• Title/Summary/Keyword: Delamination strength

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Fabrication and Electrical Insulation Property of Thick Film Glass Ceramic Layers on Aluminum Plate for Insulated Metal Substrate (알루미늄 판상에 글라스 세라믹 후막이 코팅된 절연금속기판의 제조 및 절연특성)

  • Lee, Seong Hwan;Kim, Hyo Tae
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.4
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    • pp.39-46
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    • 2017
  • This paper presents the fabrication of ceramic insulation layer on metallic heat spreading substrate, i.e. an insulated metal substrate, for planar type heater. Aluminum alloy substrate is preferred as a heat spreading panel due to its high thermal conductivity, machinability and the light weight for the planar type heater which is used at the thermal treatment process of semiconductor device and display component manufacturing. An insulating layer made of ceramic dielectric film that is stable at high temperature has to be coated on the metallic substrate to form a heating element circuit. Two technical issues are raised at the forming of ceramic insulation layer on the metallic substrate; one is delamination and crack between metal and ceramic interface due to their large differences in thermal expansion coefficient, and the other is electrical breakdown due to intrinsic weakness in dielectric or structural defects. In this work, to overcome those problem, selected metal oxide buffer layers were introduced between metal and ceramic layer for mechanical matching, enhancing the adhesion strength, and multi-coating method was applied to improve the film quality and the dielectric breakdown property.

Adhesive Strength and Electrochemical Properties of Li(Ni0.5Co0.2Mn0.3)O2Electrodes with Lean Binder Composition (바인더 함량에 따른 Li(Ni0.5Co0.2Mn0.3)O2 전극의 접착력 및 전기화학 성능에 관한 연구)

  • Roh, Youngjoon;Byun, Seoungwoo;Ryou, Myung-Hyun;Lee, Yong Min
    • Journal of the Korean Electrochemical Society
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    • v.21 no.3
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    • pp.47-54
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    • 2018
  • To maximize the areal capacity($mAh\;cm^{-2}$) of $LiNi_{0.5}Co_{0.2}Mn_{0.3}O_2$(NCM523) electrode with the same loading level of $15mg\;cm^{-2}$, three NCM523 electrodes with 4, 2, and 1 wt% poly(vinylidene fluoride)(PVdF) binder content are fabricated. Due to the delamination issue of electrode composite at the edge during punching process, the 1 wt% electrode is excluded for further evaluation. When the PVdF binder content decreases from 4 to 2 wt%, both adhesion strength and shear stress decrease from 0.4846 to $0.2627kN\;m^{-1}$ by -46% and from 3.847 to 2.013 MPa by -48%, respectively. Regardless of these substantial decline of mechanical properties, their initial electrochemical properties such as initial coulombic efficiency and voltage profile are almost the same. However, owing to high loading level, the 2 wt% electrode not only exhibits worse cycle performance than the 4 wt% electrode, but also cannot maintain its mechanical integrity only after 80 cycles. Therefore, if the binder content is reduced to increase the area capacity, the mechanical properties as well as the cycle performance must be carefully evaluated.

Durability Evaluation of Inorganic-Impregnated Concrete Exposed to Long-Term Chloride Exposure Test (무기계 침투제를 적용한 콘크리트의 장기폭로실험을 통한 염해 내구성 평가)

  • Kwon, Seung-Jun;Park, Sang-Soon;Lho, Byeong-Cheol
    • Journal of the Korea Concrete Institute
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    • v.20 no.3
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    • pp.283-290
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    • 2008
  • The repair technique using surface impregnation of reactive compound is so effective for deteriorated concrete structures that many researches are recently focused on these works. Particularly, inorganic impregnant is regarded as ecofriendly material because there is no air-pollution during manufacturing process as well as field coating works. Furthermore, The delamination between old concrete and impregnated surface does not occur, resulting from different material characteristics. In order to evaluate the durability performance of surface-impregnated concrete, durability evaluation through the long-term exposure tests is significant, however, experiments are usually limited to the temporary and qualitative laboratorial scope. In this study, durability characteristics for inorganic and organic/inorganic impregnated concrete specimens are evaluated through longterm chloride exposure test. The specimens with 21MPa and 34MPa strength have been prepared and exposed to chloride attack in the atmospheric, tidal, and submerged conditions. Evaluation for compressive strength, chloride penetration, and electrical potential (half cell potential) for steel corrosion are performed for the specimens exposed for 2 years. From the results, no distinct strength gaining is observed but the resistance to chloride penetration and steel corrosion is evaluated to be improved through surface impregnation. The more improved resistance to chloride attack is measured in the inorganic impregnated concrete and the results from atmospheric condition show more improved resistance to chloride attack than those from submerged and tidal condition.

Flexural Strength Analysis of RC T-Beams Strengthened Using Fiber Sheets (섬유시트로 보강된 T형 철근콘크리트보의 휨 강도 해석)

  • Park, Tae-Hyo;Lee, Gyu-Chul
    • Journal of the Korea Concrete Institute
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    • v.15 no.2
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    • pp.234-245
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    • 2003
  • Most of the concrete bridge structures are exposed to damage due to the excessive traffic loading and the aging of the structure. The damage of concrete causes the further deterioration of the function in the concrete structure due to corrosion of the reinforced bars and decohesion between the concrete and the reinforced bar. The quick rehabilitation of the damaged concrete structures has become of great importance in the concrete structural system in order to avoid the further deterioration of the structures. Recently fiber sheets are used for strengthening the damaged concrete structures due to its many advantages such as its durability, non-corrosive nature, low weight, ease of application, cost saving, control of crack propagation, strength to thickness ratio, high tensile strength, serviceability and aesthetic. However, the lack of analytical procedures for assessing the nominal moment capacity by the fiber sheet reinforcement leads to difficulties in the effective process of decisions of the factors in the strengthening procedure. In this work, flexural strengthening effects by fiber sheets bonded on bottom face of the member are studied for the reinforced concrete T beam. In addition, auxiliary flexural strengthening effects by U-type fiber sheets bonded on bottom and side faces of the member to prevent delamination of the bottom fiber sheet are theoretically investigated. The analytical solutions are compared with experimental results of several references to verify the proposed approach. It is shown that the good agreements between the predicted results and experimental data are obtained.

Revision of Repair Materials Performance Requirement for Concrete Structures (콘크리트 구조물 단면복구공사 보수재료 품질기준개선)

  • Lee, Il Keun;Kim, Ki Hwan;Kim, Hong Sam;Yun, Sung Hwan;Kim, Woo Seok
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.43 no.1
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    • pp.9-20
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    • 2023
  • For highway concrete structures, the deterioration of the structure is accelerated due to the increase in the use of deicing materials, and sectional repair work is being frequently carried out to restore performance. However, after the repair work, re-damage such as cracks, delamination, and poor bond performance is exhibited in the repaired sectional area. In this study, overseas repair material requirements were first analyzed, and present domestic requirements were improved repair material performance through field surveys of common concrete structures, laboratory experiments, and test construction on a disused concrete bridge. In addition, performancebased quality requirements were presented so that all materials that meet the required performance can be applied, and different test methods for each material were unified into concrete test methods for consistent test results analysis. The considered performance requirements were compression strength, bending strength, and bond strength for structural properties, and length change rate, crack resistance, thermal expansion coefficient, and elasticity coefficient were for dimensional behavior. For resistance to chloride penetration resistance and freeze-thaw resistance were presented as durability. The proposed requirements for concrete repair materials are expected to contribute to the improvement of the quality of concrete sectional repair work in Korea.

Two Dimensional Size Effect on the Compressive Strength of Composite Plates Considering Influence of an Anti-buckling Device (좌굴방지장치 영향을 고려한 복합재 적층판의 압축강도에 대한 이차원 크기 효과)

  • ;;C. Soutis
    • Composites Research
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    • v.15 no.4
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    • pp.23-31
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    • 2002
  • The two dimensional size effect of specimen gauge section ($length{\;}{\times}{\;}width$) was investigated on the compressive behavior of a T300/924 $\textrm{[}45/-45/0/90\textrm{]}_{3s}$, carbon fiber-epoxy laminate. A modified ICSTM compression test fixture was used together with an anti-buckling device to test 3mm thick specimens with a $30mm{\;}{\times}{\;}30mm,{\;}50mm{\;}{\times}{\;}50mm,{\;}70mm{\;}{\times}{\;}70mm{\;}and{\;}90mm{\;}{\times}{\;}90mm$ gauge length by width section. In all cases failure was sudden and occurred mainly within the gauge length. Post failure examination suggests that $0^{\circ}$ fiber microbuckling is the critical damage mechanism that causes final failure. This is the matrix dominated failure mode and its triggering depends very much on initial fiber waviness. It is suggested that manufacturing process and quality may play a significant role in determining the compressive strength. When the anti-buckling device was used on specimens, it was showed that the compressive strength with the device was slightly greater than that without the device due to surface friction between the specimen and the device by pretoque in bolts of the device. In the analysis result on influence of the anti-buckling device using the finite element method, it was found that the compressive strength with the anti-buckling device by loaded bolts was about 7% higher than actual compressive strength. Additionally, compressive tests on specimen with an open hole were performed. The local stress concentration arising from the hole dominates the strength of the laminate rather than the stresses in the bulk of the material. It is observed that the remote failure stress decreases with increasing hole size and specimen width but is generally well above the value one might predict from the elastic stress concentration factor. This suggests that the material is not ideally brittle and some stress relief occurs around the hole. X-ray radiography reveals that damage in the form of fiber microbuckling and delamination initiates at the edge of the hole at approximately 80% of the failure load and extends stably under increasing load before becoming unstable at a critical length of 2-3mm (depends on specimen geometry). This damage growth and failure are analysed by a linear cohesive zone model. Using the independently measured laminate parameters of unnotched compressive strength and in-plane fracture toughness the model predicts successfully the notched strength as a function of hole size and width.

A Study on the Bonding Residual Thermal Stress Analysis of Dissimilar Materials Using Boundary Element Method (경계요소법에 의한 이종재료 접합 잔류열응력의 해석)

  • Yi, Won;Yu, Yeong-Chul;Jeong, Eui-Seob;Yun, In-Sik
    • Journal of the Korean Society for Nondestructive Testing
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    • v.15 no.4
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    • pp.540-548
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    • 1996
  • In general residual stress is measured by X-ray diffraction method but in case of bonding residual thermal stress it is inadequate technique to examine the stress singularity. Therefore Two-dimensional elastic boundary element analyses were carried out to investigate the residual thermal stress and stress singularity of bonding interface in Al/Epoxy. This boundary element results were compared with the strain gauge measurements. The effects of different interface models, sub-element and adherend thickness are presented and discussed. On the basis of the obtained results, interface delamination causing by normal stress is expected and stress singularity is observed more intensively increasing with adherend thickness. It is concluded that the bonding strength of Al/Epoxy interface can be estimated correctly by taking into account the stress singularity at the edge of the interface.

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Interaction of cracks and precipitate particles on the REBCO superconducting layers of practical CC tapes through fractographic observations

  • de Leon, Michael;Diaz, Mark A.;Shin, Hyung-Seop
    • Progress in Superconductivity and Cryogenics
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    • v.22 no.3
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    • pp.7-12
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    • 2020
  • Electromechanical properties of REBCO CC tapes are known to be limited by defects (cracks) that form in the brittle REBCO layer. These defects could be inherently acquired during the CC tapes' manufacturing process, such as slitting, and which can be initiated at the CC tapes' edges. If propagated and long enough, they are believed to cause critical current degradation and can substantially decrease the delamination strength of CC tapes. Currently, commercially available CC tapes from various manufacturers utilize different growth techniques for depositing the REBCO layers on the substrates in their CC tapes preparation. Their epitaxial techniques, unfortunately, cannot perfectly avoid the formation of particles, in which sometimes acts as current blocking defects, known as outgrowths. Collective research regarding the composition, size, and formation of these particles for various CC tapes with different deposition techniques are particularly uncommon in a single study. Most importantly, these particles might interact in one way or another to the existing cracks. Therefore, systematic investigation on the interactions between the cracks' development mechanism and particles on the REBCO superconducting layers of practical CC tapes are of great importance, especially in the design of superconducting devices. Here, a proper etching process was employed for the CC tapes to expose and observe the REBCO layers, clearly. The scanning electron microscope, field emission scanning microscope, and energy-dispersive x-ray spectroscopy were utilized to observe the interactions between cracks and particles in various practical CC tapes. Particle compositions were identified whether as non-superconducting or superconducting and in what manner it interacts with the cracks were studied.

Fatigue Fracture Assessment of Honeycomb Composite Side-Wall Panel Joint for the KTX Tilting Car Body (틸팅차량용 KTX 차체의 하니컴복합재 측벽판 체결부의 피로파괴평가)

  • Jeong, Dal-Woo;Kim, Jung-Seok;Choi, Nak-Sam
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.34 no.1
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    • pp.55-60
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    • 2010
  • The honeycomb composite joint structure designed for application to a tilting KTX railroad car body is subjected to bending loads of a cantilever type. Honeycomb sandwich composite panel-joint attached in the real tilting car body was fabricated and sectioned as several beam-joint specimens for the bending test. The fracture behaviors of these specimens under static loads were different from those under cyclic loads. Static bending loads caused shear deformation and fracture in the honeycomb core region, while fatigue cyclic bend loading caused delamination along the interface between the composite skin and the honeycomb core, and/or caused a fracture in the welded part jointed with the steel under-frame. These fracture behaviors could occur in other industrial honeycomb composite joints with similar sub-structures, and be used for improving design parameters of a honeycomb composite joint structure.

Relations Between Impact Damage and Ply Angle Under Same Impact Energy Condition (同一한 衝擊에너지 條件下의 CFRP 斜交積層板의 衝擊損傷과 配向角의 關係)

  • ;笠野英秋
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.16 no.10
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    • pp.1824-1832
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    • 1992
  • This study investigated the compressive Young's modulus and the impactinduced damage of CFRP angle-ply laminate under same impact energy condition. The specimens of angle-ply laminate composites [0.deg.$_{6}$/ .theta..deg.$_{10}$/ 0.deg.$_{6}$] with .theta..deg. =30.deg., 45.deg., 60.deg. and 90.deg. were employed, and damaged by steel balls of diameter of 5mm and 10mm propelled by air gun type impact testing machine. The impact damaged zones were observed through a scanning acoustic microscope(SAM), and their cross-sections were observed through a scanning electron microscope(SEM). The compressive Young's moduli before and after impact were measured, and compared with the theoretical values calculated. The results obtained were as follows: (1) The damage areas on the interfacial boundaries showed more severe change on the back side interface than on the impact side interface with increasing ply-angle. (2) The damage areas on the interfacial boundaries became larger with increasing impact velocity or ply-angle. (3) The impact damaged zone showed the delamination on the interfacial boundaries and transverse cracks inside laminas. (4) The impact damaged zone was affected by the impactor size and speed or ply-angle under same impact energy condition. (5) Compressive Young's moduli before and after impact were lower than theoretical value, but showed a similar change according to ply-angle. (6) Compressive Young's moduli after impact were higher than those before impact, but there was no remarkable change in apparent compressive modulus after impact.t.act.