• 한국연초학회지
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• 제25권1호
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• pp.39-46
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• 2003

The essential oils from Burley 21 tobacco was isolated by using the SDE (Simultaneous Distillation & Extraction) apparatus coupled with gas chromatography and mass spectrometry analysis. Burley 21 tobaccos were divided and collected by six stages at intervals of five days during air-curing process. Air curing was conducted with horizontal hanging method in greenhouse settled by shading materials. 55 components were identified by comparisons of retention indices and mass spectral data, including 22 hydrocarbons, 6 alcohols, 3 aldehydes, 9 ketones and 15 miscellaneous compounds. Neophytadiene was the major components of the oils and almost all hydrocarbons were gradually decreased during air-curing process. Most of alcohols were also diminished, on the contrary, 1-pentanol and benzyl alcohol among them were increased. Aldehydes and ketones were increased during air-curing and especially, the concentrations of solanone, $\beta$-damascone, $\beta$-damascenone and megastigmatrienones were much increased. Indole level of miscellaneous compounds were continuously increased during air-curing of Burley 21 tobacco.

• The Journal of Advanced Prosthodontics
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• 제7권4호
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• pp.317-322
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• 2015

PURPOSE. The aim was to evaluate the effect of curing mode and different dentin surface pretreatment on microtensile bond strength (${\mu}TBS$) of self-adhesive resin cements. MATERIALS AND METHODS. Thirty-six extracted human permanent molars were sectioned horizontally exposing flat dentin surface. The teeth were divided into 12 groups (3 teeth/group) according to the dentin surface pretreatment methods (control, 18% EDTA, 10% Polyacrylic acid) and curing mode (self-curing vs. light-curing) of cement. After pretreatment, composite resin blocks were cemented with the following: (a) G-CEM LinkAce; (b) RelyX U200, followed by either self-curing or light-curing. After storage, the teeth were sectioned and ${\mu}TBS$ test was performed using a microtensile testing machine. The data was statistically analyzed using one-way ANOVA, Student T-test and Scheffe's post-hoc test at P<.05 level. RESULTS. For G-CEM LinkAce cement groups, polyacrylic acid pretreatment showed the highest ${\mu}TBS$ in the self-cured group. In the light-cured group, no significant improvements were observed according to the dentin surface pretreatment. There were no significant differences between curing modes. Both dentin surface pretreatment methods helped to increase the ${\mu}TBS$ of RelyX U200 resin cement significantly and degree of pretreatment effect was similar. No significant differences were found regarding curing modes except control groups. In the comparisons of two self-adhesive resin cements, all groups within the same pretreatment and curing mode were significantly different excluding self-cured control groups. CONCLUSION. Selecting RelyX U200 used in this study and application of dentin surface pretreatment with EDTA and polyacrylic acid might be recommended to enhance the bond strength of cement to dentin.

• Design & Manufacturing
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• 제16권3호
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• pp.9-15
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• 2022

In order to reduce the manufacturing costs of the glass lens, it is necessary to manufacture a lens using a UV curable resin or a thermosetting resin, which is a curable material, in order to replace a glass lens. In the case of forming a lens using a thermosetting material, it is necessary to form several lenses at once using the wafer-level lens manufacturing technologies due to the long curing time of the material. When a lens is manufactured using a curable material, an error in the shape of the lens due to the shrinkage of the material during the curing process is an important cause of defects. The major factors for these shape errors and deformations are the shrinkage and the change of mechanical properties in the process of changing from a liquid material during curing to a solid state after complete curing. Therefore, it is necessary to understand the curing process of the material and to examine the shrinkage rate and change of physical properties according to the degree cure. In addition, it is necessary to proceed with CAE for lens molding using these and to review problems in lens manufacturing in advance. In this study, the viscoelastic properties of the material were measured during the curing process using a rheometer. Using the results, Rheological investigation of cure kinetics was performed. At the same time, The shrinkage of the material was measured and simple mathematical models were created. And using the results, the molding process of a single lens was analyzed using Comsol, a commercial S/W. In addition, the experiment was conducted to compare and verify the CAE results. As a result, it was confirmed that the shrinkage rate of the material had a great influence on the shape precision of the final product.

• 콘크리트학회지
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• 제11권2호
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• pp.85-94
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• 1999

플라이애쉬 대체량에 따른 변화, 양생방법이 미치는 영향 그리고 조기강도를 높이기 위해 첨가된 화학 혼화제가 시멘트-플라이애쉬 페이스트의 특징 및 콘크리트 강도에 미치는 영향을 알아보았다. 시멘트-플라이애쉬 페이스트의 압축강도는 시멘트로만 만들어진 페이스트보다 낮았으며, 플라이애쉬의 대체량이 증가할수록 강도차이가 증가하였다. 그러나 증기양생시 시멘트-플라이애쉬 페이스트는 수중양생시보다 압축강도가 증가하였으며, 특히 조기강도가 크게 향상되었다. 조기강도 증진을 목적으로 혼입한 활성화제($Na_2SO_4$)의 첨가는 시멘트-플라이애쉬 페이스트 조기강도를 증진시켰으며, 또한 $Na_2SO_4$와 플라이애쉬를 30% 함유한 플라이애쉬 콘크리트의 강도도 월등히 향상되었다.

• The Journal of Advanced Prosthodontics
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• 제3권3호
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• pp.136-139
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• 2011

PURPOSE. A new light curing urethane dimethacrylate and a cold curing resin with simpler and faster laboratory procedures may have even improved flexural properties. This study investigated the 3-point flexural strengths and flexural moduli of two alternate base materials. MATERIALS AND METHODS. A cold curing resin (Weropress) and a light curing urethane dimethacrylate base material (Eclipse). Along with Eclipse and Weropress, a high impact resin (Lucitone199) and three conventional base materials (QC 20, Meliodent and Paladent 20) were tested. A 3-point bending test was used to determine the flexural strengths and flexural moduli. The mean displacement, maximum load, flexural modulus and flexural strength values and standard deviations for each group were analyzed by means of one-way analysis of variance (ANOVA) (with mean difference significant at the 0.05 level). Post hoc analyses (Scheffe test) were carried out to determine the differences between the groups at a confidence level of 95%. RESULTS. Flexural strength, displacement and force maximum load values of Eclipse were significantly different from other base materials. Displacement values of QC 20 were significantly different from Lucitone 199 and Weropress. CONCLUSION. The flexural properties and simpler processing technique of Eclipse system presents an advantageous alternative to conventional base resins and Weropress offers another simple laboratory technique.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2019년도 추계 학술논문 발표대회
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• pp.141-142
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• 2019

In this study, we conducted a comparative analysis of the effects of retention time and resuscitation method on the degree of resuscitation after reapplying mortar with much FA replacement. Results After applying NaOH to the top surface of 60 % FA-substituted mortar, the degree of resuscitation at $40^{\circ}C$ was high enough to increase the overall curing time, but there was no significant difference. However, with regard to the curing method, middle curing showed the greatest manifestation, followed by wrapping and underwater curing, but there was no significant difference. The resuscitation level on the 28th of the lumber was found to be revived to about 70~80 % at around 30 % without resuscitation.

• 한국축산식품학회지
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• 제23권1호
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• pp.32-38
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• 2003

식염농도 7%의 염지액을 이용하여 돼지고기 등심을 염지할 때에 염지온도와 기간이 염지육의 이화학적 특성과 기호성에 미치는 영향을 검토하였다. 열지온도 1$0^{\circ}C$에서 15일째에 염지육의 pH와 보수력이 현저히 저하되었다. 염지온도 1$0^{\circ}C$에서 염지액과 염지육 표면부위의 일반세균수는 12째에 현저히 많아졌으나 중심부위는 거의 검출되지 않았다. 임시 온도가 높을수록 염지기간에 관계없이 식염 침투가 빠르고 염지육 식염함량이 많아졌으며, 표면부위에 대한 중심분위의 식염함량 비율은 염지기간이 길수록 크게 나타났다. 염지육의 식염함량은 가열에 의하여 적어졌다. 염지 가열육의 짠맛과 풍미는 염지 초기에는 높은 온도에서, 후기에는 낮은 온도에서 우수하였다. 열지 가열육은 1$^{\circ}C$에서 12일, 5$^{\circ}C$에서 9일 염지하여 제조하면 기호성이 우수하였다.

• 한국연초학회지
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• 제22권2호
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• pp.133-137
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• 2000

The bulk curing experiment to improve the quality of flue-cured leaves were carried out to evaluate relationship between the modified(3 step-up) drying and conventional drying method in bulk curing process. Modified drying method was somewhat higher values in yellowing color index of cured leaves, and less brittle than those in conventional drying program. As to the chemical properties, there was no difference in chemical component levels in cured leaves between the modified and the conventional methods, while the major chemical compounds in relation to aromatic essential oil of cured leaves showed mostly higher level in the modified method than that in conventional drying method. Additionally 3 step-up drying method increased the tobacco quality by 2 % in price per kg compared with conventional drying method.

• Restorative Dentistry and Endodontics
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• 제47권4호
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• pp.45.1-45.10
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• 2022

Objectives: This study evaluated the relationship between the battery charge level and irradiance of light-emitting diode (LED) light-curing units (LCUs) and how these variables influence the Vickers hardness number (VHN) of a bulk-fill resin. Materials and Methods: Four LCUs were evaluated: Radii Plus (SDI), Radii-cal (SDI), Elipar Deep Cure (Filtek Bulk Fill, 3M Oral Care), and Poly Wireless (Kavo Kerr). Irradiance was measured using a radiometer every ten 20-second activations until the battery was discharged. Disks (4 mm thick) of a bulk-fill resin (Filtek Bulk Fill, 3M Oral Care) were prepared, and the VHN was determined on the top and bottom surfaces when light-cured with the LCUs with battery levels at 100%, 50% and 10%. Data were analyzed by 2-way analysis of variance, the Tukey's test, and Pearson correlations (α = 5%). Results: Elipar Deep Cure and Poly Wireless showed significant differences between the irradiance when the battery was fully charged versus discharged (10% battery level). Significant differences in irradiance were detected among all LCUs, within each battery condition tested. Hardness ratios below 80% were obtained for Radii-cal (10% battery level) and for Poly Wireless (50% and 10% battery levels). The battery level showed moderate and strong, but non-significant, positive correlations with the VHN and irradiance. Conclusions: Although the irradiance was different among LCUs, it decreased in half of the devices along with a reduction in battery level. In addition, the composite resin effectiveness of curing, measured by the hardness ratio, was reduced when the LCUs' battery was discharged.

• Journal of the Korean Wood Science and Technology
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• 제40권2호
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• pp.110-122
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• 2012

This study investigated the effects of layered clay on the thermal curing behavior and tensile properties of resole phenol-formaldehyde (PF) resin/clay/cellulose nanocomposites. The thermal curing behavior of the nanocomposite was characterized using conventional differential scanning calorimetry (DSC) and temperature modulated (TMDSC). The addition of clay was found to accelerate resin curing, as measured by peak temperature ($T_p$) and heat of reaction (${\Delta}H$) of the nanocomposite’ curing reaction increasing clay addition decreased $T_p$ with a minimum at 3~5% clay. However, the reversing heat flow and heat capacity showed that the clay addition up to 3% delayed the vitrification process of the resole PF resin in the nanocomposite, indicating an inhibition effect of the clay on curing in the later stages of the reaction. Three different methods were employed to determineactivation energies for the curing reaction of the nanocomposite. Both the Ozawa and Kissinger methods showed the lowest activation energy (E) at 3% clay content. Using the isoconversional method, the activation energy ($E_{\alpha}$) as a function of the degree of conversion was measured and showed that as the degree of cure increased, the $E_{\alpha}$ showed a gradual decrease, and gave the lowest value at 3% nanoclay. The addition of clay improved the tensile strengths of the nanocomposites, although a slight decrease in the elongation at break was observed as the clay content increased. These results demonstrated that the addition of clay to resole PF resins accelerate the curing behavior of the nanocomposites with an optimum level of 3% clay based on the balance between the cure kinetics and tensile properties.