• 대한치과보철학회지
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• 제42권2호
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• pp.167-174
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• 2004

Statement of problem: Removable partial denture and complete denture often require denture base relines to improve the fit against the tissue-bearing mucosa because of gradual changes in edentulous ridge contours and resorption of underlying bone structure. Purpose: This study was performed to investigate the effect of surface design on bond strength of relining denture base resins to denture base acrylic resin. Materials and method: Heat curing resin(Lucitone 199, Dentsply U.S.A. and Vertex, Dentimex, Holland), self curing resin(Tokuso rebase, Tokuyama, Japan), and visible light curing resin(Triad, Dentsply, U.S.A.) were used in this study. The surface designs were classified as butt, bevel and rabbet joint and the bond strengths were measured by Universial Testing Machine (Zwick 2020, Zwick Co., Germany). Results and Conclusion: The obtained results from this study were as follows ; 1. The bond strength of Vertex resin was higher than those of Tokuso rebase and Triad. 2. The bond strength of rabbet and bevel joint was higher than that of butt joint. 3. The failure mode of Triad and Tokuso rebase was mainly adhesive, but cohesive failure was shown mainly in vertex.

• 폴리머
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• 제24권2호
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• pp.220-227
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• 2000

충전물의 함량비 및 배합방법을 달리하여 실리카/카본블랙 충전 천연고무 가황물을 제조하였다. 충전물의 함량은 고무에 대해 70 phr이 되도록 하였으며, 이들을 동시에 배합하여 제조한 가황물과 실리카를 먼저 배합하고 일정 시간 경과 후 카본블랙을 배합하여 제조한 가황물의 가황특성, 모폴로지, 그리고 인열특성 및 크랙성장속도 등의 파열특성을 비교하였다. 가공시, 단계배합물은 동시배합물보다 경화 속도($t_{90}$ )는 약간 느렸으나, 긴 유도시간($t_2$), 낮은 최대 토오크 값($T_{max}$ )을 보였다. 단계 배합물은 인열특성 및 크랙성장 특성에 있어서도 상대적으로 우수함을 보였으며, 실리카의 함량이 30 phr인 경우에 가공성 및 파열 특성이 가장 우수하였다.

• Geomechanics and Engineering
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• 제29권1호
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• pp.13-23
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• 2022

Peat soil has the characteristics of high moisture content, large void ratio and low shear strength. In this study, unconfined compressive strength and SEM tests are conducted to investigate the effects of ultrahigh moisture content, cement content, organic content and pH value on the strength of solidified peat. As an increase in the cement content and curing period, the failure mode of solidified peat soil changes from ductile failure to brittle failure. The influence of moisture content on the strength of solidified peat is greater than the cement content. As cement content increases from 10% to 30%, strength of solidified peat at a curing age of 28 days increases by 161%~485%. By increasing water content by 100%, decreases of solidified peat at a curing age of 28 days is 42%~79%. Compared with the strength of solidified peat with a pH value of 5.5, the strength of peat with a pH value of 3.5 reduces by 10% ~ 46%, while the strength of peat with a pH value of 7.0 increases by 8% ~ 38%. It is recommended to use filler materials for stabilizing peat soil with moisture content greater than 200%. Because of small size of clay particles, clay added in the cement solidified peat can improve much higher strength that that of sand.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1995년도 하계학술대회 논문집 C
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• pp.1171-1173
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• 1995

Polyimide thin films were fabricated through the vapor deposition polymerization method, and the structure and capacitance characteristics of them were investigated in detail. It was found that the chemical structure and uniformity of the film could be stabilized with curing. The peaks of $720cm^{-l},\;1380cm^{-1}\;and\;1780cm^{-1}$ show C=O stretch mode, C-N stretch mode and carbonyl stretch mode, and those of polyimide which cured over $300^{\circ}C$ were fixed. It was found that capacitance was changed in proportion to temperature.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2000년도 추계학술발표대회 논문집
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• pp.84-87
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• 2000

Square tubes used for vehicle structure components have an important role on keeping its stiffness and preserving occupant safety in vehicle collision and rollover in which it experience axial collapse, bending collapse or both. Bending collapse, which absorbs kinetic energy of the impact and retains a survival space for the occupant, is a dominant failure mode in oblique collision and rollover. Thus, in this paper, the bending collapse characteristics such as the maximum bending moment and energy absorption capacity of the square tube replaced by light-weight material were evaluated and presented. The bending test of cantilever tubes which were fabricated with aluminum, GFRP and aluminum/ GFRP hybrid by co-curing process was performed. Then the maximum bending moment and the energy absorption capacity from the moment-angle curve were evaluated. Based on the test results, it was found that aluminum/ GFRP hybrid tube can show better specific energy absorption capacity compared to the pure aluminum or GFRP tube and can convert unstable collapse mode which may occur in pure GFRP tube to stable collapse mode like a aluminum tube in which plastic hinge is developed.

• Restorative Dentistry and Endodontics
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• 제32권1호
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• pp.28-36
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• 2007

본 연구는 광중합형 복합레진 중합 시 기존의 중합법과 가변광도 중합형인 soft start 중합법 및 exponential 중합법 간의 중합수축효과를 비교하고자 하였다. 본 연구를 위해 3종의 복합레진 (Synergy Duo Shade, Z250, Filtek Supreme) 및 3종의 광조사기 (Spectrum 800, Elipar Highlight, Elipar Trilight)를 사용하였다. 총 중합시간은 40초로 일정하게 유지하였으며, 선형 중합수축률의 측정은 linometer를 이용하였으며, 90초간의 선형 수축률을 0.5초 간격으로 측정하였다. 재료별로 각 중합 방법별 시간에 따른 중합수축률을 one-way ANOVA test로 분석하여 최종 중합수축률에 도달하는 시간을 산출하였고, 90초 후 최종 선형 중합수축률을 two-way ANOVA test를 이용하여 재료, 광조사 방법, 재료 및 광조사 방법의 교호작용이 중합수축에 미치는 영향이 있는지를 검증하였다. 또한 90초까지의 선형 중합수축률에 대한 20초까지의 선형 중합수축률의 비를 two-way ANOVA로 비교하고, 각각의 통계치를 95% Scheffe test로 검증하였는바, 다음과 같은 결과를 얻었다 1. Supreme을 제외한 다른 군에서는 재료 및 광조사 방법에 관계없이 대부분의 중합 수축이 광조사 후 20초 이내에 이루어졌다 (p < 0.05). 2. 90초 후, 최종 중합수축률은 재료 (p = 0.000)와 광조사 방법 (p = 0.003) 모두 유의성 있는 영향을 끼쳤으나, 재료와 광조사 방법 상호간의 작용은 영향이 없었다. 3. 90초 후 최종 중합수축률은 총 광에너지가 가장 낮은 exponential 중합법에서 유의성 있게 낮았다 (p < 0.05). 4. 20초까지의 초기 수축률은 soft start와 exponential중합법 등 가변광도 중합이 conventional 중합법에 비하여 유의성 있게 낮은 수축률을 보였다 (p < 0.05). 본 실험 결과만을 토대로 볼 때, 가변광도 중합법은 초기 중합수축 속도를 감소시켜 수축응력을 감소시킨다고 볼 수 있다. 그러나 총 조사 광에너지의 차이로 인해 그 물리적 성질에 영향이 있을 수 있으므로 향후 이에 대한 더 많은 고찰이 필요할 것으로 사료된다.

• 한국재료학회지
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• 제14권5호
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• pp.322-327
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• 2004

Copper-based leadframe sheets were oxidized in two kinds of hot alkaline solutions to form brown-oxide or black-oxide layer on the surface. The oxide coated leadframe sheets were molded with epoxy molding compound (EMC). After post mold curing, the oxide-coated EMC-leadframe joints were machined to form sandwiched Brazil-nut (SBN) specimens. The SBN specimens were used to measure the fracture toughness of the EMC/leadframe interfaces under mixed-mode (mode I + mode II) loading conditions. Fracture surfaces were analyzed by various equipment to investigate failure path. The results revealed that the failure paths were strongly dependent on the oxide type. In case of brown oxide, hackle-type failure was observed and failure path lay near the EMC/CuO interface with a little inclining to CuO at all case. On the other hand, in case of black oxide, quite different failure path was observed with respect to the distance from the tip of pre-crack and phase angle. Different failures occurred with oxide type is presumed to be due to the difference in microstructure of the oxides.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1993년도 하계학술대회 논문집 B
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• pp.1162-1164
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• 1993

The Thermally Stimulated Current(TSC) spectroscopy has been applied to study the influence of the structual cahange and interface on the electrical properties of epoxy composites. Three DGEBA-MeTHPA matrix model samples mixed different ratios and silica($SiO_2$) filled sample and silaln treating-filled sample has been studied. Above room temperature, the relaxation mode $\alpha$ peak associated with Tg has been located at $110^{\circ}C$. Below glass transition temperature(Tg), three relaxation modes are observed in all samples: a $\beta$ mode situated at $10^{\circ}C$, a $\gamma$ mode located at $-40^{\circ}C$ and a $\delta$ mode appeared in $-120^{\circ}C$. The analysis of its fine structure indicates that constitution of elementary processes is characterized by the activation energy and relaxation time. Also the dielectric relaxation properties have been investigated to compare the the change of the molecular structure and motion to the relaxation properties and conduction mechanism in TSC spectra.

• 대한소아치과학회지
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• 제28권3호
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• pp.471-479
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• 2001

복합레진의 광중합시간 단축과 관련하여 최근에 개발된 고강도 할로겐광 중합기를 기존의 중강도 할로겐광 중합기와 비교 평가하기 위하여, 세 종류의 광중합용 복합레진을 두께가 2, 3, 4, 5mm인 스테인레스 스틸 몰드에 충전하고, 레진 상면을 중강도 할로겐광은 (1) $400mW/cm^2$으로 40초간 고강도 할로겐광은 (2) 10초동안 $100mW/cm^2$부터 $1000mW/cm^2$까지 출력량이 증가하면서 중합하고 다음 10초동안 $1000mW/cm^2$로 중합하는 ramp 모드로 20초간, (3) $1000mW/cm^2$의 boost 모드로 10초간, (4) $850mW/cm^2$의 표준 모드로 20초간 조사하고, 상면과 하면의 표면경도를 미세경도측정기로 측정한 후 실험군간의 차이를 분석하였다. 레진 상면의 경도는 중합광의 강도와 중합시간 및 레진 두께에 따른 차이가 없었다(유의수준 0.05, 이하 동일). 레진 하면의 경도는, 두께 2mm의 중강도군(1)을 제외하고, 상면의 경도보다 낮았다. 레진 하면의 경도는 두께 2mm에서 중강도군(1)이 ramp군(2) 및 boost군(3)보다 높았고 중강도군(1)과 표준군(4) 간 및 ramp군(2)과 boost 군(3) 간에 차이가 없었으며, 두께 3mm에서 중강도군(1)이 가장 높았고 표준군(4)이 boost군(3)보다 높았다. 따라서, 복합레진의 중합 깊이 측면에서 볼 때, $1000mW/cm^2$의 고강도 할로겐광을 10초간 조사한 것은 $400mW/cm^2$의 중강도 할로겐 광을 40초간 조사한 것에 미치지 못하였으며, 레진 두께 2mm이내인 경우에는 $850mW/cm^2$의 고강도 할로겐광을 20초간 조사함으로써 $400mW/cm^2$의 중강도 할로겐광을 40초간 조사한 것과 대등한 중합을 일으킬 수 있었다.

• 한국재료학회지
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• 제15권1호
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• pp.1-5
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• 2005

Copper-based leadframe sheets were immersed in two kinds of hot alkaline solutions to form brown-oxide or black-oxide layer on the surface. The oxide-coated leadframe sheets were molded with epoxy molding compound (EMC). After post mold curing, the oxide-coated EMC-leadframe joints were machined to form sandwiched double-cantilever beam (SDCB) specimens. The SDCB specimens were used to measure the fracture toughness of the EMC/leadframe interfaces under quasi-Mode I loading conditions. Fracture surfaces were analyzed by various equipment to investigate failure path. The present paper deals with the failure path, and the cause of the failure path formation with an adhesion model will be treated in the succeeding paper.