• 한국세라믹학회지
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• 제43권4호
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• pp.199-202
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• 2006

In this study, SiC whiskers were grown on a porous SiC diesel particulate filter for nanoparticle filtering. To grow the whiskers at the inner pore without closing the pores, we used chemical vapor infiltration with a solution source and a dilute. As the deposition time increased, the whiskers grew and formed a network structure. After 180 min of deposition, the mean diameter of the whiskers was 174 nm and the compressive strength was 58.4 MPa. The pores shrank from $10{\mu}m\;to\;0.4{\mu}m$ and, because the whiskers filed the inner pores, the gradient of permeability decreased as the deposition time increased. However, by using the network structure of whiskers deposited for 120 min and 180 min, we obtained a diesel particulate filter with pores of $0.98{\mu}m\;and\;0.4{\mu}m$, respectively. Furthermore, the filter shows better permeability than a porous body with pores of $1{\mu}m$. In short, by filtering the nanoparticulate materials, the network structure of whiskers improves the strength, reduces the pore size and minimizes the permeability drop.

• 한국세라믹학회지
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• 제55권3호
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• pp.285-289
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• 2018

We synthesized silicon carbide (${\beta}-SiC$) nanowires with nano-scale diameter (30 - 400 nm) and micro-scale length ($50-200{\mu}m$) on a porous body using low-grade silica and carbon black powder by carbothermal reduction at $1300-1600^{\circ}C$. The SiC nanowires were formed by vapor-liquid-solid deposition with self-evaporated Fe catalysts in low-grade silica. We investigated the characteristics of the SiC nanowires, which were grown on a porous body with Ar flowing in a vacuum furnace. Their structural, optical, and electrical properties were analyzed with X-ray diffraction (XRD), transmission electron microscopy (TEM), and selective area electron diffraction (SAED). We obtained high-quality SiC single crystalline nanowire without stacking faults that may have uses in industrial applications.

• 한국세라믹학회지
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• 제29권12호
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• pp.981-989
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• 1992

This is a study on the effects of cristobalite transition of quartz in semi-vitrious whiteware body, as addition of alkali and alkali earth oxides, prepared by pottery stone, feldspar, kaolin and clay minerals. The amounts of ${\alpha}$-quartz to ${\alpha}$-cristobalite transition, F.O.C. (fraction of cristobalite), were increased with firing temperature. In MgO added body, ${\alpha}$-quartz was decreased and the formation of cristobalite was increased. Effects of K2O addition was remarkably decreased the formation of cristobalite. Additive effects of MgO and K2O were confirmed that it was very different to variation of transition temperature of metakaolinite to Si-Al spinel structure in thermal reaction of kaolinite minerals. Result CaO addition was ineffective to transition temperature, and the transition temperature in Na2O added body was decreased, but relative intensity of quartz and cristobalite crystal in XRD results was decreased. This was characterized by the effects on the formation of liquid phase much more.

• 한국세라믹학회지
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• 제16권2호
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• pp.77-82
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• 1979

Diopside-Anorthite body was easily synthesized at relatively low temperature 1225℃, compared with the synthesizing temperature 1425℃ of Anorthite. Of Diopside-Anorthite body, the synthesizing temperature was considered to be higher than 1225℃ because Gehlenite, probably formed at 1220℃, was detected by X-ray diffraction. This body has excellent physical and electrical properties, i.e. electric resistivity (1.2×1014Ωcm), low dielectric constant (6.26) and low thermal expansion coeffcient (61.9×10-7/℃). It's hardness was good enough for electrical subsidiary. In addition, this body, Diopside-Anorthite, has exellent properties for heat resisting wares.

• 한국세라믹학회지
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• 제34권5호
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• pp.528-534
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• 1997

There have been many studies on the preparation of slip, forming and drying in the slip casting process. However, is has not been yet on the rheological properties of consolidated body which largely affect on the workability. It was investugated that the rheological properties of the consolidated bodies formed by slip casting in the form of cakes from well dispersed(slip C) and weakly agglomerated slip(slip B) in the clay and clay-fly ash systems. The state of dispersion of slip was found to affected the critical moisture content which was largely affected by the pore and moisture distribution of the consolidated body. The cake C show lower critical moisture content than cake B in the clay system. However, the cake B gives lower critical moisture content than cake C in the clay-fly ash system.

• 한국세라믹학회지
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• 제47권4호
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• pp.296-301
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• 2010

The objective of the present research is to develop the body for Temmoku Teabowl, in order to manufacture the Temmoku Teabowl with the characteristics of Jian Ware, which has a rich dark brown color and has been extolled as the representative fine article of Temmoku Teabowl. Basic composition was first determined using domestically produced clay, kaolin and pottery stone as starting materials. After the addition of calcinated Hwangto, which is rich in iron, the mixture was subjected either to oxidizing calcination at $1260^{\circ}C$ to produce a body with a color suitable for Hanam ware or to reducing calcination at $1230^{\circ}C$ to produce a body with a color suitable for Jian Ware. The bodies produced in this research showed the strength value of $380{\sim}36\;Kg/cm^2$, the specific gravity of 2.304~2.310, the absorption ratio of 4.103~3.897, and the porosity of 8.608~8.207%.

• 한국세라믹학회지
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• 제12권3호
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• pp.3-7
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• 1975

The usefulness of the domestic shale contained chiastolite as additive were investigated. Crude mixed minerals were separated into shale and chiastolite. Refractory body added simple component or multiple components as additives was obtained when firing at 125$0^{\circ}C$ for each body. Compressive strength, refractories, apparent sp. gr., water absorption, corrosion test by slag, hot linear expansion were measured and X-ray diffraction analysis was observed. As the result of study, refractory body contained separated minerals as additives showed slightly increasing in refractoriness, lowering in sintering effect, the excellent effect for corrosion resistance by acidic slag. With more containing separated minerals, hot linear expansion for the body can be decreased.

• 한국세라믹학회지
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• 제26권2호
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• pp.171-178
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• 1989

In order to develope hydroxyapatite ceramics which has mechanical strength as bio-implant materials and get the basic data for the study and application of biocompatibility, hydroxyapatite was synthesized at Ca/P=1.67~1.75, pH 7~11 by precipitation method. Using prepared powders, the sintered body, fluorine substituted body and the porous body was formed and their properties were investigated. The sample obtained in condition of Ca/P=1.67, pH 7 and sintering at 1,15$0^{\circ}C$ was decomposed to $\beta$-tricalcium phosphate, and co-existed with hydroxyapatite. Hydroxyapatite synthesized at pH 11 was not easily decomposed to $\beta$-tricalcium phosphate at sintering process. The substitution of a small amount of fluorine for hydroxyapatite prevented hydroxyapatite from being decompsed to $\beta$-tricalcium phosphate. Hydroxyapatite ceramics which substited of 10% fluorine was prepared at 1,15$0^{\circ}C$, and the valueof bending strength for this body were found to be 112MPa.

• 한국전기전자재료학회논문지
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• 제28권1호
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• pp.1-6
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• 2015

Generating output characteristics of a ${\pi}$-type piezoelectric harvester depending on size of the ceramic and the elastic body were studied. The ${\pi}$-type piezoelectric harvester consists of a rectangular piezoelectric ceramic and a ${\pi}$ shaped elastic body. If the tensions is applied at both ends of an elastic body legs, the piezoelectric effect occurs at the ceramics through the form change of the elastic body. The structure of this ${\pi}$-type harvester can be used in a various area than an existing type generator, because it prevent from direct pressure to the ceramic. Generating characteristics of the harvester were analyzed by using finite element method program. The piezoelectric harvester was fabricated on the basis of analyzed results and attached on a frequency controllable vibrator to measure the output characteristics. And generating characteristics were defined by comparing analysis results and experimental results. The highest output voltage was obtained when the ceramic length, thickness were 20 mm, 0.5 mm in the analysis result. And experiment was performed by analysis results at low frequency region, output voltage was generated about 6 V.

• 한국세라믹학회지
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• 제36권2호
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• pp.178-185
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• 1999

Si3N4 겔캐스팅공정 제어를 위하여, 슬립 조성의 영향이 슬립의 점성특성과 성형체의 기계적 특성 및 소결체의 밀도에 미치는 영향에 대하여 조사하였다. 아크릴아마이드 모노머, 고분자전해질, 그리고 질화규소의 혼합물을 어트리터에 예비혼합한 후 볼밀링하여 슬립을 제조하였다. 개시제가 혼합된 슬립을 진공탈포하고 몰드에 주입하고 중합을 진행하였으며, 겔화된 슬립을 건조하여 성형체를 얻었다. 슬립의 특성과 성형체의 기계적 특성을 평가하기 위해, 슬립의 점도 측정과 직경방향 압축시험을 행하였다. 그 결과, near net shaping을 위한 낮은 점도를 갖는 46 vol%의 고농도 질화규소 슬립의 제조가 가능하였다. 성형체가 기계적 특성은 주로 모노머의 농도에 비례하여 증가하였다. 또한, 겔캐스트 성형체의 인장강도가 약 3MPa이 넘으면 기계적 가공이 가능하였으며, 겔캐스팅 성형체를 176$0^{\circ}C$, 3시간 상압소결하여 약 98.5%의 상대밀도를 얻을 수 있었다.