연구)

  • Park, Chang-Yong;Kweon, Hyun-Kyu;Peng, Bo;Jung, Bong-Gyo
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.15 no.1
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    • pp.26-33
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    • 2016
  • In this study, a new method to develop a fixed diamond wire for silicon wafer machining by the multi-wire cutting method was developed. The new twist diamond wire has improved performance with high breaking strength and chip flutes structure. According to these characteristics, the new twist diamond wire can be used in the higher speed multi-wire cutting process with a long lifetime. Except the design of the new structure, the twist diamond wire is coating by electroless-electroplating process. It is good for reducing breakage and the falling-off of diamond grains. Based on the silicon material removal mechanism and performance of the wire-cutting machine, the optimal processing condition of the new twist diamond wire has been derived via mathematical analysis. At last, through the tensile testing and the machining experiments, the performance of the twist diamond wire has been obtained to achieve the development goals and exceed the single diamond wire.

Stochastic Analysis of the Diamond Particle Distribution on the Surface of Circular Diamond Saw Blade (원형 다이아몬드 톱의 세그먼트 표면에서의 다이아몬드 입자 분포의 확률적인 해석)

  • 이현우;변서봉;정기정;김용석
    • Journal of Powder Materials
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    • v.10 no.3
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    • pp.201-208
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    • 2003
  • Distributions of diamond particles protruding on the surface of worn diamond segments in circular saw has been investigated. Scanning electron microscope was used to examine the worn ,surface and radial saw blade wear and grinding ratio was measured. The number of protruded diamond particle was approximately 50% of the total number of particles, and that was independent of diamond particle concentration and table speed. It was also noted that the inter-particle distance did not follow a symmetric function like Gaussian distribution function, instead it fitted well with a probability density function based on gamma function. The distribution of inter-particle spacing, therefore, was analyzed using a gamma function model.

Characteristics of Diamond Films Deposited on Cemented Tungsten Carbide Substrate (초경합금기판 위에 성장되는 다이아몬드 막의 특성)

  • 김봉준;박상현;박재윤
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.53 no.7
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    • pp.387-394
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    • 2004
  • Diamond films were deposited on the cemented tungsten carbide WC-Co cutting insert substrates by using both microwave plasma chemical vapor deposition(MWPCVD) and radio frequency plasma chemical vapor deposition (RFPCVD) from $CH_4$$-H_2$$-O_2$ gas mixture. Scanning electron microscopy and X-ray diffraction techniques were used to investigate the microstructure and phase analysis of the materials and Raman spectrometry was used to characterize the quality of the diamond coating. Diamond films deposited using MWPCVD from $CH_4$$-H_2$$-O_2$ gas mixture show a dense, uniform, well faceted and polycrystalline morphology. The compressive stress in the diamond film was estimated to be (1.0∼3.6)$\pm$0.9 GPa. Diamond films which were deposited on the WC-Co cutting insert substrates by RFPCVD from $CH_4$$-H_2$$-O_2$ gas mixture show relatively good adhesion, very uniform, dense and polycrystalline morphology.

Dislocation Analysis of CVD Single Crystal Diamond Using Synchrotron White Beam X-Ray Topography (가속기 백색광 X-Ray Topography를 이용한 CVD 단결정 다이아몬드 내부 전위 분석)

  • Yu, Yeong-Jae;Jeong, Seong-Min;Bae, Si-Young
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.32 no.3
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    • pp.192-195
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    • 2019
  • Single-crystal diamond obtained by chemical vapor deposition (CVD) exhibits great potential for use in next-generation power devices. Low defect density is required for the use of such power devices in high-power operations; however, plastic deformation and lattice strain increase the dislocation density during diamond growth by CVD. Therefore, characterization of the dislocations in CVD diamond is essential to ensure the growth of high-quality diamond. In this work, we analyze the characteristics of the dislocations in CVD diamond through synchrotron white beam X-ray topography. In estimate, many threading edge dislocations and five mixed dislocations were identified over the whole surface.

Gas Phase Analysis of the Diamond CVD Reaction by Hot Filament Method (열필라멘트법에 의한 다이아몬드 CVD반응의 기상 조성 분석)

  • 서문규
    • Journal of the Korean Ceramic Society
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    • v.35 no.11
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    • pp.1233-1239
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    • 1998
  • Gas phase compositions of the hot filament-assisted diamond CVD reaction were analyzed by on-line quadrupole mass analysis(QMA) technique. D2 isotope experiments showed that methance molecules were decomposed into atomic state and then recombined in to acetylene during transport the probe line. Although acetylene or ethylene was supplied instead of methane similar gas compositions were obtained when filament temperature was above 1500$^{\circ}C$ Therefore this system could be assumed near thermal equilibrium state. Filament temperature and reaction pressure variation experiments exhibited the same tendency between acetylene concentration and diamond growth rate and these results implied that acetylene molecule played the role of the reactive species in the diamond CVD reaction.

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Mechanics of Diamond Blade Sawing (다이아몬드 컷터 블레이드를 사용한 절단작업의 절단저항력 해석)

  • Seo, Young-Il;Choi, Hwan;Lee, Jong-Chan
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1995.04b
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    • pp.69-74
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    • 1995
  • A theoretical analysis is presented on the mechanics of diamond blade sawing. Experimental results are also presented, which show the effects of cutting variables such as cutting speed, feed speed, cutting area, and concentration of deamond blade on the cutting forces. The analytical results aggreed well with experimental ones.

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Mechanics of Diamond Blade Sawing (다이아몬드 블레이드를 사용한 절단가공이 절단저항력 해석)

  • Seo, Young-Il;Choi, Hwan;Lee, Jong-Chan
    • Journal of the Korean Society for Precision Engineering
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    • v.13 no.1
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    • pp.84-90
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    • 1996
  • A theoretical analysis is presented on the mechanics of diamond blade sawing. The normal and tangential components of cutting force are calculated. Experimental results are also presented, which show the effects of cutting variables such as cutting speed, feed speed, cutting area, and concentration of diamond blade on the cutting forces. The experimental results are found to be in good agreement with those predicted by the analytical calculation.

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Chromium Carbide Coating on Diamond Particle Using Molten Salts (용융염을 이용한 다이아몬드 표면의 크롬카바이드 코팅)

  • Jeong, Young-Woo;Kim, Hwa-Jung;Ahn, Yong-Sik;Choi, Hee-Lack
    • Korean Journal of Materials Research
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    • v.28 no.7
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    • pp.423-427
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    • 2018
  • For diamond/metal composites it is better to use diamond particles coated with metal carbide because of improved wettability between the diamond particles and the matrix. In this study, the coating of diamond particles with a chromium carbide layer is investigated. On heating diamond and chromium powders at $800{\sim}900^{\circ}C$ in molten salts of LiCl, KCl, $CaCl_2$, the diamond particles are coated with $Cr_7C_3$. The surfaces of the diamond powders are analyzed using X-ray diffraction and scanning electron microscopy. The average thickness of the $Cr_7C_3$ coating layers is calculated from the result of the particle size analysis. By using the molten salt method, the $Cr_7C_3$ coating layer is uniformly formed on the diamond particles at a relatively low temperature at which the graphitization of the diamond particles is avoided. Treatment temperatures are lower than those in the previously proposed methods. The coated layer is thickened with an increase in heating temperature up to $900^{\circ}C$. The coating reaction of the diamond particles with chromium carbide is much more rapid in $LiCl-KCl-CaCl_2$ molten salts than with the molten salts of $KCl-CaCl_2$.