• 제목/요약/키워드: Consolidated Sample

검색결과 51건 처리시간 0.029초

Preparation of W-V functionally gradient material by spark plasma sintering

  • Tang, Yi;Qiu, Wenbin;Chen, Longqing;Yang, Xiaoliang;Song, Yangyipeng;Tang, Jun
    • Nuclear Engineering and Technology
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    • 제52권8호
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    • pp.1706-1713
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    • 2020
  • Functionally gradient material (FGM) is promisingly effective in mitigating the thermal stress between plasma facing materials (PFM) and structural materials. However, the corresponding research with respect to W/V FGM has not been reported yet. In this work, we firstly report the successful fabrication of W/V FGM by a combined technology of mechanical alloying (MA) and spark plasma sintering (SPS). The microhardness and microstructure of the consolidated sample were both investigated. W/V stacks show significantly enhanced microhardness (>100%) compared with pure W plate, which is beneficial to the integral strength of the hybrid structure. Furthermore, we clarify that the different ductility of W and V should be carefully considered, otherwise W/V powder might aggregate and lead to the formation of compositional segregation, and simultaneously unmask the impact of V proportion on the distribution of second phase in W-V binary alloy system. This work provides an innovative approach for obtaining W-V connections with much better performance.

토목섬유로 보강된 슬래그 재료의 전단강도 및 변형 특성 (Strength and Deformation Characteristics of Geosynthetics-Reinforced Slag Materials)

  • 신동훈;이종석
    • 한국지반신소재학회논문집
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    • 제8권4호
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    • pp.27-34
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    • 2009
  • 본 연구에서는 토목섬유가 층상으로 보강된 슬래그 재료의 전단강도와 변형특성을 다루었다. PET mat와 같은 토목섬유에 의한 보강이 슬래그의 전단강도와 변형특성에 미치는 영향을 조사 및 분석하기 위해 압밀배수 조건 하에서의 대형삼축압축시험을 수행하였다. 연구에 사용된 슬래그 재료는 현장에서 사용되는 재료와 동일한 재료로서 scale effect로 인한 문제점은 없었다. 토목섬유로 보강된 슬래그의 응력-변형율 거동은 무보강시 보다 다일러턴시의 양이 작고, 축변형율 증가시 항복 이후에도 축차응력이 증가하는 변형율경화(strain hardening) 거동을 나타내었다. 토목섬유로 보강된 슬래그 재료의 겉보기 점착력과 내부마찰각 등의 강도정수는 보강되지 않은 경우의 값보다 1.2-1.4배 정도 크고, 구속압 수준이 클수록 커지는 것으로 나타났다. 따라서 슬래그를 사용한 제방의 설계나 시공시 슬래그 재료에 토목섬유를 층상으로 보강하여 사용할 경우에는 강도증가 효과에 의해 안전율을 향상시킬 수 있을 것으로 기대된다.

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Investigation of Spark Plasma Sintering Temperature on Microstructure and Thermoelectric Properties of p-type Bi-Sb-Te alloys

  • Han, Jin-Koo;Shin, Dong-won;Madavali, Babu;Hong, Soon-Jik
    • 한국분말재료학회지
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    • 제24권2호
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    • pp.115-121
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    • 2017
  • In this work, p-type Bi-Sb-Te alloys powders are prepared using gas atomization, a mass production powder preparation method involving rapid solidification. To study the effect of the sintering temperature on the microstructure and thermoelectric properties, gas-atomized powders are consolidated at different temperatures (623, 703, and 743 K) using spark plasma sintering. The crystal structures of the gas-atomized powders and sintered bulks are identified using an X-ray diffraction technique. Texture analysis by electron backscatter diffraction reveals that the grains are randomly oriented in the entire matrix, and no preferred orientation in any unique direction is observed. The hardness values decrease with increasing sintering temperature owing to a decrease in grain size. The conductivity increases gradually with increasing sintering temperature, whereas the Seebeck coefficient decreases owing to increases in the carrier mobility with grain size. The lowest thermal conductivity is obtained for the bulk sintered at a low temperature (603 K), mainly because of its fine-grained microstructure. A peak ZT of 1.06 is achieved for the sample sintered at 703 K owing to its moderate electrical conductivity and sustainable thermal conductivity.

Quantitative Comparison of Activity Calculation Methods for the Selection of Most Reliable Radionuclide Inventory Estimation

  • Hwang, Ki-Ha;Lee, Sang-Chul;Lee, Kun-Jai;Jeong, Chan-Woo;Ahn, Sang-Myeon;Kim, Tae-Wook;Kim, Kyoung-Doek;Herr, Y.H.
    • 한국방사성폐기물학회:학술대회논문집
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    • 한국방사성폐기물학회 2003년도 가을 학술논문집
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    • pp.322-327
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    • 2003
  • It is important to know the accurate radionuclide inventory of radioactive waste for the reliable management. However, estimation of radionuclide concentrations in drummed radioactive waste is difficult and unreliable because of difficulties of direct detection, high cost, and radiation exposure of sampling personnel. In order to overcome these difficulties, scaling factors (SFs) have been used to assess the activities of radionuclides that could not be directly analyzed. A radionuclide assay system has been operated at KORI site since 1996 and consolidated scaling factor method has played a dominant role in determination of radionuclides concentrations. However, some problems are still remained such as uncertainty of estimated scaling factor values, inaccuracy of analyzed sample values, and disparity between the actual and ideal correlation pairs and the others. Therefore, it needs to improve the accuracy of scaling factor values. The scope of this paper is focused on the improvement of accuracy and representativeness of calculated scaling factor values based on statistical techniques. For the selection of reliable activity determination method, the accuracy of estimated SF values for each activity determination method is compared. From the comparison of each activity determination methods, it is recommended that SF determination method should be changed from the arithmetic mean to the geometrical mean for more reliable estimation of radionuclide activity. Arithmetic mean method and geometric mean method are compared based on the data set in KORI system.

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비닐하우스 기초 토양의 다짐률 변화에 따른 전단강도 특성 (Experimental Evaluation of Shear Strength of Surface Soil Beneath Greenhouse Varying Compaction Rate)

  • 임성윤;허기석;곽동엽
    • 한국농공학회논문집
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    • 제63권6호
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    • pp.17-26
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    • 2021
  • Greenhouses have been damaged due to the uplift pressure from strong wind, for which rebar piles are often installed near the greenhouse to resist the pressure. For the effective design of rebar piles, it is necessary to access the shear strength of soil on which the greenhouse is constructed. This study experimentally evaluates the shear strength of the soil beneath the greenhouse. Four soil samples were collected from four agricultural sites, and prepared for testing with 75, 80, 85, and 90% compaction rates. One-dimensional unconfined compression test (UC), consolidated-undrained triaxial test (CU), and resonant column test (RC) were performed for the evaluation of shear strength and shear modulus. Generally, the higher shear strength and modulus were observed with the higher compaction rates. In particular, the UC shear strength increases with the increase of #200 sieve passing rate. Resulting from the CU test, the sample with the most of coarse soil had the highest friction angle, but the variation is small among samples. Resulting from the CU and RC tests, the ratio of maximum shear modulus with the major principle stress at failure was the higher at the finer soil. The ratio was two to three times greater than the ratio from the standard sand. This indicates that the shear strength is lower for the fine soil than the coarse soil at the same shear modulus. The results of this study will be a useful resource for the estimation of the pull-out strength of the rebar pile against the uplift pressure.

A comprehensive quality analysis of randomized controlled clinical trials of Asian ginseng and American ginseng based on the CONSORT guideline

  • Chen, Weijie;Li, Xiuzhu;Chen, Zhejie;Hao, Wei;Yao, Peifen;Li, Meng;Liu, Kunmeng;Hu, Hao;Wang, Shengpeng;Wang, Yitao
    • Journal of Ginseng Research
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    • 제46권1호
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    • pp.71-78
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    • 2022
  • Ginseng is an international herb that has been used for thousands of years. Two species most commonly applied and investigated in the ginseng family are Asian ginseng and American ginseng. The number of randomized controlled clinical trials (RCTs) has conspicuously increased, driven by the rapid development of ginseng. However, the reporting of RCT items of ginseng is deficient because of different trial designs and reporting formats, which is a challenge for researchers who are looking for the data with high quality and reliability. Thus, this study focused on providing an extensive analysis of these two species and examined the quality of the RCTs, based on the Consolidated Standards of Reporting Trials (CONSORT) guideline. Ninety-one RCTs conducted from 1980 to 2019 that were related to Asian ginseng and American ginseng used singly met our inclusion criteria. We found that the reporting quality of the two species has improved during the past 40 years. Publication date and sample size were significantly associated with the reporting quality. Rigorous RCTs designed for the species of ginseng are warranted, which can shed light on product research and development of ginseng in the future.

Mechanical properties of tailings with dipping interlayers under high confining pressure

  • Qinglin, Chen;Zugui, Li;Zeyu, Dai;Xiaojun, Wang;Chao, Zhang
    • Geomechanics and Engineering
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    • 제31권6호
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    • pp.557-571
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    • 2022
  • Landslides are often triggered by weak interlayers initiated in tailings dam foundations, and hazards gradually occur. This is serious for landslides in high tailings dams due to their high potential energy. Tailing samples with a fine-grained interlayer at a set dip angle were prepared. Consolidated undrained (CU) triaxial shear tests were carried out by using a high-pressure triaxial apparatus. The results were compared with the results under a low confining pressure. Four reasons were summarized for high tailings dams more prone to instability than low dams. The shear strength of the samples with dipping interlayers decreases with increasing dip angle. An obvious straight drop in the stress path after the peak occurs in samples with dipping interlayers at an angle of 60°. The effect of the interlayer on the mechanical behaviour of tailings is very sensitive, especially for the sample with a dipping interlayer at an angle of 60°. Shear slipping along the interlayer should be given more attention in tailings dams. Compared with the results under low confining pressure, the stress decreases continuously for the samples with dipping interlayers at large angles under high confining pressure. The positive pore pressure, which reduces the effective stress, occurred in tailings samples under high confining pressure. The residual strength of tailings under high confining pressure is smaller than that under low confining pressure. These factors increase the dam break risk and the disaster impact for high tailings dams.

고결모래의 비배수 전단거동 (Undrained Shear Behavior of Cemented Sand)

  • 이문주;최성근;홍성진;이우진
    • 대한토목학회논문집
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    • 제26권3C호
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    • pp.181-190
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    • 2006
  • 본 연구에서는 석고함유율을 달리한 고결된 모래 시료를 조성하여 고결정도 및 상대밀도에 따른 고결모래의 거동양상을 분석하였다. 상대밀도 25, 40, 60%의 모래에 모래중량비 5~20%의 석고를 혼합하여 교반시킨 후 상재하중 55kPa 상태에서 양생하여 시료를 조성하였다. 조성된 고결시료는 일정한 구속압(200kPa)상태에서 비배수 전단시험(CIU)이 실시되었다. 실험 결과 고결정도의 증가에 따른 고결된 모래의 항복강도 및 강성의 증가양상을 확인하였고, 고결 결합이 파괴되기 전에는 다일레이션 경향이 억제되지만, 결합이 파괴된 직후 다일레이션 경향이 오히려 증가하는 것으로 나타났다. 또한 고결정도 및 상대밀도에 따라 간극수압 발생경향이 변하였으며, 고결에 의해 상전이선 및 파괴포락선에서의 유효응력비가 변하는 것을 유효응력경로 분석을 통하여 확인하였다. 일반적으로 상대밀도에 비해 고결정도가 고결된 모래의 거동에 더 큰 영향을 끼치는 것으로 나타났다.

Reduction of Thermal Conductivity Through Complex Microstructure by Dispersion of Carbon Nanofiber in p-Type Bi0.5Sb1.5Te3 Alloys

  • P. Sharief;B. Madavali;Y. Sohn;J.H. Han;G. Song;S.H. Song;S.J. Hong
    • Archives of Metallurgy and Materials
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    • 제66권3호
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    • pp.803-808
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    • 2021
  • The influence of nano dispersion on the thermoelectric properties of Bi2Te3 was actively investigating to wide-spread thermoelectric applications. Herein this report, we have systematically controlled the microstructure of Bi0.5Sb1.5Te3 (BST) alloys through the incorporation of carbon nanofiber (CNF), and studied their effect on thermoelectric properties, and mechanical properties. The BST/x-CNF (x-0, 0.05, 0.1, 0.2 wt.%) composites powder was fabricated using high energy ball milling, and subsequently consolidated the powder using spark plasma sintering. The identification of CNF in bulk composites was analyzed in Raman spectroscopy and corresponding CNF peaks were recognized. The BST matrix grain size was greatly reduced with CNF dispersion and consistently decreased along CNF percentage. The electrical conductivity was reduced and Seebeck coefficient varied in small-scale by embedding CNF. The thermal conductivity was progressively diminished, obtained lattice thermal conductivity was lowest compared to bare sample due to induced phonon scattering at interfaces of secondary phases as well as highly dense fine grain boundaries. The peak ZT of 0.95 achieved for 0.1 wt.% dispersed BST/CNF composites. The Vickers hardness value of 101.8 Hv was obtained for the BST/CNF composites.

PL 리더십 성향과 프로젝트 특성요인이 프로젝트 참여 만족 및 성과에 미치는 영향 (The Effect of PL Leadership and Characteristics of Project on Project Participants' Satisfaction and Performance)

  • 양희동;김명진;강소라
    • Asia pacific journal of information systems
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    • 제20권4호
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    • pp.53-79
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    • 2010
  • The study was originated from recognition that project participants' satisfaction should be Improved to raise project performance and to make progress of a successful project since the above dissatisfaction was operated as a danger factor of the project. The study selected one large-scale sample project and attempted measuring characteristics of the project, participants' satisfaction and project performance with the whole project participants. The study analyzed correlations between individual level (team members) and group level (development team), and examined what effect a sub project manager under complicated hierarchical organization of the large-scale project, namely PL (project leader)'s leadership style had on each individual project participant's satisfaction and what effect project uncertainty in organization/technology environment had on project participants' satisfaction and project performance. The study verified that development team (group) had an effect on team member (individual)-level project participants' satisfaction by disclosing that there was a significant dispersion among groups within project participants' satisfaction by each individual. It is analyzed that it is necessary to make improvement through approach by each pertinent team to raise individual-level project participants' satisfaction. The study also verified PL's ideal leadership under strict methodology and hierarchical control of the large-scale project. Based on the verification of the hypotheses, the results of the analysis were produced as follows. First, the development team affects the satisfaction level that an individual has when he/she participates in a project. This suggests that the satisfaction with project participation should be improved at the team level. In addition, the project management style and leadership orientation of the manager of a sub project who is mostly affected by the team proved to have a direct influence on the satisfaction with project participation and project performances. Second, both the performance-oriented leadership and the relationship-oriented leadership of the PL of the development team were verified to have a significant effect on the satisfaction of the team members associated with project participation. In other words, when the team members recognize that the PL of the development team shows both the performance-oriented leadership and the relationship-oriented leadership, their satisfaction with project participation increases accordingly. Third, it was verified that the uncertainty of the organizational environment significantly affects the satisfaction level when the PL of the development team exerts a relationship-oriented and performance-oriented leadership. The higher the uncertainty of the organizational environment is, the more the satisfaction with project participation decreases whereas the relationship-oriented leadership has a more positive effect on the satisfaction than the performance-oriented leadership style. Fourth, when the PL of the development team exerts the relationship-related and performance-related leadership, the uncertainty of the technological environment has a significant influence on the satisfaction level. The higher the uncertainty of the technological environment is, the more the satisfaction with project participation decreases whereas the performance-oriented leadership has a more positive effect on the satisfaction than the relationship-oriented leadership style. The result of the research on the uncertainty of the project environment suggests that when the development team leader exerts a relationship-oriented and performance-oriented leadership style, the uncertainty of the organizational environment has a significant effect on the satisfaction with project participation; the higher the uncertainty of the organizational environment, the more the satisfaction level decreases, and the relationship-oriented leadership style affects the satisfaction level more positively than the performance-oriented leadership style. In addition, when the development team leader displays a relationship-oriented and performance-oriented leadership style, the uncertainty of the technological environment has a significant effect on the satisfaction with project participation; the higher the uncertainty of the technological environment. the more the satisfaction level decreases. The performance-oriented leadership style as well affects the satisfaction level more positively than the relationship-oriented leadership style. Based on the above results, the research provides the following implications when handling multiple concurrent projects. First, the satisfaction with the participation in the multiple concurrent projects needs to be enhanced at the team (group) level. Second. the manager of the project team, particularly the middle managers should have both a performance-oriented and relationship (task and human)-oriented attitude and exert a consolidated leadership in order to improve the satisfaction of team members with project participation and their performances. Third, as the uncertainty factor of the technological and organizational environment among the characteristics factors of the project has room for methodological improvement depending on one's effort even though there are some complications, we need to continuously prevent and control the risks resulting from the uncertainties of the technological and organizational environment of the project in order to enhance the satisfaction of project participation and project performances. Fourth, the performance (task)-oriented leadership is required when there is uncertainty in a technological environment while the relationship (human)-oriented leadership is required when there is uncertainty in an organizational environment. This research has the following limitations. First, this research intended to select one large-sized sample project and measure the project characteristics, the satisfaction of all the participants associated with project participation, and their performances. Therefore, it is inappropriate to generalize and apply the result of this result onto other numerous projects. Second, as this case study entailed a survey to measure the characteristics factors and performance of the project, since the result value was based on the perception of project team members, the data may have insufficient objectivity. Third, though this research targeted on all the project participants, some development teams did not provide sufficient data and questionnaires were collected from some specific development teams among the 23 development teams, causing a significant deviation in the response rate among the development teams. Therefore, we need to continuously conduct the follow-up researches making comparisons among the multiple projects, and centering on the characteristics factors of the project and its satisfaction level.