• Title/Summary/Keyword: Characterisation

Search Result 122, Processing Time 0.025 seconds

EBSD Microstructural Characterisation of Oxide Scale on Low Carbon Steel

  • Birosca, S.;De Cooman, B.C.
    • Corrosion Science and Technology
    • /
    • v.7 no.3
    • /
    • pp.182-186
    • /
    • 2008
  • The microstructures of the oxide scale developed at high temperature on steels are very complex and their development depends on many factors including time, temperature, oxidation conditions and alloying elements. The classical model of an oxide scale on steel consisting of wüstite, magnetite and haematite layers, is more complicated in reality and its properties change with the factors that affect their development. An understanding of the oxide scale formation and its properties can only be achieved by careful examination of the scale microstructure. The oxide scale microstructure may be difficult to characterise by conventional techniques such as optical or standard scanning electron microscopy. An unambiguous characterisation of the scale and the correct identification of the phases within the scale are difficult unless the crystallographic structure for each phase in the scale is considered and a simultaneous microstructure-microtexture analysis is carried out. In the current study Electron Backscatter Diffraction (EBSD) has been used to investigate the microstructure of iron oxide layers grown on low carbon steels at different times and temperatures. EBSD has proved to be a powerful technique for identifying the individual phases in the oxide scale accurately. The results show that different grain shapes and sizes develop for each phase in the scale depending on time and temperature.

Wind induced response of an elevated steel water tank

  • Sepe, Vincenzo;Zingali, Antonino E.
    • Wind and Structures
    • /
    • v.4 no.5
    • /
    • pp.383-398
    • /
    • 2001
  • The paper describes the results of the monitoring of an elevated steel water-tank with unusual shape, 85 m high and 40 m wide. The research was carried out analysing both the static and dynamic behaviour under wind actions. The instruments used (some of which were employed for the first time for this project) are described and the data processing procedures are discussed. Comparison between the experimental results and those obtained through a numerical model gives interesting information both on the structural behaviour and on the characterisation of wind actions.

Study on the Fabric Drape Behaviour with Image Analysis - Measurement, Characterisation and Instability -

  • Jeong, Y.J.;Phillips, D.G.
    • Proceedings of the Korean Fiber Society Conference
    • /
    • 1998.10a
    • /
    • pp.290-294
    • /
    • 1998
  • Colour tone, lustre, surface roughness of fabrics are very important factors in pursue of the beauty of external appearance, namely aesthetic appearance, and the dynamic functionality of fabric used to clothe the human body. Drape is one of many factors that influence the aesthetic appearance of fabric and has an outstanding effect on the formal beauty of fabric. For this reason, the measurement and understanding of drape is required to specify the performance of fabric used in clothing. (omitted)

  • PDF

Site Selection Process for Spent Fuel in Finland

  • Auvinen, Anssi;Lehtonen, Aleksis;Riekkola, Reijo
    • Proceedings of the Korean Radioactive Waste Society Conference
    • /
    • 2009.06a
    • /
    • pp.179-181
    • /
    • 2009
  • This presentation is a short summary of the Finnish process for selection and characterisation of potential sites for geological deep disposal of spent nuclear fuel. The process lasted nearly two decades from 1983 to 2000, and was concluded by the Government's Decision in Principle (DiP) on the construction of a repository in Olkiluoto. This presentation gives an outline of the early site selection criteria and a description of this process.

  • PDF

Characterisation of Some Silica Samples Modified with Aluminium by Inverse Liquid Chromatography using Squalene as Probe - Part IV

  • Zhang Zhentao;Balard Henri;Donnet J. B.
    • Proceedings of the Korean Radioactive Waste Society Conference
    • /
    • 2005.11b
    • /
    • pp.107-116
    • /
    • 2005
  • Precipitated silicas modified by aluminium were characterised using inverse liquid chromatography in anhydrous heptane with squalene as probes. Their monolayer capacities of adsorption, Langmuir's and Henry's constants were determined from the desorption isotherms according to frontal analysis. A narrow band consisting of isotherms was observed. The introduction of aluminium has little influence on the monolayer capacity, Langmuir's constants and the Henry constant. Experimental data show that neither the amounts of aluminium on the silica nor the methods of the introduction of aluminium into the silica influence the interactions between the squalene and the silicas.

  • PDF

THE CHARACTERISATION OF BMO VIA COMMUTATORS IN VARIABLE LEBESGUE SPACES ON STRATIFIED GROUPS

  • Liu, Dongli;Tan, Jian;Zhao, Jiman
    • Bulletin of the Korean Mathematical Society
    • /
    • v.59 no.3
    • /
    • pp.547-566
    • /
    • 2022
  • Let T be a bilinear Calderón-Zygmund operator, $b{\in}U_q>_1L^q_{loc}(G)$. We firstly obtain a constructive proof of the weak factorisation of Hardy spaces. Then we establish the characterization of BMO spaces by the boundedness of the commutator [b, T]j in variable Lebesgue spaces.

A CLASS OF STRUCTURED FRAMES IN FINITE DIMENSIONAL HILBERT SPACES

  • Thomas, Jineesh;Namboothiri, N.M. Madhavan;Nambudiri, T.C. Easwaran
    • The Pure and Applied Mathematics
    • /
    • v.29 no.4
    • /
    • pp.321-334
    • /
    • 2022
  • We introduce a special class of structured frames having single generators in finite dimensional Hilbert spaces. We call them as pseudo B-Gabor like frames and present a characterisation of the frame operators associated with these frames. The concept of Gabor semi-frames is also introduced and some significant properties of the associated semi-frame operators are discussed.

Genetic characterization of microsporidians infecting Indian non-mulberry silkworms (Antheraea assamensis and Samia cynthia ricini) by using PCR based ISSR and RAPD markers assay

  • Hassan, Wazid;Nath, B. Surendra
    • International Journal of Industrial Entomology and Biomaterials
    • /
    • v.30 no.1
    • /
    • pp.6-16
    • /
    • 2015
  • This study established the genetic characterisation of 10 microsporidian isolates infecting non-mulberry silkworms (Antheraea assamensis and Samia cynthia ricini) collected from biogeographical forest locations in the State of Assam, India, using PCR-based markers assays: inter simple sequence repeat (ISSR) and random amplified polymorphic DNA (RAPD). A Nosema type species (NIK-1s_mys) was used as control for comparison. The shape of mature microsporidian spores were observed oval to elongated, measuring 3.80 to $4.90{\mu}m$ in length and 2.60 to $3.05{\mu}m$ in width. Fourteen ISSR primers generated reproducible profiles and yielded 178 fragments, of which 175 were polymorphic (98%), while 16 RAPD primers generated reproducible profiles with 198 amplified fragments displaying 95% of polymorphism. Estimation of genetic distance coefficients based on dice coefficients method and clustering with un-weighted pair group method using arithmetic average (UPGMA) analysis was done to unravel the genetic diversity of microsporidians infecting Indian muga and eri silkworm. The similarity coefficients varied from 0.385 to 0.941 in ISSR and 0.083 to 0.938 in RAPD data. UPGMA analysis generated dendrograms with two microsporidian groups, which appear to be different from each other. Based on Euclidean distance matrix method, 2-dimensional distribution also revealed considerable variability among different identified microsporidians. Clustering of these microsporidian isolates was in accordance with their host and biogeographic origin. Both techniques represent a useful and efficient tool for taxonomical grouping as well as for phylogenetic classification of different microsporidians in general and genotyping of these pathogens in particular.

Characterisation and Co-pyrolytic Degradation of the Sawdust and Waste Tyre Blends to Study the Effect of Temperature on the Yield of the Products

  • Shazali, Erna Rashidah Hj;Morni, Nurul Afiqah Haji;Bakar, Muhammad Saifullah Abu;Ahmed, Ashfaq;Azad, Abul K;Phusunti, Neeranuch;Park, Young-Kwon
    • Applied Chemistry for Engineering
    • /
    • v.32 no.2
    • /
    • pp.205-213
    • /
    • 2021
  • The present study aimed to determine the effect of co-pyrolysis of sawdust biomass and scrap tyre waste employing different blending ratios of sawdust to waste tyre such as 100:0, 75:25, 50:50, 25:75, and 0:100. The thermochemical characterization of feedstocks was carried out by employing the proximate, ultimate analysis, and thermogravimetric (TGA) analyses, calorific values, and scanning electron microscope coupled with energy dispersive x-ray analysis (SEM-EDX) to select the blending ratio having better bioenergy potential amongst the studied ratios. The blending ratio of 25:75 (sawdust to waste tyre) was selected for the co-pyrolysis study in a fixed-bed pyrolysis reactor system based on its solid biofuels properties such as heating value (30.18 MJ/kg), and carbon (71.81 wt%) and volatile matter (63.82 wt%) contents. The pyrolysis temperatures were varied as 500, 600 and 700 ℃ while the other parameters such as heating rate and nitrogen flowrate were maintained at 30 ℃/min and 0.5 L/min respectively. The bio-oil yields as 31.9, 47.1 and 61.2 wt%, bio-char yields as 34.5, 34.2 and 31.4 wt% and gaseous product yields as 33.6, 18.60 and 7.3 wt% at the pyrolysis temperatures of 500, 600 and 700 ℃ respectively were obtained. The blends of sawdust and waste tyres showed the improved energy characteristics which could provide the solution for the beneficial management of sawdust and scrape tyre wastes via co-pyrolysis processing.

Morphometric Characterisation of Root-Knot Nematode Populations from Three Regions in Ghana

  • Nyaku, Seloame Tatu;Lutuf, Hanif;Cornelius, Eric
    • The Plant Pathology Journal
    • /
    • v.34 no.6
    • /
    • pp.544-554
    • /
    • 2018
  • Tomato (Solanum lycopersicum) production in Ghana is limited by the root-knot nematode (Meloidogyne incognita, and yield losses over 70% have been experienced in farmer fields. Major management strategies of the root-knot nematode (RKN), such as rotation and nematicide application, and crop rotation are either little efficient and harmful to environments, with high control cost, respectively. Therefore, this study aims to examine morphometric variations of RKN populations in Ghana, using principal component analysis (PCA), of which the information can be utilized for the development of tomato cultivars resistant to RKN. Ninety (90) second-stage juveniles (J2) and 16 adult males of M. incognita were morphometrically characterized. Six and five morphometric variables were measured for adult males and second-stage juveniles (J2) respectively. Morphological measurements showed differences among the adult males and second-stage juveniles (J2). A plot of PC1 and PC2 for M. incognita male populations showed clustering into three main groups. Populations from Asuosu and Afrancho (Group I) were more closely related compared to populations from Tuobodom and Vea (Group II). There was however a single nematode from Afrancho (AF4) that fell into Group III. Biplots for male populations indicate, body length, DEGO, greatest body width, and gubernaculum length serving as variables distinguishing Group 1 and Group 2 populations. These same groupings from the PCA were reflected in the dendogram generated using Agglomerative Hierarchical Clustering (AHC). This study provides the first report on morphometric characterisation of M. incognita male and juvenile populations in Ghana showing significant morphological variation.