• 제목/요약/키워드: DSC analysis

검색결과 786건 처리시간 0.025초

디지털 카메라를 활용한 컬러 지상영상의 분광학적 특성 분석 (Analysis of the spectroscopic characteristics of Ground color images using a digital camera)

  • 고인철;서수영
    • 한국GIS학회:학술대회논문집
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    • 한국GIS학회 2010년도 춘계학술대회
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    • pp.137-144
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    • 2010
  • DSLR 카메라를 이용하여 획득한 지상 디지털 영상자료는 지상 사진 측량, 공간모델링에 활용할 수 있다. 지상 디지털 영상에서 각 화소의 명암도는 영상을 결정하는 가장 중요한 매개변수(parameter)이다. 따라서 좀 더 명확한 명암도의 수치 자료를 획득하고 활용하기 위하여 디지털 카메라의 분광학적 특성과 파라미터를 추정해볼 필요가 있다. 본 연구에서는 Sony DSC-F828 DSLR 카메라로 연속촬영(프레임속도 0.38초)을 통하여 얻은 7장의 같은 디지털 컬러 사진으로부터 각각 RGB 밴드의 명암도 값을 추출하여 프레임 간 화소별 명암도 차이를 확인하고, 각 컬러 밴드에 대한 각 화소의 통계학적인 분석을 통하여 분광학적인 특성의 프레임별, 화소별, 밴드별 변화와 그에 따른 상관관계에 대하여 추정해 보는 것을 목적으로 한다.

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PRAM 용 GST계 상변화 박막의 조성에 따른 특성 (Properties of GST Thin Films for PRAM with Composition)

  • 장낙원
    • Journal of Advanced Marine Engineering and Technology
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    • 제29권6호
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    • pp.707-712
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    • 2005
  • PRAM (Phase change random access memory) is one of the most promising candidates for next generation Non-volatile Memories. The Phase change materials have been researched in the field of optical data storage media. Among the phase change materials. $Ge_2Sb_2Te_5$ is very well known for its high optical contrast in the state of amorphous and crystalline. However the characteristics required in solid state memory are quite different from optical ones. In this study. the structural Properties of GeSbTe thin films with composition were investigated for PRAM. The 100-nm thick $Ge_2Sb_2Te_5$ and $Sb_2Te_3$ films were deposited on $SiO_2/Si$ substrates by RF sputtering system. In order to characterize the crystal structure and morphology of these films. x-ray diffraction (XRD). atomic force microscopy (AFM), differential scanning calorimetry (DSC) and 4-point measurement analysis were performed. XRD and DSC analysis result of GST thin films indicated that the crystallization of $Se_2Sb_2Te_5$ films start at about $180^{\circ}C$ and $Sb_2Te_3$ films Start at about $125^{\circ}C$.

FRP용 불포화폴리에스터 수지들의 연소 특성 연구 (Flammability Characteristics of Unsaturated Polyesters for FRP)

  • 최원종
    • 한국화재소방학회논문지
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    • 제12권4호
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    • pp.51-57
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    • 1998
  • FRP용 모재수지로 다량 사용되는 불포화폴리에스터 수지(이소프탈산계, 비닐에스터계)의 내열성 및 연소특성을 열분석, 연소실험 및 SEM 관찰을 통하여 알아보았다. 열분석(TGA, D DSC) 결과 이소프탈산계 폴리에스터보다 비닐에스터수지의 내열 특성이 상대적으로 우수 한 것으로 나타났다. 연소실험 결과 이소프탈산계 폴리에스터는 수지에 유통이 생기면서 쉽 게 연소되었지만, 비닐에스터의 경우 연소 시 고체탄화물을 형성시켜 상대적으로 낮은 b burning rate 값을 보였다. 본 연구 결과 불포화 폴리에스터 수지가 연소될 때 많은 연기와 화염이 발생하므로 FRP 모재수지로 사용할 때 반드시 난연처리를 해야 함을 알 수 있었다.

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건자재활용을 위한 축열용 다공성 미립자 상변환 물질 흡착 특성 (Charateristics on the PCM absorbed porous media as thermal storage applicable for construction material)

  • 이효진
    • KIEAE Journal
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    • 제17권3호
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    • pp.107-112
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    • 2017
  • Purpose: Both silica gel and activated carbon black particles were adopted for use as PCM absorbed porous media applicable as construction materials. To investigate usable methods for absorbing PCM into the media, they were soaked into PCM and also tested for enhancement of PCM absorption into them. Method: To test PCM absorption into some porous media such as both ${\varphi}1{\sim}2mm$ and $10{\mu}m$ silica gels, and $50{\mu}m$ activated carbon black, $43^{\circ}C$ PCM was used as a laten heat material. The method, soaking into PCM was applied to this study, and the media were moderately rotated by centrifuge to have the extra PCM flow out. DSC analysis was conducted to investigate the melting and solidifying of the PCM absorbed into the porous media. Result: It was found that PCM was absorbed into the porous media by over 85 wt% of all particles. In addition, it was noted that the ultrasonic vibrator was accelerating the PCM absorption into the particles to three times higher speed than simple soaking. Centrifuge was adopted to remove extra PCM sticking on the particle surfaces and extra PCM was moderately removed from the surfaces of the particles. DSC analysis indicated that the latent heat of the absorbed PCM particles was 160 J/g, and the melting temperature was approximately $40^{\circ}C{\sim}50^{\circ}C$.

면직물의 음이온화에 관한 연구 (A Study on the Anionisation of Cotton Fabric)

  • 배도규;이태정
    • 한국염색가공학회지
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    • 제30권1호
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    • pp.29-37
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    • 2018
  • Cotton has no adsorption ability for the cationic dye and heavy metal but, if anionized cotton can be made, it will be possible. In this study, to enable the anionisation of cotton fabric, it was modified using sodium vinylsolfonate(SV) as the anionisation reagent, employing a pad-dry-cure(PDC) technique. The effects of curing time, treatment concentrations of urea, sodium hydroxide and SV on the weight increase were experimented and then, the physical characterizations of sulfoethyl cotton(SEC) depending on the finishing conditions were estimated, thus the application possibility of SV as anionisation reagent was investigated. It was not much changed by anionisation except wrinkle recovery. And the structure of SEC was elucidated by Raman and NMR spectoscopy. The feasibility of using Raman and NMR spectroscopy with the band at $1,043cm^{-1}$, and 50.5ppm, respectively as marker band to determine sulfoethyl group of SEC was reported. The total degree of SV substitution(DSV) was determined via elemental analysis. SEC with diverse total DSV up to 0.066 was obtained. In the thermal decomposition(pyrolysis) by DSC, it can be found that the pyrolysis temperature was about $30^{\circ}C$ lower than that of non-treated cotton fabric.

흡음재 폐기물의 재활용 방안 (Recycling of Sound Insulation Headliner Waste Material)

  • 홍영호
    • 한국산학기술학회논문지
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    • 제14권6호
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    • pp.3089-3095
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    • 2013
  • 흡음재로 널리 사용되는 헤드라이너는 발포성 폴리우레탄(PU foam)과 유리섬유(Glass Fiber,GF) 로 구성된 복합재료로, 제품의 생산 공정을 거치는 동안 부산물 형태의 폐기물이 발생한다. 헤드라이너 폐기물에 대한 효과적인 재활용을 위해 헤드라이너 구성성분에 대한 분리공정이 중요한 문제점이다. 헤드라이너에 대한 열분석결과에 의하면 중량의 감량 비율은 $400^{\circ}C$까지의 온도범위에서는 발포성 폴리우레탄 > 비발포성 폴리우레탄 > 부직포 > 1st layer > 유리섬유의 순으로 감량이 증가하는 결과를 보이고 있다. HDPE, LLDPE, PP 그리고 Master Batch 에 첨가제 형태로 폐 스크랩 첨가하여 sheet를 제작한 후 DSC 특성을 분석한 결과 PP를 제외한 다른 물질들에서는 결정화에 따른 발열전이가 나타나지 않는 것을 확인 하였다.

올리고 부틸렌 테레프탈레이트와 6-아미노 카프론산으로부터 포리에스테르 아미드의 합성 (Preparation of Polyesteramide from Oligobutylene Terephtahlate and 6-amino Caproic Acid)

  • Cho, Soon-Chae;Choi, Doo-Jin;Kim, Seon-Ho;Rhee, Johng-Moon;Pak, Pyong-Ki;Ahn, Jong-Yeol;Kim, Young-Gil
    • 한국염색가공학회지
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    • 제3권1호
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    • pp.17-24
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    • 1991
  • Polyesteramide(PEA) has been synthesized with different molar ratio of 6-aminocaproic acid(ACA) and oligo butylene terephthalate(OBT) prepared from Dimethyl terephthalate(DMT) and 1, 4-butanediol(BD) by the melt polymerization. Oligomer and polymer molecular structure were characterized by IR spectra, H'-NMR spectra. Also the thermal properties were examined by thermogravimetric analysis(TGA) and differential scanning calorimetry(DSC). DSC and TGA results exhibited that the$ T_m$ s were detectable in the vicinity of $170-220^{\circ}C$ and the Ta's were detectable in the vicinity of $380-390^{\circ}C$ . X-ray diffraction analysis results show that the synthesized polyesteramide has high degree of crystallinity.

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급냉응고된 $Ti_{50}Ni_{20}Cu_{30}$ 합금 스트립의 형상기억특성과 기계적특성 (Shape Memory Characteristics and Mechanical Properties of Rapidly Solidified $Ti_{50}Ni_{20}Cu_{30}$ Alloy Strips)

  • 김연욱
    • 한국주조공학회지
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    • 제29권5호
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    • pp.187-191
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    • 2009
  • Microstructures and shape memory characteristics of $Ti_{50}Ni_{20}Cu_{30}$ alloy strips fabricated by arc melt overflow have been investigated by means of XRD, optical microscopy and DSC. The microstructure of as-cast strips exhibited columnar grains normal to the strip surface. X-ray diffraction analysis showed that one-step martensitic transformation of B2-B19 occurred in the alloy strips. According to the DSC analysis, it was known that the martensitic transformation temperature ($M_s$) of B2 $\rightarrow$ B19 in $Ti_{50}Ni_{20}Cu_{30}$ strip is $57^{\circ}C$. During thermal cyclic deformation with the applied stress of 60 MPa, transformation hysteresis and elongation associated with the B2-B19 transformation were observed to be $3.7^{\circ}C$ and 1.6%, respectively. The as-cast strip of $Ti_{50}Ni_{20}Cu_{30}$ alloy also showed a superelasticity and its stress hysteresis was as small as 14 MPa. These mechanical properties and shape memory characteristics of the alloy strips were ascribed to B2-B19 transformation and the controlled microstructures produced by rapid solidification of the arc melt overflow process.

Dilauroyl Peroxide의 PP에 대한 기계적, 열적 성질 변화 (Influence of Dilauroyl Peroxide on Mechanical and Thermal Properties of Different Polypropylene Matrices)

  • Sirin, Kamil;Yavuz, Mesut;Canli, Murat
    • 폴리머
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    • 제39권2호
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    • pp.200-209
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    • 2015
  • In this study, the influence of dilauroyl peroxide on mechanical and thermal properties of different polypropylene (PP) matrices was investigated. Polypropylene matrices, different molecular weight isotactic PP containing 0.01, 0.02, 0.04, 0.06, 0.08, and 0.1 wt% of dilauroyl peroxide (DLP) were prepared by using a single-screw extruder. The effect of the visbreaking agent (DLP) on mechanical, physical, thermal and morphological properties of different molecular weight PP had been studied. Mechanical properties (tensile strength at break point, at yield and elongation at break point), melt flow index (MFI), scanning electron microscope (SEM) and differential scanning calorimetric (DSC) analyses of these matrices were examined. Melting ($T_m$) and crystallization ($T_c$) temperatures, crystallinity ratio (%) and enthalpies were determined. The microstructure of isotactic polypropylene matrix was investigated by scanning electron microscopy (SEM). From SEM analysis, it was observed that the surface disorder increased by the increasing amount of DLP. As a result of DSC analyses, the crystallinity ratio of the PP matrices has varied between 1.64-7.27%. Mechanical properties of the matrices have been improved. Particularly, the mechanical tests of PP have given interesting results when compounded with 0.06-0.08 wt% dilauroyl peroxide (DLP). Mechanical properties and thermal decomposition processes were all changed by increasing the amount of DLP in the matrix structure.

친환경 저비중 자기보강 복합소재 개발을 위한 공정 변수별 영향도 평가 (Study of Mechanism for Improving Tensile Elastic Modulus of Self-reinforced Composite)

  • 윤덕우;강현민
    • Composites Research
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    • 제28권4호
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    • pp.197-203
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    • 2015
  • 폴리프로필렌 기반 자기보강 복합재는 기지재와 보강재가 동일한 소재로 구성되어 기존 섬유강화 복합재와 달리 섬유와 기지재의 분리없이 바로 재활용이 가능할 뿐 아니라 폴리프로필렌 수준까지 저 비중화가 가능한 고분자 복합재이다. 본 연구에서는 더블벨트 라미네이터 공정기술을 이용하여 압력, 온도, 냉각조건과 같은 공정 변수가 폴리프로필렌으로 제조된 자기보강 복합재의 인장 물성에 미치는 영향을 연구하였다. XRD, DSC를 이용하여 결정구조의 변화에 따라 인장 탄성계수는 0.2~1.2 GPa로 약 6배까지 향상되는 것을 확인하였다. SEM 분석을 통해 함침 정도를 확인함으로써 자기보강 복합재의 함침 후 형상 변화 또한 고찰하였다.