• Title/Summary/Keyword: DCB test

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Mechanical Behaviors of CFRP Laminate Composites Reinforced with Aluminum Oxide Powder

  • Kwon, Oh-Heon;Yun, Yu-Seong;Ryu, Yeong-Rok
    • Journal of Power System Engineering
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    • v.18 no.6
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    • pp.166-173
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    • 2014
  • In this study, a laminated composite material with dispersing aluminum oxide powder between the CFRP laminate plies, and also CFRP composites without aluminium oxide powder were fabricated for Mode I experiments using the DCB specimen and a tensile test. The behavior of the crack and the change of the interfacial fracture toughness were evaluated. Also in order to evaluate the damage mechanism for the crack extension, the AE sensor on the surface of the DCB test specimen was attached. AE amplitude was estimated for CFRP-alumina and CFRP composite. And the fracture toughness was evaluated by the stress intensity factor and energy release rate. The results showed that an unstable crack was propagated rapidly in CFRP composite specimen along with the interface, but crack propagation in CFRP-alumina specimen was relatively stable. From results, we show that aluminium oxide powder spreaded uniformly in the interface of the CFRP laminate carried out the role for preventing the sudden crack growth.

H2 Plasma Pre-treatment for Low Temperature Cu-Cu Bonding (수소 플라즈마 처리를 이용한 구리-구리 저온 본딩)

  • Choi, Donghoon;Han, Seungeun;Chu, Hyeok-Jin;Kim, Injoo;Kim, Sungdong
    • Journal of the Microelectronics and Packaging Society
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    • v.28 no.4
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    • pp.109-114
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    • 2021
  • We investigated the effects of atmospheric hydrogen plasma treatment on Cu-Cu direct bonding. Hydrogen plasma was effective in reducing the surface oxide layer of Cu thin film, which was confirmed by GIXRD analysis. It was observed that larger plasma input power and longer treatment time were effective in terms of reduction and surface roughness. The interfacial adhesion energy was measured by DCB test and it was observed to decrease as the bonding temperature decreased, resulting in bonding failure at bonding temperature of 200℃. In case of wet treatment, strong Cu-Cu bonding was observed above bonding temperature of 250℃.

Processing and Mode 1 Fracture Toughness of Carbon Fiber Composites Reinforced With Carbon Nanotubes (탄소나노튜브로 보강된 탄소섬유복합재의 제조 공정과 모드 1 파괴인성)

  • Kim, Han-Sang
    • Composites Research
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    • v.24 no.5
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    • pp.39-43
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    • 2011
  • For the last twenty years, nanocomposites composed of polymer matrices reinforced with carbon nanotubes (CNTs) have been an active research area. Also, the polymeric nanocomposites reinforced with CNTs are being investigated to be used matrices of carbon fiber composites. Carbon tiber composites have achieved advanced properties in the direction of carbon fibers due to enhanced carbon fiber properties. However, the matrix dominated properties need to be improved further to fully utilize the advanced carbon fiber properties. In particular, delamination is a typical and critical reason for fracture of carbon fiber composites. Mode I fracture toughness test which is also often called double cantilever beam (DCB) test shows the resistance to delamination of carbon fiber composites and this test is performed on carbon fiber composite samples incorporated with carbon nanotubes functionalized with various functional groups. The specimens with mat-like CNT layers showed the increased fracture toughness by 10.6%.

Disposal of Highly Toxic Wastes by using High Temperature and High Pressure Combustor (난분해성 환경오염물질의 고온.고압연소)

  • Yoon, Jae-Kun;Hong, Ho-Yeun;Lee, Jeong-Woo;Kim, Jong-Pyo;Kang, Su-Sok
    • 한국연소학회:학술대회논문집
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    • 2006.04a
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    • pp.75-78
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    • 2006
  • Disposal of highly toxic wastes like polychlorinated biphenyls (PCBs) is very difficult. These substances create a growing mountain of problematic waste that has to be disposed properly. Conventional technologies that are based on common burning(rotary kiln, ${\sim}1100^{\circ}C$) and plasma technology(${\sim}10000^{\circ}C$) do not satisfy important conditions. for example, complete combustion of the toxic waste and the price of waste disposal. The combustor like a rocket engine is operated at relatively high pressure(${\sim}15$ bar) and relatively high temperature(>$3000^{\circ}C$) that are ideal for the complete destruction of extremely toxic substances. In this study, test compound($_o-DCB$) was dissolved in kerosine with a concentration of 10%. Pure gas oxygen was used as an oxidant. Analysis showed that the destruction efficiency achieved for ${o}-DCB$ was 99.9999% or better. The results show that a combustor based on liquid propllant rocket technology is a validated tool for the disposal of highly toxic waste, and a good alternative technology when applied to the destruction of extremely toxic wastes.

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Effects of Ar/N2 Two-step Plasma Treatment on the Quantitative Interfacial Adhesion Energy of Low-Temperature Cu-Cu Bonding Interface (Ar/N2 2단계 플라즈마 처리에 따른 저온 Cu-Cu 직접 접합부의 정량적 계면접착에너지 평가 및 분석)

  • Choi, Seonghun;Kim, Gahui;Seo, Hankyeol;Kim, Sarah Eunkyung;Park, Young-Bae
    • Journal of the Microelectronics and Packaging Society
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    • v.28 no.2
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    • pp.29-37
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    • 2021
  • The effect of Ar/N2 two-step plasma treatment on the quantitative interfacial adhesion energy of low temperature Cu-Cu bonding interface were systematically investigated. X-ray photoelectron spectroscopy analysis showed that Ar/N2 2-step plasma treatment has less copper oxide due to the formation of an effective Cu4N passivation layer. Quantitative measurements of interfacial adhesion energy of Cu-Cu bonding interface with Ar/N2 2-step plasma treatment were performed using a double cantilever beam (DCB) and 4-point bending (4-PB) test, where the measured values were 1.63±0.24 J/m2 and 2.33±0.67 J/m2, respectively. This can be explained by the increased interfacial adhesion energy according phase angle due to the effect of the higher interface roughness of 4-PB test than that of DCB test.

Propagation of Crack in Concrete Subjected to Dynamic Loading (동적하중(動的荷重)을 받는 콘크리트의 구열(龜裂)성장)

  • Kang, Sung Hoo;Kim, Woo
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.8 no.2
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    • pp.135-145
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    • 1988
  • This study deals with the prediction of crack propagation in concrete mortar subjected to static and dynamic load. Total 54 CLWL-DCB(Crack-line-loaded-double-cantilever beam) concrete mortar specimens were tested to measure crack growth using ASTM 561-80. Main variables were sand to cement ratio and water to cement ratio. The resulting load(P)-COD(Crack Opening Displacement; $2V_1$) curves and COD-CTOD (Crack Tip Opening Displacement; $2V_2$) curves were analyzed to calculate effective crack length and physical crack length by way of ASTM 561-80 proposed. Replica crack length were also obtained directly during the test. The differences in crack propagation between under static load and under dynamic load were investigated.

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Deactivation and Regeneration of a Used De-NOx SCR Catalyst for Wastes Incinerator (소각로 SCR 폐탈질 촉매의 피독과 효율재생에 관한 연구)

  • Lee, Sang-Jin;Hong, Sung-Chang
    • Applied Chemistry for Engineering
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    • v.19 no.3
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    • pp.259-263
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    • 2008
  • The catalytic activity of the used catalyst, $V_2O_5/TiO_2$, for MSW incinerators was investigated focusing on its regeneration. As the result of the experimental analysis, the NOx removal efficiency difference between the fresh catalyst and used catalyst is about 60% at $260^{\circ}C$ and 1, 2-dichlorobenzen (1, 2-DCB) removal efficiency difference is about 14% at $200^{\circ}C$, in honeycomb test. And the catalysts, both the fresh and used, were characterized by XRD, TGA, and ICP techniques in order to investigate the deactivation. On the basis of the results, it is found that the used catalyst is deactivated by ammonium-sulfates, heavy metals (Pb, As etc.), alkali metals (Ca), and phase transfer of $TiO_2$. Also calcination treatment under nitrogen and air condition was excellent than washing and calcination treatment.

Numerical Study on Inverse Analysis Based on Levenberg-Marquardt Method to Predict Mode-I Adhesive Behavior of Fiber Metal Laminate (섬유금속적층판의 모드 I 접합 거동 예측을 위한 Levenberg-Marquardt 기법 기반의 역해석 기법에 관한 수치적 연구)

  • Park, Eu-Tteum;Lee, Youngheon;Kim, Jeong;Kang, Beom-Soo;Song, Woojin
    • Composites Research
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    • v.31 no.5
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    • pp.177-185
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    • 2018
  • Fiber metal laminate (FML) is a type of hybrid composites which consist of metallic and fiber-reinforced plastic sheets. As the FML has a drawback of the delamination that is a failure of the interfacial adhesive layer, the nominal stresses and the energy release rates should be determined to identify the delamination behavior. However, it is difficult to derive the nominal stresses and the energy release rates since the operating temperature of the equipment is restricted. For this reason, the objective of this paper is to predict the mode-I nominal stress and the mode-I energy release rate of the adhesive layer using the inverse analysis based on the Levenberg-Marquardt method. First, the mode-I nominal stress was assumed as the tensile strength of the adhesive layer, and the mode-I energy release rate was obtained from the double cantilever beam test. Next, the finite element method was applied to predict the mode-I delamination behavior. Finally, the mode-I nominal stress and the mode-I energy release rate were predicted by the inverse analysis. In addition, the convergence of the parameters was validated by trying to input two cases of the initial parameters. Consequently, it is noted that the inverse analysis can predict the mode-I delamination behavior, and the two input parameters were converged to similar values.

Adhesion Reliability Enhancement of Silicon/Epoxy/Polyimide Interfaces for Flexible Electronics

  • Kim, Sanwi;Kim, Taek-Soo
    • Journal of the Microelectronics and Packaging Society
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    • v.19 no.3
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    • pp.63-69
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    • 2012
  • Adhesion and mechanical reliability of silicon/epoxy/polyimide interfaces are critical issues for flexible electronics. Bonds between these interfaces are mainly hydrogen bonds, so their adhesion is weaker than cohesive fracture toughness and vulnerable to moisture. In order to enhance adhesion and suppress moisture-assisted debonding, UV/Ozone treatment and innovative sol-gel derived hybrid layers were applied to silicon/epoxy/polyimide interfaces. The fracture energy and subcritical crack growth rate were measured by using a double cantilever beam (DCB) fracture mechanics test. Results showed that UV/Ozone treatment increased the adhesion, but was not effective for improving reliability against humidity. However, by applying sol-gel derived hybrid layers, adhesion increase as well as suppresion of moisture-assisted cracking were achieved.

DETECTION OF INTERFACIAL CRACK LENGTH BY USING ULTRASONIC ATTENUATION COEFFICIENTS ON ADHESIVELY BONDED JOINTS

  • Chung, N.Y.;Park, S.I.
    • International Journal of Automotive Technology
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    • v.5 no.4
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    • pp.303-309
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    • 2004
  • In this paper, an interfacial crack length has been detected by using the ultrasonic attenuation coefficient on the adhesively bonded double-cantilever beam (DCB) joints. The correlations between energy release rates which were investigated by experimental measurement, the boundary element method (BEM) and Ripling's equation are compared with each other. The experimental results show that the interfacial crack length for the ultrasonic attenuation coefficient and energy release rate increases proportionally. From the experimental results, we propose a method to detect the interfacial crack length by using the ultrasonic attenuation coefficient and discuss it.