• 한국표면공학회:학술대회논문집
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• 한국표면공학회 1999년도 춘계학술발표회 초록집
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• pp.97-97
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• 1999

Dross formation in the zinc bath is inevitable under any condition as long as coating process on steel strip continues. Thus, bath aluminum and temperature are precisely managed to suppress the increase of dross. Also, excessive dross for normal coating process is generally eliminated physically by bubbling and skimming. Total amount of dross in the bath can be sometimes high enough to cause coating defect. On the other hand, local concentration of dross can make coating defect even with satisfactory level of total amount of dross. Reduction of dross in the bath was attempted by using ceramic foam filter made of mainly alumina. Dross in molten zinc was almost reduced to the levels of solubility of iron and aluminum in molten zinc at $450~460^{\circ}C$. Their solubility levels were confirmed by thermodynamic calculations or DEAL program. Two kinds of filters were tested for dross reduction. One was #20 ppi, porous per inch, and the other #30 ppi filter. Both were effective in reducing the bath dross to the solubility levels at the static state. Bath iron was reduced by 24 wt% and 19 wt% with #20 filter, and by 35 wt% and 29 wt% with #30 filter for GI and GA pot, respectively. Also, ceramic foam filter did not make any harm to the zinc bath composition after filtering test.

• 대한화학회지
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• 제67권1호
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• pp.33-41
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• 2023

Nanocrystallne WO₃ and MoO₃ with several different sizes and crystal structures were prepared by simple acid precipitation and subsequent heat treatment. The photochromic (PC) properties of these samples were comparatively investigated in powder state by monitoring diffuse reflectance spectral changes after bandgap irradiation. The PC effect of hexagonal WO₃ and monoclinic WO₃ strongly depended upon crystallite size rather than crystal structure. The smaller the crystallite size, the better the PC effect. However, orthorhombic WO·H₂O and MoO₃ having hexagonal and orthorhombic structures did not follow this trend. One consistent result for all WO₃ and MoO₃ samples is that the heat treatment in air, which changes crystallinity, whether it changes the crystal structure or only the crystallite size, reduces the PC effect. Since the thermal treatment reduces the surface oxygen defect sites, we believe that the PC effect of WO₃ and MoO₃ depends critically on the surface oxygen defect sites that serve as deep trap sites for photogenerated electrons and oxygen radical holes. We also found that the proton insertion claimed by double charge injection model is not critical for the PC effect.

• 한국건설관리학회논문집
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• 제18권5호
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• pp.59-67
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• 2017

공사 완료 시점에는 다양한 마감 공정들이 집중적으로 수행된다. 이는 현장관리자의 업무 부담을 가중시켜 경험에 근거한 임기응변적 품질관리 업무수행을 강제함으로써 감독자나 작업자의 개인역량에 따라 공사품질의 편차가 발생한다. 또한 품질관리와 관련된 정보가 시방서, 도면 등 다양한 유형의 문서에 산재하여 점검사항이 누락되는 경우가 빈번하다. 하자예방과 관련된 정보들을 체계적으로 저장하고, 상호참조 가능한 상태로 연계하여 실무자에게 점검업무 전 또는 수행 중에 효과적으로 제공할 수 있는 도구가 필요하다. 본 논문은 공동주택 마감공사의 품질점검 대상 액티비티 또는 실 단위로 필요한 정보를 체계적으로 저장 검색이 가능한 품질점검 지원 모델을 제안한다. 시방서, 설계기준, 체크리스트, 법규, 하자사례, 도면을 마감공사 프로세스 및 실과 연계하여 하자예방 정보베이스와 정보연계 넥서스를 구축하였으며 이를 바탕으로 정보등록 및 검색 인터페이스를 제시하였다. 내용적으로 다양한 하자예방 정보들을 마감공사 액티비티 및 실을 중심으로 연계하여 활용 가능한 틀을 제시함으로써 일정 수준 이상의 시공품질 확보에 기여할 수 있다.

• 한국세라믹학회지
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• 제54권4호
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• pp.323-330
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• 2017

To understand the defect chemistry of multiferroic $BiFeO_3-based$ systems, we synthesized nonstoichiometric $Bi_{1+x}FeO_{3{\pm}{\delta}}$ ceramics by conventional solid-state reaction method and studied their structural, dielectric and high-temperature charge transport properties. Incorporation of an excess amount of $Bi_2O_3$ lowered the Bi deficiency in $BiFeO_3$. Polarization versus electric field (P-E) hysteresis loop and dielectric properties were found to be improved by the $Bi_2O_3$ addition. To better understand the defect effects on the multiferroic properties, the high temperature equilibrium electrical conductivity was measured under various oxygen partial pressures ($pO_2{^{\prime}}s$). The charge transport behavior was also examined through thermopower measurement. It was found that the oxygen vacancies contribute to high ionic conduction, showing $pO_2$ independency, and the electronic carrier is electron (n-type) in air and Ar gas atmospheres.

• 한국철도학회:학술대회논문집
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• 한국철도학회 2007년도 춘계학술대회 논문집
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• pp.1656-1664
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• 2007

본 논문에서는 고속선에 사용 중인 UM71C 궤도회로의 결함진단을 위한 개선방안을 연구하였다. 고속선 궤도회로는 구간이 길어 유지보수자에 의한 점검 시 많은 시간과 노력이 소요된다. 따라서 주기적으로 검측차를 운행하고 있다. 그러나, 궤도회로 결함 시 차상검측데이터의 변화를 정확히 알 수 없으므로 실제, 고속선 운행선상의 샘플개소를 선정하여 환경에 따른 선로정수를 구하고 전송라인의 특성임피던스와 전파정수를 반영시켜 단락전류에 대한 시뮬레이션을 수행하였으며, 임의의 지점에 결함을 발생시켜 측정한 결과와 시뮬레이션 수행한 결과를 비교하였다. 이렇게 검증된 시뮬레이션 프로그램을 이용하여 보상콘덴서의 기능저하 수량 및 용량변경에 따른 차상검측데이터를 예측하였다. 이것은 보상콘덴서의 기능저하를 사전 예측하여 열차의 안전운행을 확보하기 위해 필요하다. 또한 차상검측시스템에서 얻어진 검측데이터와의 비교를 통해 유지보수에 활용 가능한 활용지침 및 분석기준을 작성하기 위해 필요하다.

• 상하수도학회지
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• 제34권4호
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• pp.251-258
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• 2020

Sewer deterioration models are needed to forecast the remaining life expectancy of sewer networks by assessing their conditions. In this study, the serious defect (or condition state 3) occurrence probability, at which sewer rehabilitation program should be implemented, was evaluated using four probability distribution functions such as normal, lognormal, exponential, and Weibull distribution. A sample of 252 km of CCTV-inspected sewer pipe data in city Z was collected in the first place. Then the effective data (284 sewer sections of 8.15 km) with reliable information were extracted and classified into 3 groups considering the sub-catchment area, sewer material, and sewer pipe size. Anderson-Darling test was conducted to select the most fitted probability distribution of sewer defect occurrence as Weibull distribution. The shape parameters (β) and scale parameters (η) of Weibull distribution were estimated from the data set of 3 classified groups, including standard errors, 95% confidence intervals, and log-likelihood values. The plot of probability density function and cumulative distribution function were obtained using the estimated parameter values, which could be used to indicate the quantitative level of risk on occurrence of CS3. It was estimated that sewer data group 1, group 2, and group 3 has CS3 occurrence probability exceeding 50% at 13th-year, 11th-year, and 16th-year after the installation, respectively. For every data groups, the time exceeding the CS3 occurrence probability of 90% was also predicted to be 27th- to 30th-year after the installation.

• 한국분말재료학회지
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• 제24권6호
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• pp.489-493
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• 2017

In this study, the surface passivation process for InP-based quantum dots (QDs) is investigated. Surface coating is performed with poly(methylmethacrylate) (PMMA) and thioglycolic acid. The quantum yield (QY) of a PMMA-coated sample slightly increases by approximately 1.3% relative to that of the as-synthesized InP/ZnS QDs. The QYs of the uncoated and PMMA-coated samples drastically decrease after 16 days because of the high defect state density of the InP-based QDs. PMMA does not have a significant effect on the defect passivation. Thioglycolic acid is investigated in this study for the effective surface passivation of InP-based QDs. Surface passivation with thioglycolic acid is more effective than that with the PMMA coating, and the QY increases from 1.7% to 11.3%. ZnS formed on the surface of the InP QDs and S in thioglycolic acid show strong bonding property. Additionally, the QY is further increased up to 21.0% by the photochemical reaction. Electron-hole pairs are formed by light irradiation and lead to strong bonding between the inorganic and thioglycolic acid sulfur. The surface of the InP core QDs, which does not emit light, is passivated by the irradiated light and emits green light after the photochemical reaction.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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• pp.81-81
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• 2008

Applications of CdS films in this study are to exhibit a high conductivity when they are exposed at light with visible wavelength and sequentially to show a low conductivity in dark state. For this purpose, CdS films should have a high photosensitivity, still maintaining a high conductivity at a visible light. In this study, CdS films were prepared at room temperature on glass substrates by rf magnetron sputtering. In order to increase the photo-conductivity in visible light, various defect levels should be located within the CdS band gap. In order to nucleate the defect sites within the CdS band gap, CdS films were deposited on glass substrates at room temperature using various $H_2$/(Ar+$H_2$) flow ratios by an rf magnetron sputtering. Through the investigation of the structural and photoconductive properties of CdS films by an addition of hydrogen, the relationship between photo- and dark-resistance in CdS films was investigated in detail. 200-nm-thick CdS films for photoconductive sensor applications were prepared at various $H_2$/(Ar+$H_2$) flow ratios on glass substrates at room temperature by rf magnetron sputtering. Sulfur concentration in CdS films crystallized at room temperature with (002) preferred orientation depends directly on the hydrogen atmosphere and the surface roughness of the films gradually increases with increasing hydrogen atmosphere. Films deposited at 8% of $H_2$/(Ar+$H_2$) exhibit an abrupt decrease of dark- and photo-resistance, showing a low photo-sensitivity ($R_{dark}/R_{photo}$). Onthe other hand, films deposited at a hydrogen atmosphere of 42% exhibit a photo-sensitivity of $5\times10^3$, maintaining a photo-resistance of an approximately $2\times10^4\Omega$/square. The dark- and photo-resistance values of CdS films were related with a composition, surface roughness, and defect sites within the band gap.

• 비파괴검사학회지
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• 제30권2호
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• pp.104-109
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• 2010

겹치기 마찰교반용접은 새로운 고상접합법이다. 알루미늄 합금 6061-T6는 좋은 내식성과 중량 대비 높은 기계적 강도로 인해 넓은 분야에서 경량부재로 사용되고 있다. 본 논문에서 사용한 검사 방법인 위상잠금 초음파 적외선열화상기법은 넓은 면적을 동시에 검사할 수 있으며, 결함부와 건전부 사이의 위상차로부터 결함의 유무를 판단할 수 있다. 본고의 연구로부터, 위상잠금 적외선열화상기술을 이용하여 용접부의 열영상을 검출하여 기계적 강도와 비교 평가하였다.

• 비파괴검사학회지
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• 제28권4호
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• pp.323-330
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• 2008

소구경 배관 소켓 용접부의 고주기 피로특성윽 평가하고 피로 균열의 발생을 음향방출법을 이용하여 실시간 모니터링 하였다. 스테인리스 316L강 시험편은 가스텅스텐아크용접 공정으로 루트부에 결함이 없는 시험편과 용입불량 결함이 있는 시험편으로 준비하였다. 피로파단은 고응력 일때는 토우부, 상대적으로 저응력일 때는 루트부에서 일어났다. 피로시험동안 음향방출 카운트가 급격히 증가하는 시점을 균열의 발생 싸이클 ($N_i$)로 정의하였고 방사선투과법과 전자현미경을 이용하여 피로균열 생성 싸이클 전과 후에서 균열을 확인하였다. 소켓용접배관의 굽힘피로 손상 진단 및 감시를 위해 균열의 존재와 파괴모드 그리고 균열의 발생 싸이클에 관한 연구를 수행하였다.