• Title/Summary/Keyword: Coating defects

검색결과 202건 처리시간 0.025초

Improvement of osteogenic potential of biphasic calcium phosphate bone substitute coated with two concentrations of expressed recombinant human bone morphogenetic protein 2

  • Choi, Hyun-Min;Park, No-Je;Jamiyandorj, Otgonbold;Choi, Kyung-Hee;Hong, Min-Ho;Oh, Seung-Han;Park, Young-Bum;Kim, Sung-Tae
    • Journal of Periodontal and Implant Science
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    • 제42권4호
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    • pp.119-126
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    • 2012
  • Purpose: The aim of this study was to determine whether biphasic calcium phosphate (BCP) bone substitute with two different concentrations of Escherichia coli-expressed recombinant human bone morphogenetic protein 2 (ErhBMP-2) enhances new bone formation in a standardized rabbit sinus model and to evaluate the concentration-dependent effect of ErhBMP-2. Methods: Standardized, 6-mm diameter defects were made bilaterally on the maxillary sinus of 20 male New Zealand white rabbits. Following removal of the circular bony windows and reflection of the sinus membrane, BCP bone substitute without coating (control group) was applied into one defect and BCP bone substitute coated with ErhBMP-2 (experimental group) was applied into the other defect for each rabbit. The experimental group was divided into 2 subgroups according to the concentration of ErhBMP-2 (0.05 and 0.5 mg/mL). The animals were allowed to heal for either 4 or 8 weeks and sections of the augmented sinus and surrounding bone were analyzed by microcomputed tomography and histologically. Results: Histologic analysis revealed signs of new bone formation in both the control and experimental groups with a statistically significant increase in bone formation in experimental group 1 (0.05 mg/mL ErhBMP-2 coating) after a 4-week healing period. However, no statistically significant difference was found between experimental group 1 and experimental group 2 (0.5 mg/mL ErhBMP-2 coating) in osteoinductive potential (P<0.05). Conclusions: ErhBMP-2 administered using a BCP matrix significantly enhanced osteoinductive potential in a standardized rabbit sinus model. A concentration-dependent response was not found in the present study.

The effects of Hydroxyapatite nano-coating implants on healing of surgically created circumferential gap in dogs

  • Chae, Gyung-Joon;Lim, Hyun-Chang;Choi, Jung-Yoo;Chung, Sung-Min;Lee, In-Seop;Cho, Kyoo-Sung;Kim, Chong-Kwan;Choi, Seong-Ho
    • Journal of Periodontal and Implant Science
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    • 제38권sup2호
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    • pp.373-384
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    • 2008
  • Purpose: The aim of this study is to compare the healing response of various Hydroxyapatite(HA) coated dental implants by Ion-Beam Assisted Deposition(IBAD) placed in the surgically created circumferential gap in dogs. Materials and methods: In four mongrel dogs, all mandibular premolars and the first molar were extracted. After an 8 weeks healing period, six submerged type implants were placed and the circumferential cylindrical 2mm coronal defects around the implants were made surgically with customized step drills. Groups were divided into six groups : anodized surface, anodized surface with 150nm HA and heat treatment, anodized surface with 300nm HA and heat treatment, anodized surface with 150nm HA and no heat treatment, and anodized surface with 150nm HA, heat treatment and bone graft, anodized surface with bone graft. The dogs were sacrificed following 12 weeks healing period. Specimens were analyzed histologically and histomorphometrically. Results: During the healing period, healing was uneventful and implants were well maintained. Anodized surface with HA coating and $430^{\circ}C$ heat treatment showed an improved regenerative characteristics. Most of the gaps were filled with newly regenerated bone. The implant surface was covered with bone layer as base for intensive bone formation and remodeling. In case that graft the alloplastic material to the gaps, most of the coronal gaps were filled with newly formed bone and remaining graft particles. The bone-implant contact and bone density parameters showed similar results with the histological findings. The bone graft group presented the best bone-implant contact value which had statistical significance. Conclusion: Within the scope of this study, nano-scale HA coated dental implants appeared to have significant effect on the development of new bone formation. And additional bone graft is an effective method in overcoming the gaps around the implants.

안경 렌즈의 국소적 투과율 측정을 위한 방법에 관한 연구 (A Study on the Method for the Local Transmittance Measurements of the Ocular Lens)

  • 박상국;이형철;육도진;성덕용;강성수
    • 한국안광학회지
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    • 제19권4호
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    • pp.471-477
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    • 2014
  • 목적: 국소 투과율 현미경을 이용하여 안경렌즈의 투과율 분포를 분석함으로써 렌즈의 광학적 균질성을 연구하고자 한다. 방법: 안경렌즈 표면에 집광된 레이저의 투과율을 광검출기와 락인앰프로 측정하고 그 결과를 분석하였다. 코팅되지 않은 렌즈와 멀티 코팅이 된 렌즈 그리고 누진렌즈가 시료로서 분석되었다. 결과: 누진렌즈와 물리적 자극이 가해진 렌즈의 측정 결과에서 국소 투과율 현미경 분석 결과가 광학 현미경을 통한 측정 결과와 높은 일치도를 보였다. 또한 광학적 결함이 있는 곳에서 투과율의 평균값은 감소하고 표준편차는 증가하였다. 자극이 가해지지 않은 렌즈에서는 반사방지 코팅의 유무가 투과율에 큰 영향을 미치는 것을 국소 투과율 현미경과 일반적 투과율 분석 모두에서 공통적으로 분석되었다. 결론: 시료에 다양한 자극이 가해졌을 때 투과율의 분포에 변화가 생김을 국소 투과율 현미경을 통해 확인하였다. 국소 투과율 현미경을 통한 이러한 분석은 렌즈 혹은 코팅막의 균일도를 평가 혹은 확인할 수 있는 하나의 방법으로 활용될 수 있다.

토양 특성 및 전기방식에 따른 연료 가스용 강관의 부식 차이에 관한 연구 (A Study on the Corrosivity according to Soil Characteristics and Electrolytic Protection for the Materials of Fuel Gas Pipe)

  • 임상식;김지선;류영돈;이진한
    • 한국가스학회지
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    • 제20권6호
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    • pp.16-22
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    • 2016
  • 연료가스용 탄소강관이 지하에 매설되는 경우 부식을 방지하기 위해 피복강관을 사용하고 있으며, 피복강관의 결함, 타공사, 시공시 피복의 손상에 대비하여, 방식전위를 이용하여 환원 분위기를 강제로 조성한다. 일반적으로 연료가스용 탄소강관이 지하에 매설된 경우 두 방법이 병행되어 사용되지만, 토양환경의 변화를 예측 할 수 없는 불확실성과 부식 정도 또는 피복의 손상 등 배관의 결함에 대해 육안으로 직접 관찰하기 어려운 문제가 공존한다. 매설배관의 부식이 발생하는 것을 직접적으로 관찰하기 어렵기 때문에, 이를 직접적으로 관찰하기 위한 방법 중 하나가 부식쿠폰을 이용한 방법이다. 본 연구에서는 3가지 토양(마사토, 진흙, 모래)과 방식전위 사용 여부에 따라 작성된 6가지의 시나리오를 토대로 약 1년간 부식쿠폰의 부식 정도를 파악하였다. 그 결과 방식전위가 흐르는 환경의 부식쿠폰은 부식이 전혀 발생하지 않았으며, 미방식 부식쿠폰은 모두 부식이 발생하였다. 토양에 따라서는 진흙에서 가장 적은 부식속도를 보였으며, 모래와 마사토는 유사한 경향을 갖는 것으로 확인되었다. 진흙의 경우 높은 함수량에 의해 국부부식이 발생하였으며, 모래에서 부식이 발생한 것은 모래에 함유된 화학적 성분에 기인한 것으로 확인되었다.

Using the Dorsal Metacarpal Artery Perforator Flap for Reconstruction of Rheumatoid Ulcers

  • Choi, Min;Son, Kyung Min;Choi, Woo Young;Cheon, Ji Seon;Yang, Jeong Yeol
    • Archives of Reconstructive Microsurgery
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    • 제24권2호
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    • pp.79-81
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    • 2015
  • Rheumatoid arthritis is a long lasting autoimmune disorder that primarily affects joints, and patients with rheumatoid arthritis are predisposed to development of chronic skin ulcers. In addition, skin ulcers with rheumatoid arthritis tend to persist despite treatment because of sustained inflammation and poor healing capacity. Treatment of skin ulcers involves medications, wound coating agents, and surgical procedures including skin grafting, however, wound dressing or skin grafts are generally excluded because of excessive cost and time and poor intake rate. The dorsal metacarpal artery perforator (DMAP) flap, a vascular island flap for coverage of soft tissue defects on the fingers, provides promising results including matched quality and color. We experienced a case of DMAP flap for reconstruction of a rheumatoid ulcer, and a DMAP flap may be considered as a good faithful option for treatment of patients with rheumatoid ulcer.

반응석출법에 의해 피복된 TiC의 경화거동에 관한 연구 (A study on the hardening characterstics of the TiC layer formed by the reactive deposition technique)

  • 남기석;변응선;이구현;김도훈
    • 열처리공학회지
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    • 제7권4호
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    • pp.288-297
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    • 1994
  • In this study, lattice parameter, binding energy and microstructures of TiC layer according to the addition of Fe, Cr were investigated in the reactive deposition coating. From the results, the lattice parameters of the TiC layers by using ferro-titanium as a precursor were 4.329~4.339A but the lattice parameters of the TiC layers formed by ferro-titanium and ferro-chromium decreased to 4.316~4.330A. The hardness of the former's was HV(100g) 3,000~3,400kg/mm and the hardness of the latter's was HV (100g) 3,800~3,900. But, regardless of Cr and Fe, the binding energy of TiC layers were 454.75 eV for $Ti2p_{3/2}$ and were 281.85 eV for Cls. Meanwhile, the TiC layers were densified by addition of Fe, Cr and internal defects were reduced Therefore. it can be concluded that the remarkable hardness increment was obtained by the improvement of microstructures of TiC rather than the increase of bond strength or Peierls stress.

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Effect of Power Mode of Plasma Anodization on the Properties of formed Oxide Films on AZ91D Magnesium Alloy

  • Lee, Sung-Hyung;Yashiro, Hitoshi;Kure-Chu, Song-Zhu
    • 한국재료학회지
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    • 제28권10호
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    • pp.544-550
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    • 2018
  • The passivation of AZ91D Mg alloys by plasma anodization requires deliberate choice of process parameters due to the presence of large amounts of structural defects. We study the dependence of pore formation, surface roughness and corrosion resistance on voltage by comparing the direct current (DC) mode and the pulse wave (pulse) mode in which anodization is performed. In the DC plasma anodization mode, the thickness of the electrolytic oxide film of the AZ91D alloy is uneven. In the pulse mode, the thickness is relatively uniform and the formed thin film has a three-layer structure. The pulse mode creates less roughness, uniform thickness and improved corrosion resistance. Thus, the change of power mode from DC to pulse at 150 V decreases the surface roughness (Ra) from $0.9{\mu}m$ to $0.1{\mu}m$ and increases the corrosion resistance in rating number (RN) from 5 to 9.5. Our study shows that an optimal oxide film can be obtained with a pulse voltage of 150 V, which produces an excellent coating on the AZ91D casting alloy.

파이로포스포릭 락톤 변성 폴리에스터를 함유한 폴리우레탄 도료의 물성 및 난연 효과 (Physical Properties and Flame-Retardant Effects of Polyurethane Coatings Containing Pyrophosphoric Lactone Modified Polyesters)

  • 정동진;김성래;박형진;박홍수;김승진
    • 폴리머
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    • 제27권3호
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    • pp.169-175
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    • 2003
  • 무독성의 반응형 난연 도료를 제조할 목적으로 모체수지 1개의 구조단위 속에 2개의 인산기를 보유한 파이로포스포릭 락톤 변성 폴리에스터 (PATT)를 합성하고, PATT에 이소시아네이트인 toluene diisocyanate-isocyanurate를 상온경화시켜 2성분계 폴리우레탄 난연 도료(PIPUC)를 제조하였다. PIPUC로서 도막제작 후 비난연 도료와의 도막물성을 비교한 결과 난연 성분 도입에 따른 난연 도료의 물성이 저하되지 않음을 알았다. 난연성 시험 중 45$^{\circ}$ Meckel burner 법에서는 탄화길이가 3.1~4.4 cm를, LOI법에서는 LOI 27~30%를 각각 나타냄으로써 양호한 난연 효과를 보여주었고, SEM에 의한 표면 도막을 관찰한 결과 도막의 결함이나 상분리 현상이 생기지 않음을 관찰하였다.

고강도콘크리트에서 폴리머 시멘트 슬러리 도장철근의 인발부착특성 (Pull-Out Bond Properties of Polymer Cement Coated Rebars in HSC)

  • 김민호;김완기;소양섭
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2002년도 봄 학술발표회 논문집
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    • pp.215-220
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    • 2002
  • Epoxy-coated re-bar was partly used to the structures and put to practical use, but were not economical and appeared to have defects such as the diminishing of long term bond strength between concrete. The study of polymer cement slurry coated re-bar was started in order to complement the defect of epoxy coated re-bar, and ever since the basic properties appeared to be excellent. But, study of bond properties embedded in concrete specimens was insufficient until now. This study attempts to examine the possibility of improving the bond strength of polymer cement slurry coated re-bar between concrete specimens in accordance with ACI Code and KS Code through pull-out test of 150mm$\times$150mm$\times$150mm substrates with polymer cement slurry coated re-bar having polymer cement ratios of 50%, 75% and 100%, coating thickness 250${\mu}{\textrm}{m}$, 450 ${\mu}{\textrm}{m}$ and with curing ages of 3, 7 and 28 days. High strength concrete was designed having a compressive strength of 500kgf/cm2 as specified. Practical bond length ranges of 55 and 85mm were applied to each of specimen. The bond strength of polymer cement slurry coated re-bar using St/BA-1 and St/BA-2 was compared to that of plain re-bar. The results of this study showed that the bond strength of 55mm bond length was much higher than that of 85mm bond length.

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산처리에 의해 개질된 리튬이온 이차전지용 흑연 전극의 특성 (Performance of Graphite Electrode Modified with Acid Treatment for Lithium Ion Secondary Battery)

  • 김명수;문승환;김문걸;김택래;함현식;박홍수
    • 한국응용과학기술학회지
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    • 제22권2호
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    • pp.142-150
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    • 2005
  • The natural graphite particles A and heat-treated graphite particles B at $1800\;^{\circ}C$ after pitch-coating were used as the anode base materials for lithium ion secondary battery. In order to improve the performance of anode materials, the base anode materials were treated with various acids. With the acid treatments of 62% $HNO_3$ and 95% $H_2SO_4$ aqueous solution, the specific surface area and electrical conductivity of base anode materials were increased, and the initial charge-discharge capacity and cycle performance were improved due to the elimination of structural defects.