• Title/Summary/Keyword: Coating defects

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Densification and Electrical Conductivity of Plasma-Sprayed (Ca, Co)-Doped LaCrO3 Coating (플라즈마 스프레이 (Ca, Co)-Doped LaCrO3 코팅층의 치밀화 및 전기전도도)

  • Park, Hee-Jin;Baik, Kyeong-Ho
    • Korean Journal of Materials Research
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    • v.27 no.3
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    • pp.155-160
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    • 2017
  • Doped-$LaCrO_3$ perovskites, because of their good electrical conductivity and thermal stability in oxidizing and/or reducing environments, are used in high temperature solid oxide fuel cells as a gas-tight and electrically conductive interconnection layer. In this study, perovskite $(La_{0.8}Ca_{0.2})(Cr_{0.9}Co_{0.1})O_3$ (LCCC) coatings manufactured by atmospheric plasma spraying followed by heat treatment at $1200^{\circ}C$ have been investigated in terms of microstructural defects, gas tightness and electrical conductivity. The plasma-sprayed LCCC coating formed an inhomogeneous layered structure after the successive deposition of fully-melted liquid droplets and/or partially-melted droplets. Micro-sized defects including unfilled pores, intersplat pores and micro-cracks in the plasma-sprayed LCCC coating were connected together and allowed substantial amounts gas to pass through the coating. Subsequent heat treatment at $1200^{\circ}C$ formed a homogeneous granule microstructure with a small number of isolated pores, providing a substantial improvement in the gas-tightness of the LCCC coating. The electrical conductivity of the LCCC coating was consequently enhanced due to the complete elimination of inter-splat pores and micro-cracks, and reached 53 S/cm at $900^{\circ}C$.

Implementation of a system for detecting defects on optical fiber coating (Vision System을 이용한 광섬유 코팅 결함 검출 System 구현)

  • 서상일;최우창;김학일
    • 제어로봇시스템학회:학술대회논문집
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    • 1996.10b
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    • pp.796-799
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    • 1996
  • 광섬유는 코어(Core), 클레드(Clad), 그리고 1,2차 코팅(Coating)으로 구성되어 있다. 본 연구에서는 광섬유의 코팅에 생기는 결함의 유무 및 종류와 크기를 분류하는 Vision System을 구현하였다. 전처리 과정으로, CCD Camera를 이용하여 얻은 화상에 대하여 Sobel 연산자로 경계선을 추출하고, 문턱값(Threshold Value)을 적용하여 이진 화상을 만든다. 외경 정보 추출을 위하여, 투영 정보, 수리 형태학(Mathematical Morphology)적 연산을 수행하고, 결함의 종류와 크기를 효율적으로 분류하도록 Tree Classifier를 설계하였다. 실험 결과로서 각 결함 별 오차율, 전체 오차율(Total Error Rate)등을 제시하였다.

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Humidity Induced Defect Generation and Its Control during Organic Bottom Anti-reflective Coating in the Photo Lithography Process of Semiconductors

  • Mun, Seong-Yeol;Kang, Seong-Jun;Joung, Yang-Hee
    • Journal of information and communication convergence engineering
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    • v.10 no.3
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    • pp.295-299
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    • 2012
  • Defect generation during organic bottom anti-reflective coating (BARC) in the photo lithography process is closely related to humidity control in the BARC coating unit. Defects are related to the water component due to the humidity and act as a blocking material for the etching process, resulting in an extreme pattern bridging in the subsequent BARC etching process of the poly etch step. In this paper, the lower limit for the humidity that should be stringently controlled for to prevent defect generation during BARC coating is proposed. Various images of defects are inspected using various inspection tools utilizing optical and electron beams. The mechanism for defect generation only in the specific BARC coating step is analyzed and explained. The BARC defect-induced gate pattern bridging mechanism in the lithography process is also well explained in this paper.

Study of Meniscus Formation in a Double Layer Slot Die Head Using CFD (CFD를 이용한 Double Layer 슬롯 다이 헤드의 메니스커스 형성 연구)

  • Gieun Kim;Jongwoon Park
    • Journal of the Semiconductor & Display Technology
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    • v.23 no.2
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    • pp.65-70
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    • 2024
  • Using a computational fluid dynamics(CFD) simulation tool, we have provided a coating guideline for slot-die coating with a double layer slot die head. We have analyzed the fluid dynamics in terms of the coating speed, flow rate ratio, and viscosity ratio, which are critical for the stability of coating meniscus. We have identified the common coating defects such as break-up, air entrainment, and leakage by varying the coating speeds. The flow rate ratio is the critical parameter determining the wet film thickness of the top and bottom layers. It is shown that when the flow rate ratio exceeds or equals 1.8, air entrainment occurs due to insufficient hydraulic pressure in the bottom layer, even though the total flow rate remains constant. Furthermore, we have found that the flow of the bottom layer is significantly affected by the viscosity of top layer. The viscosity ratio of 4 or higher obstructs the flow of the bottom layer due to the increased hydraulic resistance, resulting in leakage. Finally, we have demonstrated that as the viscosity ratio increases from 0.1 to 10, the maximum coating speed rises from 0.4 mm/s to 1.6 mm/s, and the minimum wet film thickness decreases from 800 ㎛ to 200 ㎛.

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Effect of sodium hexa-meta phosphate as pore-sealing agent on the corrosion performance of Al-Zn coating deposited by twin-wire arc thermal spray process in 3.5 wt.% NaCl solution (3.5 중량% NaCl 용액에서 쌍선 아크 용사 공정으로 증착된 Al-Zn 코팅의 부식 성능에 대한 기공 밀봉제로서의 헥사메타인산나트륨의 영향)

  • Singh, Jitendra Kumar;Adnin, Raihana Jannat;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2022.11a
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    • pp.81-82
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    • 2022
  • Al and Zn are used to protect the steel structures from corrosion. In the present studies, 15Al-85Zn alloy wires has been used for the deposition of coating by arc thermal spray process. Moreover, this process of coating exhibited severe defects formation, therefore, this coating was post-treated with different concentrations i.e. 0.05, 0.1 and 0.5M sodium hexa meta phosphate (Na6[(PO3)6]: SHMP) to fill to defects of deposited coatings and assessed their corrosion resistance in 3.5 wt.% NaCl solution with exposure periods. After the treatment, the porosity of the coating reduced significantly by formation of composite oxide films onto the coating surface. Initially, 0.5 M SHMP treated coating exhibited highest in total impedance due to significant reduction of porosity but once the exposure periods are extended, the composite oxides are dissolved, thus, total impedance is decreased.

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Effects of ta-C Coatings on Surface Characteristics of Dental Ni-Ti Files (치과용 Ni-Ti파일의 표면특성에 미치는 ta-C코팅효과)

  • Sun-Kyun Park;Han-Cheol Choe
    • Corrosion Science and Technology
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    • v.22 no.5
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    • pp.368-376
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    • 2023
  • Dental Ni-Ti files must ensure stability and resistance to fatigue fracture. DLC and ta-C were coated to remove defects on the surface and ensure stability, and the surface characteristics were investigated. When coated with DLC, it was black, and in case of ta-C coating, it was blue-black. Scratches, which are defects caused by mechanical processing, were formed on the surface of the un-coated Ni-Ti file from the end of the file along the direction of processing, with the Pro-file appearing in the vertical direction and the K-file appearing in the file direction. Scratches were reduced on the coated surface, and the surface roughness was greatly reduced after coating compared to before coating. The un-coated Ni-Ti file had the lowest hardness, the DLC-coated file had the highest hardness, and ta-C showed relatively high hardness. The elastic modulus of the DLC coating film was high, and the ta-C elastic modulus was low. The adhesion of the DLC coating film tended to be higher than that of ta-C, and the wear loss amount of DLC coating of taC was lower. The corrosion potential of the ta-C coating increased significantly, and the corrosion current density decreased.

Print Mottle : Causes and Solutions from Paper Coating Industry Perspective

  • Lee, Hak-Lae
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.40 no.5
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    • pp.60-69
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    • 2008
  • The principal reasons for applying a pigment coating to paper are to improve appearance and printability. The pigment coating provides a surface that is more uniform and more receptive to printing ink than are the uncoated fibers and, in turn, both facilitates the printing process and enhances the graphic reproduction. The improvement in print quality is readily apparent, especially in image areas or when multiple colors are involved. Although pigment coating of paper is to improve the printability, coated paper is not completely free from printing defects. Actually there are a number printing defects that are observed only with the coated papers. Among the printing defects that are commonly observed for coated papers, print mottle during multi-color offset printing is one of the most concerned defects, and it appears not only on solid tone area but also half dot print area. There are four main causes of print mottle ranging from printing inks, dampening solution, paper, and printing press or its operation. These indicates that almost every factors associated with lithographic printing can cause print mottle. Among these variation of paper quality influences most significantly on print mottle problems in multicolor offset printing, and this indicates that paper is most often to be blamed for its product deficiency as far as print mottle problems are concerned. Furthermore, most of the print mottle problems associated with paper is observed when coated papers are printed. Uncoated papers rarely show mottling problems. This indicates that print mottle is the most serious quality problems of coated paper products. Overcoming the print mottle is becoming more difficult because the operating speeds of coating and printing machines are increasing, coating weights are decreasing, and the demands on high-quality printing are increasing. Print mottle in offset printing is caused by (a) nonuniform back trap of ink caused by a nonuniform rate of ink drying, referred as "back trap mottle, and (b) nonuniform absorption of the dampening solution. Furthermore, both forms of print mottle have some relationship to the structure of the coated layer. The surest way of eliminating ink mottling is to eliminate unevenness in the base paper. Coating solutions, often easier to put into practice, should, however, be considered. In this paper the principal factors influencing print mottle of coated papers will be discussed. Especially the importance of base paper roughness, binder migration, even consolidation of coating layers, control of the drying rate, types of binders, etc. will be described.

Analysis of Wrinkle Defects and Improvement Methods in the Bending Process of PA12 Insulation-Coated Busbars (PA12 절연 코팅 부스바의 굽힘 공정에서 주름 불량 원인 분석 및 개선방안 연구)

  • Yong-Jun Jeon
    • Design & Manufacturing
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    • v.18 no.3
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    • pp.15-21
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    • 2024
  • This study investigates the causes of wrinkle defects in PA12-insulated busbars used in electric vehicles and proposes an improvement method to address these issues. Busbars, essential components for efficient current transmission in electric vehicle battery modules, require complex three-dimensional bending to optimize internal layouts. For this study, oxygen-free copper busbars with a 0.8 mm PA12 insulation coating were subjected to three types of bending tests: flat bending, edge bending, and torsional bending. Experimental results showed that wrinkle defects only occurred during edge bending, while flat and torsional bending modes exhibited no significant issues. Cross-sectional analysis revealed that the PA12 insulation layer's thickness was uneven, with thinner sections on flat areas and thicker accumulation at the comers. This uneven distribution led to poor adhesion between the insulation and copper layers, resulting in the formation of wrinkles, particularly in areas with air gaps ranging from 75 to 250 ㎛. To further analyze the issue, finite element analysis (FEA) of the bending process was performed under adhesive and non-adhesive conditions. The results confirmed that wrinkles formed when the adhesion between the copper and PA12 coating was insufficient. Improved adhesion conditions, achieved through a heat treatment process at 120℃ for 2 hours, significantly reduced the occurrence of wrinkles during edge bending. This study demonstrates that optimizing the adhesion between the insulation coating and the copper busbar, through controlled heat treatment, can prevent wrinkle defects. The findings provide a pathway for enhancing the durability and performance of insulated busbars in electric vehicle applications.

A Study on the Contact Power by Coating Material of Spray in AT Feeding Method (AT급전방식에서 코팅재에 의한 접촉전력에 대한 연구)

  • Kim, Min-Seok;Kim, Min-Kyu;Park, Yong-Gul;Lee, Jong-Woo
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.60 no.1
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    • pp.85-92
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    • 2011
  • Main characteristic in railroad is the guided movement of the wheel by the track through a metal-to-metal contact, conferring to the rail vehicle a single degree of freedom. There are defects such as head check, shelling, corrugation, squats etc in surface of the rail by interface between the wheel and rail. These defects bring about reducing the life-cycle of rails and track components and increasing noises. In case of bad conditions, it is possible to happen to full-scale accident such as derailment. Recently, the track capacity has been increased for increasing speed and operation efficiency. So, maintenance and indirect cost have been increased. Currently, a coating method of rail construction is proposed by using the ceramics in Korea. Rails are used as the earth in electrical railroad systems. Currently traction return current is flowed through wheels of trains. In case of rails coated, problems are caused in the contact power between wheel and coating material of spray. In this paper, electric model is presented in the AT feeding method. In case of rails coated, electric model is presented. Also, standard resistance of the ceramic is demonstrated by contact power between wheel and coating material of spray.

A theoritical study on spin coating technique

  • Tyona, M.D.
    • Advances in materials Research
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    • v.2 no.4
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    • pp.195-208
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    • 2013
  • A comprehensive theory of the spin coating technique has been reviewed and the basic principles and parameters controlling the process are clearly highlighted, which include spin speed, spin time, acceleration and fume exhaust. The process generally involves four stages: a dispense stage, substrate acceleration stage, a stage of substrate spinning at a constant rate and fluid viscous forces dominate fluid thinning behaviour and a stage of substrate spinning at a constant rate and solvent evaporation dominates the coating thinning behaviour. The study also considered some common thin film defects associated with this technique, which include comet, striation, chucks marks environmental sensitivity and edge effect and possible remedies.