• Nuclear Engineering and Technology
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• v.53 no.8
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• pp.2629-2639
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• 2021

Within the frame of the EMPIrE test, four monolithic mini-plates were irradiated in the ATR reactor. In two of them, the monolithic U(Mo) foil had been PVD-coated with Zr before the plate manufacturing. Extensive microstructural characterizations were performed on a fresh archive mini-plate, using Optical Microscopy (OM), Scanning Electron Microscopy (SEM) combined with Energy Dispersive Spectroscopy (EDS), Electron Backscattered Diffraction (EBSD) and Focused Ion Beam (FIB)/Transmission Electron Microscopy (TEM) with nano EDS. A particular attention was paid to the examination of the U(Mo) foil, the PVD coating, the cladding/Zr and Zr/U(Mo) interfaces. The Zr coating has a thickness around 15 ㎛. It has a columnar microstructure and appears dense. The cohesion of the cladding/Zr and Zr/U(Mo) interfaces seems to be satisfactory. An almost continuous layer with a thickness of the order of 100-300 nm is present at the cladding/Zr interface and corresponds to an oxidized part of the Zr coating. At the Zr/U(Mo) interface, a thin discontinuous layer is observed. It could correspond to locally oxidized U(Mo). This work provides a basis for interpreting the results of characterizations on EMPIrE irradiated plates.

• Composites Research
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• v.33 no.6
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• pp.415-420
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• 2020

The interfacial properties in carbon fiber composites, which control the overall mechanical properties of the composites, are very important. Effective interface enhancement work is conducted on the modification of the carbon fiber surface with carbon nanotubes (CNTs). Nonetheless, most surface modifications methods do have their own drawbacks such as high temperatures with a range of 600~1000℃, which should be implemented for CNT growth on carbon fibers that can cause carbon fiber damages affecting deterioration of composites properties. This study includes the use of in-situ interfacial polymerization of polyamide 610/CNT to fabricate the carbon fiber composites. The process is very fast and continuous and can disperse CNTs with random orientation in the interface resulting in enhanced interfacial properties. Scanning electron microscopy was conducted to investigate the CNT dispersion and composites morphology, and the thermal stability of the composites was analyzed via thermogravimetric analysis. In addition, fiber pull-out tests were used to assess interfacial strength between fiber and matrix.

• Journal of Industrial and Engineering Chemistry
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• v.67
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• pp.301-311
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• 2018

In this study, the ion-gelation method was applied to fabricate novel Fe-carbon-bentonite-alginate beads ($Fe^0$/C-BABs). $Fe^0$/C-BABs could effectively control Fe release during persulfate (PS) activation in N-acetyl-p-aminophenol (APAP) oxidation. A novel two-stage approach that combined $Fe^0$/C-BABs and an oyster-shell-filled bed (OSFB) column was developed to address the low pH and high Fe concentration of the effluent of the traditional PS process. The application of the $Fe^0$/C-BABs and OSFB column regulated pH levels and Fe release during the advanced oxidation of APAP. The characteristics of $Fe^0$/C-BABs were also investigated through scanning electron microscopy, energy dispersive spectrometry, and Fourier transform infrared spectroscopy. The long-term operation performance of $Fe^0$/C-BABs in a continuous fixed-bed reactor under simultaneous PS and APAP feeding was also evaluated. The effects of initial PS concentration, pH, fixed-bed weight, in-flow rate, and dissolved oxygen (DO) were investigated. Under selected conditions, 86.3% efficiency was achieved during the first stage of APAP degradation (effluent pH of 3.05, Fe contents: $106.25mgL^{-1}$). Water quality improved after the effluent was passed through the OSFB column (effluent pH of 6.32, Fe contents: $21.43mgL^{-1}$). Moreover, this study analyzed the free radicals and intermediates produced during APAP degradation to identify the possible routes of APAP degradation.

• Korean Journal of Metals and Materials
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• v.46 no.6
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• pp.338-344
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• 2008

The crystallization kinetics of the $Cu_{43}Zr_{43}Al_7Be_7$ bulk metallic glass were studied by differential scanning calorimetry(DSC) in the continuous heating and isothermal annealing modes. Only one major peak could be detected on the DSC traces of $Cu_{43}Zr_{43}Al_7Be_7$ bulk amorphous alloy, and the activation energy for crystallization corresponding to the peak determined by the Kissinger method was resulted of 239 kJ/mol. The isothermal kinetic, analyzed by the Johnson-Mehl-Avrami equation yielded values for the Avrami exponents in the range 1.69 to 2.37, which implied a crystallization governed by a three-dimensioned growth. Primary phases were essentially the cubic structure CuZr together with the $Cu_{10}Zr_7$ phase. At higher temperature, the CuZr disappeared while the $Cu_{10}Zr_7$ became predominant. After long term annealing at 731 K, the phases were $Cu_{10}Zr_7$, $Cu_2ZrAl$ and $Al_3Zr_5$.

• Korean Journal of Metals and Materials
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• v.48 no.5
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• pp.377-386
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• 2010

An investigation was conducted into the effects of $\kappa$-carbides on the cracking phenomenon, which often occurred in cold-rolled light-weight steel plates. Three kinds of steels were fabricated by varying the C content, and their microstructures and tensile properties were investigated. In the two steels that contained a high carbon content, the band structures of ferrites and $\kappa$-carbides that were severely elongated along the rolling direction were well developed, whereas continuous arrays of $\kappa$-carbides were formed in the steel that contained a low carbon content. Detailed microstructural analyses of the deformed region beneath the tensile fracture surface showed that the cracks initiated at arrays of $\kappa$-carbides or $\kappa$-carbides formed interfaces between the band structures, which initiated cleavage fractures in the ferrite bands, while the bands populated with a number of $\kappa$-carbides did not play an important role in propagating the cracks. Thus, the minimization of interfacial $\kappa$-carbides or $\kappa$-carbide arrays by increasing the carbon content was essential for preventing cracking from occurring during cold rolling.

• Fashion & Textile Research Journal
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• v.24 no.1
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• pp.138-145
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• 2022

Today, graphene loaded textiles are being considered promising smart clothing due to their high conductivity. In this study, we reported reduced graphene oxide(r-GO) deposited pure cotton fabrics fabricated with a colloidal solution of graphene(GO), using a one-step aerosol spray pyrolysis(ASP) process and their potential application on smart textiles. The ASP process is advantageous in that it is easily implementable and can be applied for continuous processing. Moreover, this process has never been applied to deposit r-GO on pure cotton fabric. The field emission-scanning microscopy (FE-SEM) observation, Fourier transform-infrared(FT-IR) analysis, Raman spectroscopy, X-ray diffraction(XRD) analysis, and ultraviolet transmittance(UVT) were used to evaluate material properties of the r-GO colloids. The resistance was also measured to evaluate the electrical conductivity of the specimens. The results revealed that the r-GO was successfully deposed on specimens, and the specimen with the highest electrical conductivity demonstrated an electrical resistance value of 2.27 kΩ/sq. Taken together, the results revealed that the ASP method demonstrated a high potential for effective deposition of r-GO on cotton fabric specimens and is a prospect for the development of conductive cotton-based smart clothing. Therefore, this study is also meaningful in that the ASP process can be newly applied by depositing r-GO on the pure cotton fabric.

• Journal of Digital Policy
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• v.1 no.2
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• pp.17-24
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• 2022

In China, the continuous promotion and coverage of scanning code payment has caused an imbalance in the coin market. Coin changers can not only alleviate this problem, but also affect the business development of commercial banks. Therefore, it is meaningful to study the coin changer. The purpose of this paper is to study the impact of coin changers on the business of commercial banks in China. Through on-the-spot visits and based on the manually collected customer data of Chinese commercial banks as the object, combined with the calculation method of financial indicators to conduct case analysis. The results of the study show that the coin changer has a positive impact on the business development of Chinese commercial banks. This paper provides feasible suggestions and new ideas for business development to Chinese commercial banks. At present, there are few related studies on coin exchange machines. This study combines the calculation of financial indicators to verify the policy results, which is the innovation of this study.

• Journal of the Korean Society of Industry Convergence
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• v.25 no.6_2
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• pp.1119-1125
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• 2022

The depletion of resources and waste disposal caused by the continuous development of industry have emphasized the need to reduce consumption and production, recycle and reuse, and the importance of remanufacturing has increased in recent years. The spindle part of the aging planner miller, which is currently being remanufactured, is one of the factors that has the greatest impact on the performance of the machine tool. When designing the spindle part of the spindle shaft, there are considerations such as the configuration size bearing performance of the main shaft, but the diameter of the main shaft, the dangerous speed bearing, and the arrangement that affect the machining accuracy should be basically considered. As such, various studies have been conducted on the design of machine tool spindle spindles, but research on the reverse engineering of existing aging machine tool spindle spindles is poor. Reverse engineering is designing in the direction of improving performance by extracting specifications from already finished products, and first scanning the reverse engineered object through a 3D scanner, 3D modeling is performed based on the collected data, and then the process of deriving improvement plans by reverberating to improve performance by identifying wear and damage conditions is followed. Therefore, in this study, the purpose of this study is to provide data on reverse engineering by deriving improvement plans through optimal design for the bearing position of the aging planar Miller spindle spindle using central composite programming.

• Journal of radiological science and technology
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• v.46 no.1
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• pp.29-36
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• 2023

To have highly reliable diagnostic performance of it, this study comparatively analyzed spatial resolution of SPECT images and interrelationship depending on the changes of system uniformity of ga㎜a camera through phantom analysis. This study chose 6 kinds of results from quality control (uniformity) of triple head SPECT scanner operated in an university hospital in Seoul for six months. Then, study measured spatial resolutions (FWHM) of the images restructured by injecting radiopharmaceuticals to Jaszczak phantom, and doing SPECT scanning under the same conditions as clinical ones using the analytical program (image J). Quality controls performed by the experimental institution showed that differential uniformity of UFOV ranged from 2.76% to 7.61% (4.46±2.07), and integral uniformity of UFOV ranged from 1.98% to 5.42% (3.01±1.43). Meanwhile, Quantitative analysis evaluations of phantom images depending on the changes of uniformity of SPECT scanner detector showed that as the uniformity values of UFOV and CFOV decreased, FWHM values of phantom images decreased from 8.5 ㎜ to 5.8 ㎜. That is, it was quantitatively identified that the higher uniformity of detector is, the better spatial resolution of images gets (P<0.05). It is very important to perform continuous and consistent quality control of the nuclear medicinal system, and users should be clearly conscious of it.

• Restorative Dentistry and Endodontics
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• v.47 no.4
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• pp.36.1-36.17
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• 2022

Objectives: This study aimed to evaluate the effect of aging on the marginal quality of glass hybrid (GH) material used to elevate dentin gingival margins, and to analyze the consistency of the results obtained by 3 in vitro methods. Materials and Methods: Ten teeth received compound class II cavities with subgingival margins. The dentin gingival margins were elevated with GH, followed by resin composite. The GH/gingival dentin interfaces were examined through digital microscopy, scanning electron microscopy (SEM) using resin replicas, and according to the World Dental Federation (FDI) criteria. After initial evaluations, all teeth were subjected to 10,000 thermal cycles, followed by repeating the same marginal evaluations and energy dispersive spectroscopy (EDS) analysis for the interfacial zone of 2 specimens. Marginal quality was expressed as the percentage of continuous margin at ×200 for microscopic techniques and as the frequency of each score for FDI ranking. Data were analyzed using the paired sample t-test, Wilcoxon signed-rank test, and Pearson and Spearmen correlation coefficients. Results: None of the testing techniques proved the significance of the aging factor. Moderate and strong significant correlations were found between the testing techniques. The EDS results suggested the presence of an ion-exchange layer along the GH/gingival dentin interface of aged specimens. Conclusions: The marginal quality of the GH/dentin gingival interface defied aging by thermocycling. The replica SEM and FDI ranking results had stronger correlations with each other than either showed with the digital microscopy results.