• 제목/요약/키워드: Degree of cure

검색결과 168건 처리시간 0.025초

백수의 수질에 따른 라이너지의 AKD 사이징 (Effect of White Water Quality on AKD Sizing of Linerboard)

  • 이학래;서만석;신종호;윤혜정
    • 펄프종이기술
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    • 제38권2호
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    • pp.9-15
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    • 2006
  • Neutral sizing is required for linerboard to solve the troubles in strength and process caused by recycled raw materials. AKD sizing efficiency can be influenced by process condition like white water quality, fines retention and so on. Therefore, this study was aimed to evaluate sizing performance of general and fast cure type AKDs using process water obtained from linerboard mill. To evaluate effect of process water quality on AKD sizing, white water was diluted with tap water at the different dilution ratios and UKP slurry was sized using the prepared water. Also, effects of inorganic and organic ion material on sizing were examined. When white water was used for stock forming, UKP sheet showed very low sizing degree. Sizing degree of sheet was increased with increase of dilution ratio because water quality was improved. Especially anionic organic material had a greater influence on AKD sizing than inorganic material. When white water quality was deteriorated, fast cure type AKD showed superior sizing performance to general type AKD.

양생조건에 따른 경화제 무첨가 에폭시수지 혼입 PMM의 경화특성 (Hardening Properties of Hardener-Free Epoxy-Modified Mortars by Curing Conditions)

  • 이재화;김주영;김완기
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2012년도 추계 학술논문 발표대회
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    • pp.255-257
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    • 2012
  • Epoxy resin without any hardener can harden in the presence of hydroxide ions in cement mortars and concretes at ambient temperature. The purpose of present study is to examine the hardening properties of hardener-free epoxy-modified mortars by curing conditions. The hardener-free epoxy-modified mortars using diglycidyl ether of A epoxy resin are prepared with various polymer-cement ratios, and subjected to initial moist/dry curing, initial steam(90℃) curing, initial steam/heat(80℃, 100℃) curing.As a result, degree of hardening of epoxy resin in initial moist/dry cured, initial steam cured and initial steam/heat(80℃) cured hardener-free epoxy-modified mortars is decreased with increasing polymer-cement ratio. However, it is markedly improved with additional dry-curing periods. On the other hand, regardless of the polymer-cement ratio and dry curing periods, degree of hardening of hardener-free epoxy-modified mortars with initial steam/heat(100℃) cure is over 95%.

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광섬유 센서를 이용한 에폭시 수지의 경화도 측정 (Study on Cure Monitoring for Epoxy Resin Using Fiber Optic Sensor System)

  • 김진봉;변준형;이창훈;이상관;엄문광
    • 한국복합재료학회:학술대회논문집
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    • 한국복합재료학회 2005년도 춘계학술발표대회 논문집
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    • pp.37-41
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    • 2005
  • The curing of thermoset resin is accompanied with the changes in chemical and physical properties. The cure monitoring techniques can be designed by tracing these property changes. This paper presents the cure monitoring technique with fiber optic sensors to detect the change of refractive index during the polymerization process of engineering epoxy resin. The fiber optic sensor system was developed to measure the reflection coefficient at the interface between the fiber optic and the resin. The correlation between the sensor output and the degree of cure was performed following Lorentz-Lorenz law. The isothermal data from the sensors are compared with the data from differential scanning calorimeter.

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치과 환자의 만족도에 영향을 미치는 요인 - 치과의원에서 기공실의 개설여부에 따라 - (Dental Patient's Satisfaction Degree Factors -Concerned with installation of dental clinics -)

  • 김남중;황경숙
    • 대한치과기공학회지
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    • 제22권1호
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    • pp.129-143
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    • 2000
  • With increasing number of dental patients, it is also increasing patient's desire to get better medical service. As the concern for improvement of dental medical service quality is growing, satisfaction degree of dental patients is becoming very important. This study was to investigate difference of patients' satisfaction degree concerned with installation of dental labs and the reason. The data for this study were collected through Self-Administered Questionnaires from 284 patients who had visited dental clinics more than two times. The results are as follows: Female respondents ratio was as twice much as male ones. And 54.2% of the respondents were found out to have completed university education. Dental clinics with dental labs scored higher than others in patients' satisfaction and recommendation willingness degree. Dental clinics without dental labs scored higher in patients' revisiting willingness degree. With simple Correlation Analyses it was found out that the most influential variable concerned with patients' general satisfaction degree was medical facility in dental clinics with dental labs, dentist ability to cure in dental clinics without dental labs. There were some discrepancies with other subordinate variables. Through Stepwise Multiful Regression Analyses it was found out that the most influential variable with patients' general satisfaction degree was dentist ability to cure in total and dental clinics without dental labs and medical facility in dental clinics with dental labs. There were also some discrepancies with other subordinate variables.

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광원의 종류에 따른 복합레진의 중합거동 및 중합률에 관한 연구 (THE POLYMERIZATION RATE AND THE DEGREE OF CONVERSION OF COMPOSITE RESINS BY DIFFERENT LIGHT SOURCES)

  • 류주희;이인복;유현미;김미자;석창인;권혁춘
    • Restorative Dentistry and Endodontics
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    • 제29권4호
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    • pp.386-398
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    • 2004
  • Objectives: The purpose of this study was to observe the reaction kinetics and the degree of polymerization of composite resins when cured by different light sources and to evaluate the effectiveness of the blue Light Emitting Diode Light Curing Units (LED LCUs) compared with conventional halogen LCUs. Materials and Methods: First, thermal analysis was performed by a differential scanning calorimeter (DSC). The LED LCU (Elipar Freelight, $320{\;}mW/\textrm{cm}^2$) and the conventional halogen LCU (XL3000, $400{\;}mV/\textrm{cm}^2$) were used in this study for curing three composite resins (SureFil, Z-250 and AEliteFLO). Second. the degree of conversion was obtained in the composite resins cured according to the above curing mode with a FTIR. Third, the measurements of depth of cure were carried out in accordance with ISO 4049 standards. Statistical analysis was performed by two-way ANOVA test at 95% levels of confidence and Duncan's procedure for multiple comparisons. Results: The heat of cure was not statistically different among the LCUs (p > 0.05). The composites cured by the LED (Exp) LCUs were statistically more slowly polymerized than by the halogen LCU and the LED (Std) LCU (p < 0.05). The composite resin groups cured by the LED (Exp) LCUs had significantly greater degree of conversion value than by the halogen LCU and the LED (Std) LCU (p =0.0002). The composite resin groups cured by the LED (Std) LCUs showed significantly greater depth of cure value than by the halogen LCU and the LED (Exp) LCU (p < 0.05).

The effect of thickness and translucency of polymer-infiltrated ceramic-network material on degree of conversion of resin cements

  • Barutcigil, Kubilay;Buyukkaplan, Ulviye Sebnem
    • The Journal of Advanced Prosthodontics
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    • 제12권2호
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    • pp.61-66
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    • 2020
  • PURPOSE. The aim of the present study was to determine the degree of conversion of light- and dual-cured resin cements used in the cementation of all-ceramic restorations under different thicknesses of translucent (T) and high-translucent (HT) polymer-infiltrated ceramic-network (PICN) material. MATERIALS AND METHODS. T and HT PICN blocks were prepared at 0.5, 1.0, 1.5, and 2.0 mm thicknesses (n=80). Resin cement samples were prepared with a diameter of 6 mm and a thickness of 100 ㎛. Light-cured resin cement was polymerized for 30 seconds, and dual-cure resin cement was polymerized for 20 seconds (n=180). Fourier transform infrared spectroscopy (FTIR) was used for degree of conversion measurements. The obtained data were analyzed with ANOVA and Tukey HSD, and independent t-test. RESULTS. As a result of FTIR analysis, the degree of conversion of the light-cured resin cement prepared under 1.5- and 2.0-mm-thick T and HT ceramics was found to be lower than that of the control group. Regarding the degree of conversion of the dual-cured resin cement group, there was no significant difference from the control group. CONCLUSION. Within the limitation of present study, it can be concluded that using of dual cure resin cement can be suggested for cementation of PICN material, especially for thicknesses of 1.5 mm and above.

유한요소법을 이용한 복합재 구조물의 3차원 경화 수치모사 (Three-dimensional cure simulation of composite structures by the finite element method)

  • 민경재;박훈철;윤광준
    • 한국항공우주학회지
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    • 제30권6호
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    • pp.39-45
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    • 2002
  • 본 논문에서는 복합재의 3차원 경화 수치모사를 위해 유한요소 정식과정을 제시하였다. 이 정식을 기초로 하여 유한요소 프로그램을 개발하였다. 개발한 프로그램을 검증하기 위해 참고문헌에 제시된 수치예제에 대한 해석을 수행하였다. 본 논문에서의 경화 수치모사결과가 측정된 경화온도와 잘 일치하였다. 본 3차원 경화 수치모사에서는 1, 2차원 해석과는 달리 복합재 구조물의 임의 지점에서의 수치모사 결과분석이 가능하다. 개발된 유한요소 프로그램을 이용하면 불규칙한 형상을 가진 복합재 구조물과 일정하지 않은 오토클레이브 내부 온도분포 하에서의 경화 수치모사를 할 수 있다.

Degree of conversion of resin composite cured by light through a translucent fiber posts

  • Urapepon, Somchai
    • The Journal of Advanced Prosthodontics
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    • 제6권3호
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    • pp.194-199
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    • 2014
  • PURPOSE. This study evaluated the depth of cure of resin composite cured by light through a translucent fiber post. MATERIALS AND METHODS. The opaque plastic tubes in various lengths of 2, 4, 6, 8, 10, 12, 14 mm. were filled with resin composite in which two different translucent fiber posts were inserted into the center and photo-polymerized for 40 seconds. The degree of conversion of the cured composite at bottom surface were examined using Fourier transform infrared attenuated total reflection spectrometer (FTIR/ATR) at 0.1, 0.5 and 1.0 mm apart from the post surface. RESULTS. The degree of conversion of the 0.1 mm, 0.5 mm, 1.0 mm apart from the post surface was highest at the 2 mm level and continuously decreased when the distance from the light source was increased and drastically decreased when the depth from the top of the post was greater than 4-6 mm. For each level, the highest degree of conversion was at 0.1 mm from the post surface and decreased continuously when the distance apart from the post surface was increased. CONCLUSION. The quantity of light transmission depends on the type of post and the light transmission capability of the post, especially after 4-6 mm depth and the area further apart from the post surface, are insufficient for clinical light activation of resin composite.

유리섬유/에폭시 후판 복합재료의 경화공정 및 압밀해석 (Cure simulation and Consolidation for a Thick Glass/Epoxy Laminate)

  • 오제훈;이대길
    • 대한기계학회논문집A
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    • 제24권11호
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    • pp.2853-2865
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    • 2000
  • During the curing process of thick glass/epoxy laminates, a substantial amount of temperature lag and overshoot at the center of the laminates is usually experienced due to the large thickness and low thermal conductivity of the glass/epoxy composites. Also, it takes a longer time for full and uniform consolidation. In this work, temperature, degree of cure and consolidation of a 20 mm thick unidirectional glass/epoxy laminate were investigated using an experiment and a 3-dimentional numerical analysis. From the experimental and numerical results, it was found that the experimentally obtained temperature profile agreed well with the numerical one, and the cure cycle recommended by the prepreg manufacturer should be modified to prevent a temperature overshoot and to obtain full consolidation.

코어용 레진의 두께가 중합에 미치는 영향 (Influence of Thickness on the Degree of Cure of Composite Resin Core Material)

  • 권병철;박정원
    • Restorative Dentistry and Endodontics
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    • 제31권5호
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    • pp.352-358
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    • 2006
  • 본 연구는 코어용 이중 중합 레진의 중합도에 미치는 두께의 영향과 빛이 감소된 깊은 와동에서 자가 중합에 의한 영향을 조사하고자 하였다. Luxacore Dual과 Luxacore Self (DMG Inc, Hamburg, Germany) 두 종류의 코어용 레진 수복재를 지름 10 mm, 두께가 2, 4, 6, 8 mm 의 Teflon mold에 주입하고 자가중합 시키거나 혹은 $500 mW/cm^2$의 광도로 제조자의 지시에 따라 중합 후 $37^{\circ}C$ 증류수에 24시간동안 저장하였다. 각 시편의 윗면과 아랫면에서 Knoop's hardness를 측정하였다. 결과는 ANOVA로 통계 분석 하였고 Tukey's test로 사후 검정하였다. Luxacore Self와 Luxacore Dual을 자가중합 시킨 군의 중합도는 두께에 따른 영향을 받지 않았다. Luxacore dual을 광중합한 경우 중합은 2 mm, 4 mm와 6 (적층충전) mm군에서는 밑면의 효과적인 중합이 일어났으나 8 (적층충전) mm군, 6, 8 (단일충전) mm군은 밑면에서 불완전한 중합을 보였다 (p < 0.05). 따라서 이 실험 결과에 의하면 4 mm를 초과하는 경우 단일충전보다 적층충전이 더 좋은 것으로 나타났다.