• Title/Summary/Keyword: Crystal Orientation

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Synthesis and characterization of layered basic zine p-toluenesulfonates (층상구조의 염기성 zinc p-toluenesulfonate의 합성 및 성질에 관한 연구)

  • 김형동;조영식;허영덕
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.4
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    • pp.651-654
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    • 1998
  • The layered basic zinc p-toluenesulfonates has been directly synthesized by the surface modification. The chemical formula of layered basic zinc p-toluenesulfonate is determined by CHNS and TG-DTA. From the X-ray diffraction data and the guest size, the orientation of the p-toluenesulfonate onto the zinc hydroxide layer is determined. The molecular plane of the p-toluenesulfonate lies perpendicular to the zinc hydroxide layers.

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The structure and synthesis of intercalation compound between a layered double hydroxide and an organic compound (유기화합물이 삽입된 층상이중수산화물의 합성과 구조)

  • 우은경;허영덕
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.8 no.1
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    • pp.36-41
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    • 1998
  • Intercalation compounds of alkyl sulfonates into layered double hydroxides (LDH) have been directly synthesized. From the X-ray diffraction data and the alkyl sulfonates size, the orientation of the intercalated alkyl sulfonate into the layered double hydroxide was determined. The intercalated alkyl sulfonate is arranged with molecular chain perpendicular to the hydroxide layer with an antiparallel pattern.

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Effects of seeding layers on electrical properties of PLZT thin films prepared by sol-gel method (Seeding층이 sol-gel법에 의한 PLZT 박막의 제조시 전기적 특성에 미치는 영향)

  • 이진홍;박병욱
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.10 no.2
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    • pp.140-144
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    • 2000
  • ($Pb_{0.91}$$La_{0.09}$)($Zr_{0.65}$$Ti_{0.35}$)$O_3$ thin films were prepared on ITO-coated glass by spin-coating. As $Pb_{0.9}$$La_{0.1}$)$TiO_3$ thin films were used as seeding layers, formation temperature of perovskite was reduced and theUrosette" structure was disappeared. PLZT thin films with a seeding layer of 40 nm thick showed a (100) preferred orientation and better dielectric and ferroelectric properties.ties.

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The structure of intercalation compound between a layered double hydroxide and an ethyl orange (층상이중수산화물과 에틸오렌지의 삽입화합물의 구조)

  • Jung, Woo-Chan;Huh, Young-Duk
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.7 no.1
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    • pp.137-142
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    • 1997
  • We synthesized the intercalation compound between a layered double hydroxide and an ethyl orange. The orientation of the intercalated ethyl orange into the layered double hydroxide was investigated. The molecular plane of the ethyl orange and its N=N axis lie nearly perpendicular to the hydroxide layers with an antiparallel pattern.

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The Surface Recrystallization Behavior of Single Crystal CMSX-2 (단결정 CMSX-2의 표면재결정 거동)

  • Jo, Chang-Yong;Na, Yeong-Sang;Kim, Hak-Min;Kim, Woo-Yeol;Bae, Cha-Hurn;Lee, Sang-Lae
    • 연구논문집
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    • s.23
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    • pp.15-27
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    • 1993
  • The single crystal specimens were solidified by modified Bridgeman method. The surface recrystallized single crystal specimens were prepared by shot peening followed by heat treatment. The surface recrystallization begins at the dendrite cores on the surface. The recrystallized grains grew into the inner side of the specimen. The growth of recrystallized grains was inhibited by the pores and eutectic phases. The primary $\gamma'$ phases were dissolved at the recrystallized grain boundaries during the grain growth. The grain growth of recrystallized grains was similar to the cellular type transformation. No orientation relationships were found bewteen the recrystallized grains and the parent phase.

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The Effect of Cold Forging on Carburizing Microstructure

  • Yanjun Huo;Baixuan Liu;Qingpo Xi;Hua Liu
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10b
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    • pp.40-42
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    • 2003
  • The aim of this paper is to illustrate which factors influence the martensite grain fineness made by subsequently surface carburizing of extruded component. The effects of surface decarburizing by annealing, residual stress, initial microstructure and crystal oriental made by forward extrusion were taken into account. The available evidence suggests that the residual stress inside crystal or the crystal orientation is the main factor that results coarse martensite while cold extruded component was treated by carburizing.

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Texture in hot-pressed silicon carbide (고온가압소결한 탄화규소의 집합조직)

  • 김영욱;김원중
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.4
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    • pp.343-350
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    • 1995
  • A Abstract Systematic studies of the effects of crystalline forms of starting powders and p processing variables on the texture of hot - pressed silicon carbide are described. The results I indicate that hot - pressing of $\beta$ - SiC can produce strong textures and composite type duplex microstructure due to the ${\beta} {\rightarrow} {\alpha}$ phase transformation of SiC. The texture variations d during post - annealing have been observed. In the case of using a - SiC as starting pow¬d ders, the degree of preferred orientation by hot - pressing is relatively weak.

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Micro-Contact Printing Method for Patterning Liquid Crystal Alignment Layers

  • Jung, Jong-Wook;Kim, Hak-Rim;Lee, You-Jin;Kim, Jae-Hoon
    • Journal of Information Display
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    • v.7 no.2
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    • pp.12-15
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    • 2006
  • We propose a patterning method of liquid crystal (LC) alignment layer for producing multi-domain LC structures. By controlling thermal conditions during micro-contact printing procedures and facilitating wetting properties of patterning materials, patterned LC orientation can be easily obtained on a bare ITO surface or other polymer films. The newly proposed patterning method is expected to be a very useful tool for fabricating multi-domain LC structures to enhance or design electro-optic properties of LC-based devices.

Composition Control and Annealing Effects on the Growth of YBaCuO Superconducting Thin Films by RF Magnetron Sputtering (RF Magnetron Sputtering 방법에 의한 고온 초전도 박막 제조를 위한 조성 조절 및 열처리 효과)

  • 한택상;김영환;염상섭;최상삼;박순자
    • Journal of the Korean Ceramic Society
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    • v.27 no.2
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    • pp.249-255
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    • 1990
  • High Tc Supperconducting thin films were fabricated by rf magnetron sputtering method. We have successfully controlled the compositions of films by adding sintered CuO pellets on YBa2Cu3O7-x single target. High Tc thin films with large grian size and good crystal habit were obtained by rapid thermal annealing process. The films deposited on SrTiO3(100) single crystal substrate indicated the existence of c-axis prefered orientation confirmed by XRD and SEM analysis. The Tc, zero's of sharp resistive transition for rapid annealed films deposited on polycrystalline YSZ substrate and on SrTiO3(100) single crystal substrate were 79K and 88K, respectively.

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Effects of UV Irradation on the Alignment of Liquid Crystal (러빙배향된 액정셀에 대한 자외선 조사효과)

  • Kim, Young-Sik;Kim, Jae-Hyung
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.11b
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    • pp.324-327
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    • 2001
  • Liquid crystal alignments on a rubbed polyimide layer were investigated by using optical transmission method. Using this technique, we also studied the pretilt angle of the polymer molecules near the surface of a side-chain polymer layer as a function of the rubbing strength. In particular, we obtained the optical characteristics of liquid crystal orientations and pretilt angles for LC cell photo-aligned by UV as well after rubbing alignment. High pretilt angle of 3.84 degree was obtained on the weekly rubbed polymide layer duribg UV irradation time of 60min.

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