• 대한치과보철학회지
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• 제48권2호
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• pp.143-150
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• 2010

연구목적: 본 연구의 목적은 냉간 정수압 성형법 (cold isostatic press forming)을 이용한 새로운 지르코니아 블록의 제조와 이를 이용한 코어와 완전 도재관의 적합도를 비교 평가하여 임상적 이용 가능성을 평가 하고자 함이다. 연구 재료 및 방법:지르코니아 분말 (KZ-3YE Type A)을 단일 압축 성형하여 블록의 형태로 제작 한 후, 냉간 정수압 성형하여 블록을 제작하고, 성형이 끝난 지르코니아 블록은 $1040^{\circ}C$의 온도에서 반 소결하였다. 대조군은 상용 제품 ($Everest^{(R)}$, KAVO, Biberach/$Ri{\beta}$.)을 이용하였다. $1450{^{\circ}C}$의 온도에서 완전 소결된 실험군 블록과 대조군 블록의 수축률을 측정하고 비교하였다. CAD/CAM을 이용하여 총 21개의 코어를 제작하고 세 그룹으로 나누었다. Group I은 대조군 블록을 이용해 7개의 코어를 제작하고, Group II는 실험군 블록을 이용해 7개의 코어를 제작하였다. Group III은 실험군 블록을 이용해 7개의 코어를 제작하고 도재 ($Cerabien^{TM}$)를 축성하여 완전 도재관을 제작하였다. 제작된 코어와 완전 도재관을 모형에 합착한 후 레진으로 매몰하여 치관 장축의 협설과 근원심 방향을 따라 절단하고 지대치와 코어 사이의 변연 간격과 내부 축면 간격 그리고 내부 교합면 간격을 SEM ($S-4700^{(R)}$)을 이용해 측정하였다. 모든 측정값은 평균과 표준편차를 계산하고, one-way ANOVA test를 시행하여 실험 결과를 분석하였고, 95%유의 수준으로 검정하였다. 결과:실험군과 대조군 블록의 수축률을 측정한 결과 실험군 블록의 수축률은 19.00%였고, 대조군 블록의 수축률은 20.09%로 실험군 블록의 수축률이 더 낮은 것으로 나타났다. 적합도 측정 결과 변연 간격의 측정값에서 Group II의값($29.67{\pm}6.58 {\mu}m$)이 Group I의값($36.84 {\pm}7.18 {\mu}m$)보다 통계적으로 유의하게 작은 것으로 나타났다. 또한 Group II와 Group III의 값 사이에서는 유의한 차이가 없었다. 내부 측면 간격의 측정값에서 Group III의값($32.23{\pm}6.33 {\mu}m$)이 Group I와 Group II의내부측면간격의값($37.57{\pm}6.81{\mu}m$, $38.14{\pm}6.81{\mu}m$)보다 큰 것으로 나타났다. 각 부위의 간격 측정결과 내부 교합면 간격의 값이 변연 간격 및 내부 축면 간격의 값보다 유의하게 큰 것으로 나타났다. 결론: 현재 상용중인 대조군 블록과 비교하여 냉간 정수압 성형법으로 제조된 실험군 블록의 적합도는 유의한 차이를 보이지 않았다. 변연 적합도는 실험군에서 더 우수하였으며 도재를 축성한 완전 도재관의 적합성이 약간 더 향상되는 경향을 보였다. 변연 적합도는 대조군과 실험군 모두에서 임상적으로 허용되는 양호한 수치를 보였다.

• 한국초전도ㆍ저온공학회논문지
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• 제4권2호
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• pp.16-20
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• 2002

Bi-axially textured Ni tapes for YBCO coated conductors were Prepared by cold rolling and heat treatment of Ni Powder compacts. The Ni powder used in this study was 5 urn in particle size and 99.99 % in purity. The process of this study consists of filling of hi powder into a rubber mold, cold-isostatically Pressing and sintering of the powder compacts at 110$0^{\circ}C$ for 6h in 96 % Ar - 4 % H$_2$ atmosphere. The sintered compacts were cold rolled with a 5 % step reduction ratio into a 100 micron-thick tapes and then heat-treated at 100$0^{\circ}C$ for various time periods. The (200) texture of Ni tape was successfully developed through the recrystallization heat treatment of the cold rolled Ni tapes. At 100$0^{\circ}C$, the degree of texture of the heat-treated Ni tapes seems not to be significantly affected by the heat-treatment time. The short heat treatment of S min was sufficient to develop the complete (200) cube texture. The degree of in-Plane and out-of-plane texture of the prepared Ni tapes was 8-10$^{\circ}$. The heat treated Ni tapes consisted of equiaxed grains with a size 50-70 microns. and the AFM sol-face roughness was as smooth as 3 nm.

• Progress in Superconductivity
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• 제4권1호
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• pp.94-98
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• 2002

Two kinds of multifilament Bi-2223／Ag tapes, which are different in the precursor calcination temperatures, were heat treated for different time (12, 20, 30, 50, 70, or 100 h) firstly to obtain varied B2223 contents, and then followed by the same pressing and sintering cycles. The relation of the 2223 phase contents after the first sintering and the transport property of the fully processed tapes was studied. The results show that 75-80% 2223 phase formed in tapes before the first cold pressing is beneficial to get a high $I_{c}$ in the final tapes. Compensating the total heat treatment time of the tapes first sintered for 20 h to the same length as that first sintered for 50 h in the subsequent sintering stages, different $I_{c}$ enhancements were observed in these two tapes. No improvement on $I_{c}$ was found in the tape made from the powder calcined at higher temperature, whereas for the tape prepared with the lower temperature calcined powder, the $I_{c}$ was increased to the same level as that first sintered for 50 h. The 2223 contents before the intermediate mechanical work is related to the residual reactants, especially to the liquid phase, which is of vital importance to the phase conversion and healing microcracks, meanwhile, to the size and distribution of the non-superconducting secondary phases. The lower temperature calcined powder resulted in slow formation of 2223 phase, but also provided more reactants and liquid phase for the further phase conversion, as a consequence, for the Improvement of $I_{c}$. c/.

• 한국결정성장학회지
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• 제24권4호
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• pp.176-182
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• 2014

상온 압축 성형 후 고상 반응 소결 공정을 통하여 $Mg_3Sb_2$ 소결체를 제조하고자 하였다. Mg과 Sb의 성분의 몰비와 반응온도에 따른 결정상의 변화를 조사하였다. 773~843 K에서 얻어진 고상반응 소결체들은 전형적인 $Mg_3Sb_2$ 결정상을 형성하였으나 소결체의 위치에 따라 약간 다른 상적 구성을 보였다. 소결체 하단 부위에서 전형적으로 얻어지는 결정상이 얻어졌으며 823 K 온도에서는 Mg : Sb = 3.15 : 1.85 조성일 때, 843 K 온도에서는 Mg의 몰 수가 3.10 이상인 모든 조성에서 ${\alpha}-Mg_3Sb_2$ 상과 정확히 일치하는 결정상이 얻어졌다. 미량 남아있는 Mg 성분은 응고 후 냉각 시 ${\alpha}-Mg_3Sb_2$ 상으로부터 석출된 것으로 보인다.

• 한국분말재료학회지
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• 제24권3호
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• pp.202-209
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• 2017

A cold-work tool steel powder is used to fabricate 3-dimensional objects by selective laser melting using a high-pressure gas atomization process. The spherical powder particles form continuous carbide networks among the austenite matrix and its decomposition products. The carbides comprise Nb-rich MC and Mo-rich $M_2C$. In the SLM process, the process parameters such as the laser power (90 W), layer thickness ($25{\mu}m$), and hatch spacing ($80{\mu}m$) are kept fixed, while the scan speed is changed from 50 mm/s to 4000 mm/s. At a low scan speed of 50 mm/s, spherical cavities develop due to over melting, while they are substantially reduced on increasing the speed to 2000 mm/s. The carbide network spacing decreases with increasing speed. At an excessively high speed of 4000 mm/s, long and irregularly shaped cavities are developed due to incomplete melting. The influence of the scan pattern is examined, for which $1{\times}1 mm^2$ blocks constituting a processing layer are irradiated in a random sequence. This island-type pattern exhibits the same effect as that of a low scan speed. Post processing of an object using hot isostatic pressing leads to a great reduction in the porosity but causes coarsening of the microstructure.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 추계학술대회 논문집
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• pp.181-184
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• 2009

The hot press farming process, which is the press hardening of steel parts using cold dies, can utilize both ease of shaping and high strength due to the hardening effect of rapid quenching during the pressing. In this study, a thermo-elastoplastic analysis of the hot press forming process using the finite element method was performed in order to investigate the deformation behavior and temperature history during the process and the mechanical properties of the pressed parts.

• 한국세라믹학회지
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• 제46권3호
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• pp.317-322
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• 2009

Statistical designs of experiments were applied in order to understand the effect of processing variables on the brightness of inorganic electroluminescent displays. The main effects and interaction of phosphor and dielectric layers are estimated to be statistically significant. Additional improvement was made on removing the pores in the thick films, using the defoaming in pastes and cold isostatic pressing in bonding the top and bottom parts of the inorganic electroluminescent devices. Such optimization contributed to the reduction in the corresponding threshold voltage and enhancement in the brightness.

• 한국가구학회지
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• 제18권1호
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• pp.20-30
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• 2007

This experiment was carried out to investigate the effects of number and location of finger joints on the bending strength of glue-laminated lumbers. Urea resin adhesives were used in this experiment and the resin content was 70% for cold pressing. The lamina were edge-jointed and end-jointed. The specimen were composed of one or three layers. The obtained results are summarized as follows; The effects of finger joints on the decrease of bending strength of glue laminated woods were different according to the number and location of finger joints. The decrease of MOR was highest on the middle position of laminated woods. The effects of several arrangements of finger joints on the bending strength of glue laminated woods showed on Figure 7 and 8. The variance of thickness-laminating on the bending strength of glue laminated woods were larger than those of width-laminating.

• 한국분말재료학회지
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• 제16권1호
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• pp.50-55
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• 2009

Numerical simulations of the powder extrusion need an appropriate pressure-dependent constitutive model for densification modeling of the magnesium powders. The present research investigated the effect of representative powder yield function of the critical relative density model. We could obtain reasonable physical properties of pure magnesium powders using cold isostatic pressing. The proposed densification model was implemented into the finite element code. The finite element analysis was applied to simulation of powder extrusion of pure magnesium powder in order to investigate the densification and processing load at room temperature.

• 대한방사선기술학회지:방사선기술과학
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• 제23권1호
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• pp.97-101
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• 2000

In this study, the highly sensitive $CaSO_4:Tm$-PTFE TLDs has been fabricated for the purpose of measurement of high energy electron. $CaSO_4:Tm$ phosphor powder was mixed with polytetrafluoroethylene(PTFE) powder and moulded in a disk type(diameter 8.5 mm. thickness $90\;mg/cm^2$) by cold pressing. The absorbed dose distribution and ranges for high energy electron were measured by using the $CaSO_4:Tm$-PTFE TLDs. The ranges determined were $R_{100}=14.5mm$, $R_{50}=24.1mm$ and $R_P=31.8mm$, respectively and the beam flatness, the variation of relative dose in 80% of the field size, was 4.5%. The fabricated $CaSO_4:Tm$-PTFE TLDs nay be utilized in radiation dosimetry for personal, absorbed dose and environmental monitoring.