• Title/Summary/Keyword: Cu matching method

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The Study on Analytical Method of Lead, Cadmium and Chromium in Copper Metal by Matrix Matching Method of Inductively Coupled Plasma Atomic Emission Spectrometer (유도결합 플라즈마 발광분광기의 매트릭스 보정법에 의한 구리 중납, 카드뮴 및 크롬 분석에 관한 연구)

  • Joo, Sung-Kyun;Kim, Joon;cheong, Nam-Yong;Lim, Kyu-Chual;Choi, Young-Hwan;Kim, Sang-Kyung
    • Journal of the Korean Chemical Society
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    • v.53 no.3
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    • pp.293-301
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    • 2009
  • Analytical results of a fixed concentration of Pb, Cd and Cr in the synthetic copper standard solution (RMs) for using the matrix no matched standard calibration curve at various wavelength by ICP showed that accuracy (140 $\sim$ 1,070% in case of Pb) is very poor at all wavelengths because of the Cu matrix effect. Analytical results of a fixed concentration of Pb, Cd and Cr in the different concentration solutions of Cu showed that found values were on the increase or decrease as the rate of a regular equation as the concentration of Cu was increased. Accuracies by the Cu matching method in the analysis of Pb, Cd and Cr in the synthetic copper standard solution (RMs) were higher than 99.9%.

Simple Algorithm of Structure Features Extration for Stereo Image Matching (스테레오 영상 정합을 위한 새로운 구조 정보 추출 알고리즘)

  • 최환언
    • Journal of the Korean Graphic Arts Communication Society
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    • v.9 no.1
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    • pp.1-11
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    • 1991
  • In this reseach, double-layered photoconductor consist of the carrier generation layer(CGL) of $\varepsilon$ type copper phthalocyanine thin film by an aqueous coating method and the carrier transport layer(CGL) of polyvinyl carbazol(PVK) by spin coating. We inverstigated effect of the surfactant solution and cathod electrolysis to the crystal type of $\varepsilon$-CuPc in CGL with TEM, SEM and X- ray diffraction spectroscopy and studied the mechanism of an aqueous coating for the preparation of CGL. The effect of the washing of CGL about the electrophotographic characteristics of the $\varepsilon$-CuPc/PVK doublelayered photoconductors is studied also.

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A Study on the Change of Dyeability and Colorfastness of Lotus Leaf Extract with Mordanting Treatment (매염처리에 따른 연(蓮)잎 추출물의 염색성 및 염색견뢰도 변화에 관한 연구)

  • Park Young-Deuk
    • Journal of the Korean Home Economics Association
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    • v.42 no.12 s.202
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    • pp.69-76
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    • 2004
  • The purpose of this study was to investigate the colorfastness of cotton and silk fabric dyed with extract of Lotus leaf princeps. The experimental items were classified into mordanting treatments, fabric components and kind of mordants. The experimental test was done by laundering, abrasion(dry/wet), perspiration(acid/alkali) , light fastness, color difference by C.C.M(computer color matching) system and K/S test. The summarized findings resulting from the experiment and investigation are as follows: In the C.C.M and K/S test on mordanting method and kind of fabrics, co-mordanting treatment method and protein fabric (silk) were the most effective. Especially, Fe mordanting treatment was higher than Al, Cu, Cr and none-mordanting. In colorfastness on the mordants, perspiration and laundering fastness showed high grade (4-5) but grades of perspiration(2-3/4) and light fastness(1-3) were low.

The Development of Enzymatic Mordanting Using Laccase for Phenolic Natural Dye (라카아제 촉매 활성에 의한 홍차 염색물의 매염효과)

  • Lee, Hye Bin;Song, Ji Eun;Shim, Eui Jin;Kim, Hye Rim
    • Fashion & Textile Research Journal
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    • v.20 no.3
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    • pp.323-330
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    • 2018
  • This study aim is to provide new coloration method by laccase-catalyzation on natural phenolic dyeing process. In this study, silk was dyed with black tea, which is one of polyphenolic dye, extracted in distilled water. The dyed samples were catalyzed by laccase as the eco-friendly mordanting process. To optimize the conditions of laccase-catalyzed coloration, conditions were varied by different mordanting methods (one-bath, two-bath), temperature and treatment time. The dye affinity in terms of the value of K/S, $L^*$, $a^*$, $b^*$, and H, V, C was measured by Computer Color Matching System (CCM, CM-2600d, Spectra Magic NX, Korea). The effect of laccase-catalyzed coloration on washing fastness was evaluated and compared with the synthetic mordant (Al, Cu, and Fe). As the result of color analysis of dyed silk, the optimum conditions of laccase-catalyzed coloration were determined to post-mordanting by one-bath at $50^{\circ}C$ for 3 hours. Under the optimum laccase-catalyzed conditions, the dyed silk was shown the color of yellowish-red. After laccase-catalyzed coloration on the dyed silk, the improvement of washing fastness was obtained compared with mordanted silk by synthetic mordant (Al, Cu, and Fe). Therefore, the present study was demonstrated that the effective enzymatic mordanting method by laccase for phenolic natural dyeing with vivid color and good fastness.

Gallnut dyeing of Crabyon Fiber Contained Cotton Towels (크라비욘 원사가 함유된 면타올의 오배자 염색)

  • Woo, Ji-Hae;Lee, Shin-Hee
    • Fashion & Textile Research Journal
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    • v.17 no.6
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    • pp.1030-1038
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    • 2015
  • The purpose of this study is to investigate the dyeability of crabyon fiber contained cotton towels after dyeing with gallut. In this study, the colorants of gallnut were extracted with boiling water at 60℃ and 60min. Crabyon, composite fiber of Chitin/Chitosan and cellulose, is manufactured by uniformly blending Chitin/Chitosan and cellulose viscose and extruding the blended viscose into spin-bath. Cotton towels with crabyon fiber dyed with extracted solution from gallnut according to concentration, temperature and time. Crabyon fiber contained cotton towels dyed using gallnut were pre of post-mordanted using Al, Cu, and Fe. The dyeability(K/S) and color characteristics(L*, a*, b*, C, and h(color angle)) of dyed crabyon fiber contained cotton towels were measured by computer color matching machine and photographs. The crabyon fiber composition of cotton towels was conformed by amide peak(-CONH-) of chitin or chitosan of FT-IR spectroscopy. The results obtained were as follows; The amide peak of crabyon fiber contained cotton towels appeared at about 1652 cm−1. The dyeability of crabyon fiber contained cotton towel was increased gradually with increasing concentration of gallnut dyeing solution and saturated at about 150%(o.w.f). The optimum dyeing temperature and dyeing time were 90~100℃ and 80minutes expectively. The crabyon fiber contained cotton towels were dyed reddish yellow by non, Al, and Cu mordanting, reddish blue by Fe mordanting, respectively. The fastness to washing according to concentration of gallnut in and mordanting method indicated good grade result as more than 3~4 degree in all conditions.

Pigment Analysis and Conservation Method of Avalokitesvara in Potalaka of Hyeondeungsa, Gapyeong (가평 현등사 수월관음도의 안료분석 및 보존방법)

  • Seo, Jeong-Ho;Cha, Byung-Gap;Jung, Hee-Soo
    • Journal of Conservation Science
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    • v.27 no.2
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    • pp.223-229
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    • 2011
  • Buddha painting cultural properties couldn't avoid the change of colors and the exfoliation phenomenon by the characteristic of material and environmental factors. Especially, because in the beginning of the fine crack and the decoloration phenomenon on the surface of pigment would be significantly decrease stability of the whole object, it is necessary to take particular measure. Therefore, this is a study on conservation of Avalokitesvara in Potalaka in Hyeondeungsa in Gapyeong. It treated damaged parts of the object, carried out backing papers and matching colors. And then, it examined scientific analysis of pigments. Also, it performed nondestructive testing like XRF, FT-IR, and image microscope to investigate the quality of the material of hanji using the object and the component and characteristic of pigments. As a result, FT-IR spectrum matching Korean traditional paper(hanji) was detected in hanji of Avalokitesvara in Potalaka in Hyeondeungsa. The black pigment making a thin layer over the white pigment would estimate carbon compounds of unconfirmed ink stick or soot as XRF and FT-IR. Also, the white pigment was lead white($PbCO_3{\cdot}Pb(OH)_2$) involving Pb(Lead) and a carbonate. It was observed that the crystal of blue pigment had the different sizes of the particles from the microscope. In the case of this blue pigment, it showed cobalt blue and lead white was mixed when it used because both Cu and Pb were highly detected in XRF data.

Evaluation of Fracture Toughness of Copper Thin Films by Combining Numerical Analyses and Experimental Tests (해석과 실험을 결합한 구리 박막의 파괴인성 평가)

  • Kim, Hyun-Gyu;Oh, Se-Young;Kim, Kwang-Soo;Lee, Haeng-Soo;Kim, Seong-Woong;Kim, Jae-Hyun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.37 no.2
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    • pp.233-239
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    • 2013
  • In this paper, a method of combining numerical analyses and experimental tests is used to evaluate fracture toughness of copper thin films of $15{\mu}m$ thickness. Far-field loadings of a global-local finite element model are inversely estimated by matching crack opening profiles in experiments with numerical results. The fracture toughness is then evaluated using the J-integral for cracks in thin films under far-field loadings. In experiments, Cu thin films attached to Aluminum sheets are loaded indirectly, and crack opening profiles are observed by microscope camera. Stress versus strain curves of Cu thin films are obtained through micro-tensile tests, and the grain size of Cu thin films is observed by TEM analysis. The results show that the fracture toughness of Cu thin films with $500nm{\sim}1{\mu}m$ sized grains is $6,962J/m^2$.

Jangdo(Small Ornamental Knives) manufacturing process and restoration research using Odong Inlay application (오동상감(烏銅象嵌)기법을 활용한 장도(粧刀)의 제작기술 및 복원연구)

  • Yun, Yong Hyun;Cho, Nam Chul;Jeong, Yeong Sang;Jang, Chu Nam
    • Korean Journal of Heritage: History & Science
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    • v.49 no.2
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    • pp.172-189
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    • 2016
  • In this research, literature research on the Odong material, mixture ratio, casting method and casting facility was conducted on contemporary documents, such as Cheongong Geamul. Also, a long sword was produced using the Odong inlay technique. The sword reproduction steps were as follows; Odong alloying, silver soldering alloying, Odong plate and Silver plate production, hilt and sheath production, metal frame and decorative elements, such as a Dugup (metal frame), production, Odong inlay assembly and final assembly. For the Odong alloy production, the mixture ratio of the true Odong, which has copper and gold ratio of 20:1, was used. This is traditional ratio for high quality product according to $17^{th}$ century metallurgy instruction manual. The silver soldering alloy was produced with silver and brass(Cu 7 : Zn 3) ratio of 5:1 for inlay purpose and 5:2 ratio for simple welding purpose. The true Odong alloy laminated with silver plate was used to produce hilt and sheath. The alloy went through annealing and forging steps to make it into 0.6 mm thick plate and its backing layer, which is a silver plate, had the matching thickness. After the two plates were adhered, the laminated plate went through annealing, forging, engraving, silver inlaying, shaping, silver welding, finishing and polishing steps. During the Odong colouring process, its red surface turns black by induced corrosion and different hues can be achieved depending on its quality. To accomplish the silver inlay Odong techniques, a Hanji saturated with thirty day old urine is wrapped around a hilt and sheath material, then it is left at warm room temperature for two to three hours. The Odong's surface will turn black when silver inlay remains unchanged. Various scientific analysis were conducted to study composition of recreated Odong panel, silver soldering, silver plate and the colouring agent on Odong's surface. The recreated Odong had average out at Cu 95.57 wt% Au 4.16wt% and Cu 98.04 wt% Au 1.95wt%, when documented ratio in the old record is Cu 95wt% and Au 5wt%. The recreated Odong was prone to surface breakage during manufacturing process unlike material made with composition ratio written in the old record. On the silver plate of the silver and Odong laminate, 100wt% Ag was detected and between the two layers Cu, Ag and Au were detected. This proves that the adhesion between the two layers was successfully achieved. The silver soldering had varied composition of Ag depending on the location. This shows uneven composition of the silver welding. A large quantities of S, that was not initially present, was detected on the surface of the black Odong. This indicates that presence of S has influence on Odong colour. Additional study on the chromaticity, additional chemical compounds and its restoration are needed for the further understanding of the origin of Odong colour. The result of Odong alloy testing and recreation, Odong silver inlay long sword production, scientific analysis of the Odong black colouring agent will form an important foundation of knowledge for conservation of Odong artifact.

Wavelet Transform-based Face Detection for Real-time Applications (실시간 응용을 위한 웨이블릿 변환 기반의 얼굴 검출)

  • 송해진;고병철;변혜란
    • Journal of KIISE:Software and Applications
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    • v.30 no.9
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    • pp.829-842
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    • 2003
  • In this Paper, we propose the new face detection and tracking method based on template matching for real-time applications such as, teleconference, telecommunication, front stage of surveillance system using face recognition, and video-phone applications. Since the main purpose of paper is to track a face regardless of various environments, we use template-based face tracking method. To generate robust face templates, we apply wavelet transform to the average face image and extract three types of wavelet template from transformed low-resolution average face. However template matching is generally sensitive to the change of illumination conditions, we apply Min-max normalization with histogram equalization according to the variation of intensity. Tracking method is also applied to reduce the computation time and predict precise face candidate region. Finally, facial components are also detected and from the relative distance of two eyes, we estimate the size of facial ellipse.