• 한국정밀공학회지
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• 제22권10호
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• pp.121-128
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• 2005

The research on electromagnetic shielding has been advanced for military applications as well as for commercial products. Utilizing the reflective properties and absorptive properties of shielding material, the replied signal measured at the rear surface or at the signal source can be minimized. The shielding effect was obtained from materials having special absorptive properties and structural characteristics such as stacking sequence. Recently researchers studied the electromagnetic properties of nano size particles. In this research {glass fiber}/{epoxy}/{nano particle} composites(GFR-Nano composites) was fabricated using various nano particles, and their properties in electromagnetic shielding were compared. For the visual observation of the nano composite materials, SEM(Scanning Electron Microscope) and TEM(Transmission Electron Microscope) were used. For the measurement of electromagnetic shielding, HP8719ES S-parameter Vector Network Analyser System was used on the frequency range of 8 GHz${\~}$12GHz. Among the nano particles, carbon black and Multi-Walled Carbon Nano-Tube (MWCNT) revealed outstanding electromagnetic shielding. Although silver nano particles (flake and powder) were expected to have effective electromagnetic shielding due to their excellent electric conductivities, test results showed little shielding characteristics.

• Transactions on Electrical and Electronic Materials
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• 제14권4호
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• pp.165-171
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• 2013

Nanostructured pure a-C and nitrogen doped a-C: N thin films with small particle size of, ~50 nm were obtained by Aerosol-assisted CVD method from the natural precursor camphor oil. Five samples were prepared for the a-C and a-C: N respectively, with the deposition temperatures ranging from $400^{\circ}C$ to $600^{\circ}C$. At high temperature, the AFM clarifies an even smoother image, due to the increase of the energetic carbon ion bombardment at the surface of the thin film. An ohmic contact was acquired from the current-voltage solar simulator characterization. The higher conductivity of a-C: N, of ${\sim}{\times}10^{-2}Scm^{-1}$ is due to the decrease in defects since the spin density gap decrease with the nitrogen addition. Pure a-C exhibit absorption coefficient, ${\alpha}$ of $10^4cm^{-1}$, whereas for a-C:N, ${\alpha}$ is of $10^5cm^{-1}$. The high ${\sigma}$ value of a-C:N is due to the presence of more graphitic component ($sp^2$ carbon bonding) in the carbon films.

• Carbon letters
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• 제22권
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• pp.48-59
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• 2017

This study synthesized pure anatase carbon doped $TiO_2$ photocatalysts supported on a stainless steel mesh using a sol-gel solution of 8% polyacrylonitrile (PAN)/dimethylformamide (DMF)/$TiCl_4$. The influence of the pyrolysis temperature and holding time on the morphological characteristics, particle sizes and surface area of the prepared catalyst was investigated. The prepared catalysts were characterized by several analytical methods: high resolution scanning electron microscopy (HRSEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), Brunauer-Emmett-Teller (BET), and X-ray photoelectron spectroscopy (XPS). The XRD patterns showed that the supported $TiO_2$ nanocrystals are typically anatase, polycrystalline and body-centered tetragonal in structure. The EDS and XPS results complemented one another and confirmed the presence of carbon species in or on the $TiO_2$ layer, and the XPS data suggested the substitution of titanium in $TiO_2$ by carbon. Instead of using calcination, PAN pyrolysis was used to control the carbon content, and the mesoporosity was tailored by the applied temperature. The supported $TiO_2$ nanocrystals prepared by pyrolysis at 300, 350, and $400^{\circ}C$ for 3 h on a stainless steel mesh were actual supported carbon doped $TiO_2$ nanocrystals. Thus, $PAN/DMF/TiCl_4$ offers a facile, robust sol-gel related route for preparing supported carbon doped $TiO_2$ nanocomposites.

• 한국자기학회지
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• 제15권3호
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• pp.172-176
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• 2005

화학기상응축법(CVC)에 의한 제조된 네 개의 나노-Fe 입자 시료들이 뫼스바우어, XRD, BET와 TEM에 의하여 조사되었다. 네 개의 시료들은 고순도 이송가스와 분해온도에 의해 구성이 되었다. 각 시료를 구성하고 있는 입자들은 2 또는 3층구조로 형성되었음을 TEM분석으로 알 수 있었다. 평균입도의 경우에는 분해온도에 정비례하는 특성을 보여 주었다. 분해온도가 $500^{\circ}C$일 경우에, 이송가스를 CO로 사용하게 되면 $Fe_3C$의 형성이 $CH_4$보다 용이한 것으로 나타났다. 그러나 $1,100^{\circ}C$의 경우에는, CO와 $CH_4$모두에서 $Fe_3C$의 형성이 대부분을 차지하고 있는 것으로 나타났다.

• Composites Research
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• 제23권6호
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• pp.1-6
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• 2010

복합재 항공기 동체의 낙뢰손상방지를 목적으로 탄소섬듐-주석 산화물(ITO) 나노입자를 코팅함으로써 탄소섬유강화플라스틱(CFRP) 복합재료의 전기전도도를 향상하였다. 탄소섬유에 코팅된 ITO 나노입자는 10~40%의 농도로 콜로이드 상태에서 분사되었다. CFRP의 전기전도도는 코팅 후 3배 이상 증가하였으며 현재 B-787 복합재 항공기 동체에 사용 중인 기술인 금속메쉬를 CFRP 외층에 매몰한 경우보다도 높은 전기전도도를 얻을 수 있었으며, 나노입자 코팅으로 섬유-기지 계면에 미지는 악영향은 발견되지 않았다. 모의 낙뢰에 의한 손상영역은 각각 다른 처리를 한 재료와 조건에 따라 초음파 C-scan 이미지로 확인하였다. ITO 40% 코팅 시편의 경우 전기전도도는 B-787 샘플의 경우보다 높았지만 낙뢰에 의한 손상영역의 크기는 거의 비슷한 수준이었다.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 2004년도 추계학술발표회 발표논문집
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• pp.1047-1048
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• 2004

Simulation Coated layers of a nuclear fuel particle were evaluated by field emission scanning electron microscopy and nano-indentation method to give basic data to estimate 'Amoeba effect' and give an optimum fabrication condition and high quality control. Coated layers on the fuel kernel are in the order of buffer pyrolytic carbon, inner pyrolytic carbon, silicon carbide and outer pyrolytic carbon layers, which average thicknesses are 95, 25, 30 and 28 ${\mu}m$, respectively. Their densities and hardnesses are 1.08, 1.15, 3.18, 1.82 $g/cm^3$ and 0.522, 0.874, 9.641, and 2.726 GPa, respectively. Comparing theoretical density of pyrolytic carbon of 2.22 $g/cm^3$, the relative amount of porosity in each layer is about 52% for buffer, 48% for inner PyC and 18% for outer PyC.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2007년도 춘계학술대회
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• pp.200-203
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• 2007

Parametric investigation of the polyol process for the preparation of carbon supported Pt nano particles as catalysts for fuel cells was carried out. It was found that the concentration of glycolate anion, which is a function of pH, plays an important role in controlling Pt particle size and loading on carbon. It was observed that Pt loading decreased with increasing alkalinity of the solution. As evidenced by zeta potential measurement, this was mainly due to poor adsorption or repulsive forces between the metal colloids and the supports. In order to modify the conventional polyol process, the effect of the gas purging conditions on the characteristics of Pt/C was examined. By the optimization of the gas environment during the reaction, it was possible to obtain high loading of 39.5wt% with a 2.8 nm size of Pt particle. From the single cell test, it was found that operating in ambient $O_{2}$ at 70oC can deliver high performance of more than 0.6 V at 1.44 A $cm^{-2}$.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2021년도 봄 학술논문 발표대회
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• pp.195-196
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• 2021

The pore distribution of the cement mortar mixed with carbon nanotubes was found to have a large number of pores at (370~80)㎛, and the distribution ratio was larger as the carbon nanotubes were mixed. However, the pores with a fine particle diameter of (10-0.5) ㎛ were found to be larger as the carbon nanotubes were incorporated. However, the distribution of pores of the test specimens of conductive cement mortar with deterioration damage was found to be distributed in a number of particle diameters of (500 to 100) ㎛ and (10 to 0.5) ㎛. It is judged that the particle diameter of the internal pores increased due to the damage. However, as the mixing ratio of the test specimen with carbon nanotubes increased, the distribution of voids was relatively lower than that of plain, and it was judged to have excellent resistance to deterioration damage.

• 대한설비공학회:학술대회논문집
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• 대한설비공학회 2008년도 하계학술발표대회 논문집
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• pp.189-193
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• 2008

Performance of refrigerant oil at the thrust-bearing and at the journal-bearing of a scroll compressor is a significant factor. This paper presents the friction and anti-wear characteristics of nano oil with a mixture of a refrigerant oil and carbon nano particles in the journal bearing of scroll compressors. The characteristics of friction and anti-wear using nano-oil is evaluated using the disk on disk tester and the journal bearing tester for measuring friction surface temperature and the coefficient of friction at the journal bearing tester. In journal bearing test, the average friction coefficient of high concentration nano-oil was decreased down to 18% compared to raw oil under 4,500 N and 3,600 rpm. It is believed that nano particles can be coated on the wear surfaces and the interaction of nano particles between surfaces can be improved the lubrication in the friction surfaces. Worn surfaces of frictional specimen were measured with straightness. carbon nano oil enhances the characteristics of the anti-wear and friction at the joural bearing of scroll compressors.

• 한국추진공학회지
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• 제19권6호
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• pp.42-53
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• 2015

고체추진제에 첨가되는 알루미늄 입자의 크기에 따른 탄소 복합재 노즐의 기계적 삭마특성 변화를 예측하는 연구를 수행하였다. 추진제에 첨가되는 알루미늄 입자의 초기 크기에 따라 연소생성물 응집체($Al(l)/Al_2O_3(l)$)의 크기와 분포를 예측할 수 있는 모델을 개발하여 사용하였으며, 모델 예측 결과로 얻어지는 응집체의 크기를 초기조건으로 하여 상용 수치해석 프로그램(STAR CCM+)을 이용한 복합재 노즐에서의 기계적 삭마특성 해석을 수행하였다. 본 연구를 통해 초기 알루미늄 첨가제의 크기가 작을수록 응집체의 크기가 작아지고, 기계적 삭마가 감소하는 특성을 확인하였으며, 특히 나노입자를 사용할 때 기계적 삭마가 확연히 개선됨을 확인하였다.