• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.04a
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• pp.219-222
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• 2004

The effects of short fiber and particle hybrid reinforcement on fatigue crack propagation behaviors in aluminum matrix composites have been investigated. Single and hybrid reinforced 6061 aluminum containing same 20 $Al_2O_3\;volume\%$ with four different constituent ratios of short fibers and particles were prepared by squeeze casting method and tested to check the near-threshold and stable crack growth behavior. The fatigue threshold of the composites increased with portion of particle contents and showed the improved crack resistance especially in low stress intensity range. Addition of particle instead of short fiber also increased fracture toughness due to increase of inter-reinforcement distance. These increase in both fatigue threshold and fracture toughness eventually affected the fatigue crack growth behavior such that the crack growth curve shift low to high stress intensity factor value. Overall experimental results were shown that particle reinforcement was enhanced the fatigue crack resistance over the whole stress intensity factor range.

• Journal of Adhesion and Interface
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• v.12 no.1
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• pp.16-25
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• 2011

Multi core-shell composite particles were prepared by the water-born emulsion polymerization of various core monomer such as methyl methacrylate (MMA), n-butyl methacrylate (BMA), and shell monomer such as MMA, BMA, stylene (St), 2-hydroxyl ethyl methacrylate (2-HEMA) and acrylic acid (AA) in the presence of different concentration of sodium dodecyl benzene sulfonate (SDBS). The following conclusions are drawn from the measured conversion, particle size and distribution, average molecular weight, molecular structure, glass transition temperature with DSC, morphology, tensile strength and elongation. In the case of the concentration of 0.02 wt% SDBS, the conversion of MMA core-(BMA/St/AA) shell composite particle was excellent as 98%. In the case of the concentration of 0.03 wt% SDBS, the particle size of BMA core-(MMA/St/AA) shell composite particle was high as $0.47{\mu}m$. We confirmed that 3 points of glass transition temperatures appear for multi core-shell composite particles compared to 2 points of glass transition temperatures appear for general core-shell composite particles. We showed that it is possible to adjust glass transition temperatures according to the kind and composition of the inner shell monomer that it is can be used as a adhesive binder material with improved adhesive power.

• Preventive Nutrition and Food Science
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• v.3 no.3
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• pp.292-294
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• 1998

Surimi sol and gel were prepared by mixing egg albumin, starch, oil and carrageenan, which are used as representative ingredients in the surimi composite, at different ratio. Structural properties in surimi composite were investigated by examining the phase changes and dispersion pattern (average particle size, size range and the averge number of particle) of the particulate ingredients in sol and gel with an image analyzer. A staining technique of the specimen containing egg albumin in surimi gel was developed by adjusting pH of a toluidine staining solution. Image analysis revealed that size and density of ingredient particles were function of the level and dispersion of ingredients except of starch-incorporated surimi gel which showed maximum particle size at 6%.

• Journal of the Korean Society of Manufacturing Technology Engineers
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• v.8 no.5
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• pp.42-46
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• 1999

The strengthening of a metal matrix composite(MMC) by the shape memory effect(SME) of dispersed TiNi particles was theoretically studied. An analytical model was constructed for the prediction of the average residual stress(<$\delta$>m) on the base of the Eshelby's equivalent inclusion method. The analysis was performed on the TiNi particle/Al metal matrix composites with varying volume fractions and prestrains of the particle. The residual stress caused by the shape memory of predeformed fillers has been predicted to contribute significantly to the strengthening of this composite.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.1
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• pp.25-31
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• 2001

The theoretical modeling to predict the modulus of elasticity by the shape memory effect of dispersed particles in a metal matrix composite was studied. The modeling approach is based on the Eshelbys equivalent inclusion method and Mori-Tanakas mean field theory. The calculation was performed on the TiNi particle dispersed Al metal matrix composites(PDMMC) with varying volume fractions and prestrains of the particle. It was found that the prestrain has no effect on the Yonugs modulus of PDMMC but the volume fraction does affects it. This approach has an advantage of definite control of Youngs modulus in PDMMCs.

• Journal of the Korean Ceramic Society
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• v.30 no.2
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• pp.123-130
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• 1993

Dispersed type Al2O3-SiC composite powders were synthesized from Al-isopropoxide (Al(i-OC3H7)3) and Si(OC2H5)4 precursors by hydrolysis of mixed alkoxides and carbothermal reaction method. The characteristics of the synthesized (dispersed type) Al2O3-SiC composite powders were investigated using XRD, SEM, TEM, BET and particle size analyzer. Carbothermal reaction to produce Al2O3-SiC composite was completed in 10h at 135$0^{\circ}C$ on 3~4㎤/s (0.21~0.28cm/s) of H2 flow rate and about 1/1 of carbon/oxides(=SiO2＋Al2O3) molar ratio. The synthesized powders were observed to have the mean particle size range of 0.4~1.26${\mu}{\textrm}{m}$ and showed finer particle size with increasing SiC content.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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• 1998.10a
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• pp.124-130
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• 1998

The wear characteristics and wear mechanisms of dental composite resins were investigated. Composite resins such as Metalii, Silux Plus, Heliomolar and Palfique Estelite were selected as specimens and contents of filler in specimens in order to analyze the effect of Prepolymerized Particle Fillers in friction and wear characteristics. Ball on flat wear tester was used for a wear test. Friction and wear tests are carried out at room temperature. The friction coefficient of Metafil was quite high relatively, and the wear resistance of Silux Plus and Palfique Estelite was better than that of Metafil and Hellomolar at the same experimental condition. The main wear mechanism is plastic flow and abrasive wear by crack propagation.

• Bulletin of the Korean Chemical Society
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• v.23 no.8
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• pp.1127-1134
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• 2002

Fine ceramic particles of zirconia toughened alumina (ZTA), titania toughened alumina (TTA), and zirconia-titania toughened alumina (ZTTA) have been synthesized by ultrasonic spray pyrolysis (USP) at various temperatures from starting salt solutio ns of various compositions aiming for the development of catalytic material. These particles were characterized for properties such as shape, size and size distribution, diffraction pattern, and chemical and phase composition of elements by scanning electron microscopy (SEM), particle size analyzer (PSA), x-ray diffraction (XRD), and inductively coupled plasma-atomic emission spectroscopy (ICP-AES). Chemical compositions and sizes of ceramic composites have been controled by the stoichiometry of salt solutions and the flow rate of spraying solutions. The optimum experimental conditions for the various composite particle syntheses have been proposed.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 1999.05a
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• pp.147-152
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• 1999

The strengthening of a metal matrix composite(MMC) by the shape memory effect(SME) of dispersed TiNi particles was theoretically studied. An analytical model was constructed for the prediction of the average residual stress(<$\sigma$>/sub/m) on the base of the Eshelby's equivalent inclusion method. The analysis was performed on the TiNi particle/Al metal matrix composites with varying volume fractions and prestrains of the particle. The residual stress caused by the shape memory of predeformed fillers has been predicted to contribute significantly to the strengthening of this composite.

• Journal of the Semiconductor & Display Technology
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• v.10 no.2
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• pp.91-95
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• 2011

Ni-CNT(carbon nanotubes) composite coating is often used for the surface treatment of electronic/mechanical devices to improve the properties of the exisiting Ni electroplating. For this, the dispersion of CNT particle is a critical process. In this study, ball milling and additive called sodium dodecyl sulfate(SDS) are employed for dispersion. Electroplated Ni-CNT films were examined by SEM-EDX, AES, microhardness tester, 4-point probe and contact angle measurement to find the optimum dispersion conditions. Ni-CNT coatings formed by ball milling for 9 hrs and with addition of SDS 12 times of CNT contents showed the highest hardness, reasonable resistivity and non-stick characteristics.