• Title/Summary/Keyword: Deposition pressure

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양축 정렬된 Ni기판 위에 MOCVD법에 의한 YBCO 초전도 선재용 $CeO_2$ 완충층의 증착 (Deposition of $CeO_2$ buffer layer for YBCO coated conductors on biaxially textured Ni substrate by MOCVD technique)

  • 김호진;주진호;전병혁;정충환;박순동;박해웅;홍계원;김찬중
    • 한국초전도ㆍ저온공학회논문지
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    • 제4권2호
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    • pp.21-26
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    • 2002
  • Textured CeO2 buffer layers for YBCO coated conductors were deposited on biaxially textured Ni substrate by metalorganic chemical vapor deposition (MOCVD). The degree of texture of deposited $CeO_2$ films was strong1y dependent on the deposition temperature (Td) and oxygen Partial Pressure(PO2). ($\ell$00) textured $CeO_2$ films were well deposited at T=500~52$0^{\circ}C$. PO2=0.90~3.33 Torr. The surface morphology showed that the films consisted of columnar CeO2 films grown from the Ni substrates. The root mean square roughness of CeO$_2$ films estimated by atomic force microscopy(AFM) increased as the deposition temperature(Td) increa- sed. The growth rate of the $CeO_2$ films deposited at T=52$0^{\circ}C$ and PO2=2.30 Torr was 150~200 nm/min that was much faster than that of other Physical deposition methods.

다결정 $Si_{1-x}Ge_x$박막 증착에 관한 연구(I) 증착변수에 따른 증착속도 및 Ge조성 변화 (A study on the Poly-$Si_{1-x}Ge_x$ thin film deposition (I) Variation of the deposition rate and Ge composition with deposition parameters)

  • 이승호;어경훈;소명기
    • 한국결정성장학회지
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    • 제7권4호
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    • pp.578-588
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    • 1997
  • RTCVD법으로 $SiH_4$$GeH_4$ 가스를 이용하여 oxidized Si 위에 SiH$_4$: $GeH_4$ flow ratio(1 : 0.1~2 : 1), 증착온도(400~$600^{\circ}C$) 그리고 증착압력(1~50 torr)인 조건에서 다결정 $Si_{1-x}Ge_x$박막을 증착하여, 증착변수 변화에따른 $Si_{1-x}Ge_x$ 박막의 Ge 조성 변화와, Ge 조성이 증착속도에 미치는 영향 등에 대해 살펴보았다. 실험결과, 증착온도와 Ge 조성 증가에따라 증착속도는 증가하였으나 증착온도 증가에따라 Ge 조성이 감소하였다. 또한 증착압력 변화에따른 증착속도와 Ge조성 변화는, 증착압력 10 torr까지는 거의 직선적으로 증가하였으나 그이상에서는 서서히 증가함을 알 수 있었다. 이와같이 10 torr 이상의 증착압력에서 증착속도가 서서히 증가하는것은 물질전달 속도에 비해 표면반응 속도가 늦어져 나타난 현상으로 생각된다.

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Reactive RF 마그네트론 스퍼터링법으로 Si(100) 기판에 MgO박막 제조시 증착변수의 영향 (Effect of Deposition Parameters on MgO Thin Films on Si(100) Substrates by Reactive RF Magnetron Sputtering)

  • 이영준;백성기
    • 한국세라믹학회지
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    • 제31권6호
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    • pp.643-650
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    • 1994
  • Highly [100]-oriented MgO thin films were deposited on Si(100) single crystal substrates by reactive RF magnetron sputtering. The effects of substrate temperature, gas pressure, RF input powder, and gas composition on the characteristics of MgO thin films were studied. The higher substrate temperature and the lower operating pressure were, the better crystallinity of the deposited MgO thin films were. The influences of the RF input power and oxygen to argon ratio were very complex. The physical characteristics of the films changed dramatically with deposition conditions. Highly smooth and epitaxial MgO films were obtained at the deposition conditions as follows; subatrate temperature, $600^{\circ}C$; operating pressure, 10 mtorr; RF input power density, 2 W/$\textrm{cm}^2$; the percentage of oxygen, 10%.

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DC 반응성 스퍼터링된 TiN 박막의 구조적 및 전기적 특성 (Structural and Electrical Properties of Reactively Sputtered Titanium Nitride Films)

  • 류성용;오원욱;백수현;신두식;오재응;김영남;심태언;이종길
    • 전자공학회논문지A
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    • 제29A권8호
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    • pp.49-55
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    • 1992
  • We Have investigated the properties of the titanium nitrite films widely used in VLSI devices as diffusion barrier in Al-based metallization. TiN films were formed by reactive sputtering from Ti target in Ar-N$_2$ mixtures, varying deposition parameters such as N$_2$ partial pressure, substrate temperature, power, and total pressure. All the samples received the heat treatment at 45$0^{\circ}C$ for 30 min. The resulting films are characterized by mechanical stylus($\alpha$-step), x-ray diffraction(XRD), scanning electron microscopy(SEM), and four point probe method. The Tin film properties strongly depend on the deposition condition. The stoichiometry and Ti deposition rate are critically affected by nitrogen partial pressure, and the resistivity, in particular, is dependent on both the substrate temperature and sputtering power.

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PLD 법으로 제작된 PLZT 박막의 산소압에 따른 구조 및 전기적 특성 (Oxygen Pressure Dependence of Structural and Electrical Characteristics of PLZT Thin Films Prepared by a PLD)

  • 장낙원
    • Journal of Advanced Marine Engineering and Technology
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    • 제30권8호
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    • pp.927-933
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    • 2006
  • The structural and electrical characteristics of PLZT thin films fabricated onto $Pt/IrO_2/Ir/Ti/SiO_2/Si$ substrates by a pulsed laser deposition were investigated to develop the high dielectric thin films for capacitor layer of semiconductor memory devices The slim region 14/50/50 PLZT thin films were fabricated by PLD and estimated the characteristics for memory application 14/50/50 PLZT thin films have crystallize into perovskite structure at the $600^{\circ}C$ deposition temperature, 200 mTorr of oxygen pressure, and 2 $J/cm^2$ of laser energy density. In this condition PLZT thin films had the dielectric constant as high as 985, storage charge density 8.17 ${\mu}C/cm^2$ and charging time 0.20 ns. Leakage current density was less than $10^{-10}A/cm^2$ up to 5 V bias voltage.

Influence of Mg Vapor Pressure on the $MgB_2$/Carbon Fiber Fabricated by Physical Vapor Deposition method

  • Li, Xiang;Ha, Hong-Soo;Kim, Cheol-Jin
    • 한국초전도ㆍ저온공학회논문지
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    • 제13권4호
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    • pp.5-9
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    • 2011
  • We have fabricated the superconducting $MgB_2$/carbon fiber by physical vapor deposition method. Mg (Magnesium) and B (Boron) were simultaneously deposited on the carbon fiber using the RF-sputtering and thermal evaporation, respectively. To ensure the relatively high vapor pressure of Mg at the growth region and the subsequent phase stability of $MgB_2$ at the deposition temperature, inverted funnel-like guide made of Mg-foil was employed while one side of the guide were open for the sputtered B flux. Mg vapor pressure should be controlled precisely to secure the complete reaction. The $MgB_2$/carbon fiber showed a uniformly deposited thin layer with dense and well-formed grains. The $MgB_2$/carbon fibers in this study showed $T_c$~37.5K, $J_c$ ~ $2{\times}10^4\;A/cm^2$ in the 20K, 0T.

감압화학증착의 이단계 성장으로 실리콘 기판 위에 증착한 in-situ 인 도핑 다결정 실리콘 박막의 미세구조 조절 (Manipulation of Microstructures of in-situ Phosphorus-Doped Poly Silicon Films deposited on Silicon Substrate Using Two Step Growth of Reduced Pressure Chemical Vapor Deposition)

  • 김홍승;심규환;이승윤;이정용;강진영
    • 한국전기전자재료학회논문지
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    • 제13권2호
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    • pp.95-100
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    • 2000
  • For the well-controlled growing in-situ heavily phosphorus doped polycrystalline Si films directly on Si wafer by reduced pressure chemical vapor deposition, a study is made of the two step growth. When in-situ heavily phosphorus doped Si films were deposited directly on Si (100) wafer, crystal structure in the film is not unique, that is, the single crystal to polycrystalline phase transition occurs at a certain thickness. However, the well-controlled polycrtstalline Si films deposited by two step growth grew directly on Si wafers. Moreover, the two step growth, which employs crystallization of grew directly on Si wafers. Moreover, the two step growth which employs crystallization of amorphous silicon layer grown at low temperature, reveals crucial advantages in manipulating polycrystal structures of in-situ phosphorous doped silicon.

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Effect of residual oxygen in a vacuum chamber on the deposition of cubic boron nitride thin film

  • Oh, Seung-Keun;Kang, Sang Do;Kim, Youngman;Park, Soon Sub
    • Journal of Ceramic Processing Research
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    • 제17권7호
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    • pp.763-767
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    • 2016
  • The structural characterization of cubic boron nitride (c-BN) thin films was performed using a B4C target in a radio-frequency magnetron sputtering system. The deposition processing conditions, including the substrate bias voltage, substrate temperature, and base pressure were varied. Fourier-transform infrared spectroscopy and X-ray photoelectron spectroscopy were used to analyze the crystal structures and chemical binding energy of the films. For the BN film deposited at room temperature, c-BN was formed in the substrate bias voltage range of -400 V to -600 V. Less c-BN fraction was observed as the deposition temperature increased, and more c-BN fraction was observed as the base pressure increased.

저압 CVD에 의한 $Si_{0.8}Ge_{0.2}$ epitaxial growth에 대한 Phosphorus doping 효과 (Phosphorus doping effect on $Si_{0.8}Ge_{0.2}$ epitaxial growth by LPCVD)

  • 이철진;엄문종;성만영
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1997년도 추계학술대회 논문집 학회본부
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    • pp.314-316
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    • 1997
  • We have studied the epitaxial growth and electrical properties of $Si_{0.8}Ge_{0.2}$, films on Si substrates at $550^{\circ}C$ by LPCVD. In a low $PH_3$, partial pressure region such as below 1.25 mPa, the phosphorus doping concentration increased proportionally with increasing $PH_3$ partial pressure while the deposition rate and the Ge fraction x were constant. In a higher $PH_3$ partial pressure region, the phosphorus doping concentration and the deposition rate decreased, while the Ge fraction slightly increased. The dependence of P incorporation rate on the $PH_3$ partial pressure was similar to the phosphorus doping concentration. According to test results, it suggests that high surface coverage of phosphorus atoms suppress both the $SiH_4$ adsorption/reaction and the $GeH_4$ adsorption/reaction on the surfaces, and the effect is more stronger on $SiH_4$ than on $GeH_4$. In a higher $PH_3$ partial pressure region, the deposition is largely controlled by surface coverage effect of phosphorus atoms.

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입자층 에어로졸여과의 과도거동에 관한 실험연구 : 압력강하에 대한 입자 퇴적의 영향 (An Experimental Study on Transient Behavior of Granular Aerosol Filtration : Effect of Particle Deposition on Pressure Drop)

  • 정용원
    • 한국대기환경학회지
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    • 제13권3호
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    • pp.193-205
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    • 1997
  • Experiments on granular filtration of polydispersed aerosols were conducted to determine the changes in pressure drop necessary to maintain a given gas flow rate as filter becomes clogged with deposited particles. Among the various variables which affect the increase in the pressure drop during the filtration, the most important one was found to be the size of the deposited aerosol particles. It was shown that for a given extent of the total deposition, the extent of increase in pressure drop increases with the decrease of the deposited aerosol size. For the general case where the deposited particles have different sizes, a procedure was proposed for correlating and predicting experimental results on pressure drop. This procedure was found applicable to bidispersed aerosols and polydispersed aerosols.

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